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Impact of the SiC addition on the morphological,structural and mechanical properties of Cu-SiC composite powders prepared by high energy milling
Affiliation:1. Mechanical Engineering Postgraduate Program, UFRN, 59078-970 Natal, Brazil;2. Federal Institute of Education, Science and Technology of Rio Grande do Norte, IFRN, 59291-727 Caicó, Brazil;3. Mechanical Engineering Postgraduate Program, UFPB, 58051-900 João Pessoa, Brazil;4. Department of Theoretical and Experimental Physics, UFRN, 59078-970 Natal, Brazil;5. Materials Science and Engineering Postgraduate Program, UFRN, 59078-970 Natal, Brazil;6. Federal University of São Carlos, Graduate Program in Materials Science and Engineering, 13565-905 São Carlos, Brazil;7. Materials Science and Engineering Postgraduate Program, UFPB, 58051-900 João Pessoa, Brazil
Abstract:The effect of the SiC content on the microstructural, mechanical, and magnetic properties of Cu(1 ? x)SiC(x) composite powders (x = 0, 2, 10 and 15 wt%) prepared by high energy milling for 30 h was investigated. The results showed that Cu particles were severely deformed and formed plate like particles of different sizes, while SiC particles were fragmented and embedded in the Cu phase, thus, forming composite particles. As the SiC content increased, the average particle size decreased from 40.75 to 12.84 µm. Besides, XRD data showed a decrease in the crystallite sizes of the Cu phase (from 23.66 to 21.56 nm), accompanied by an increase in the lattice micro-strain (from 0.41 to 0.46%). Changes in the lattice parameters of the Cu phase were observed. The Vickers microhardness were measured in compacted powder samples and reached a maximum value of 135.22 HV for the sample with 15 wt% SiC. The samples showed hysteresis magnetic behavior at 300 K, and with a maximum saturation magnetization of 0.123 emu/g. The weak magnetic signal is mainly due to Co impurities present in the WC from the milling media.
Keywords:High Energy Milling (HEM)  Cu-SiC composite powder  Microstructure  Magnetic properties  Mechanical property
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