| 氧化铟纳米立方块的合成及其自组装膜 |
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| 引用本文： | 王明峰,张敬,李福平,刘国栋.氧化铟纳米立方块的合成及其自组装膜[J].纳米科技,2013(4):43-47. |
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| 作者姓名： | 王明峰 张敬 李福平 刘国栋 |
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| 作者单位： | f济宁学院化学与化工系山东省高校无机化学重点实验室,山东济宁273155 |
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| 摘 要： | 以乙酰丙酮铟为前驱体，在不同的有机溶剂中进行溶剂热反应，得到棱角规则清晰、尺寸可控的立方相氧化铟纳米立方块，通过X射线粉末衍射（XRD）、透射电子显微镜（TEM）等对产品进行详细表征，采用层层自组装技术，将氧化铟纳米立方块自组装戍厚度可控的薄膜，UV-vis吸收光谱强度的线性增长为多层膜组装提供了证据，且对氧化铟纳米立方块及其自组装薄膜的光致发光光谱进行了测试。
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| 关 键 词： | 氧化铟 溶剂热 层层自组装 |
Synthesis of In2O3 Nanocuboids and the Self-assembled Films |
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| Authors: | WANG Ming-feng ZHANG Jing LI Fu-ping LIU Guo-dong |
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| Affiliation: | (Department of Chemistry and Chemical Engineering, Jining University, Key labratiry in Inorganic Chemistry of University, Jining 273155, China) |
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| Abstract: | In2O3 nanocubes were been solvothermally synthesized by taking indium acetylacetonate as precursor. The size of nanocubes was tunable by adjusting the solvent. Characterized by X-ray powder diffraction （XRD）,transmission electron microscope （TEM） techniques in detail. The film composed of the nanoeubes was fabricated onto various substrates via layer by layer self-assembly technique. UV-vis absorption spectroscopy provided evidence for subsequent growth of muhilayer film,which exhibuted progressive enhancement of optical absorption. PL spectrums of multilayer films were also detected. |
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| Keywords: | indium oxide solvothermal LBL self-assembled |
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