冷加工变形Pb-Ca-Sn合金位错类型、密度和晶粒尺寸分布的X射线衍射峰形分析(英文)

利用X射线衍射峰形分析方法,研究冷加工变形Pb-Ca-Sn合金的位错类型、密度和晶粒尺寸分布。结果表明:该合金的位错密度在1010cm-2数量级。衍射谱峰形的应变宽化可用位错对比因子来解释。利用新开发的PM2K软件包计算了晶粒尺寸。通过假设晶粒尺寸呈对数正态分布,利用X射线峰形分析得到的晶粒尺寸参数可得到晶粒分布函数。

X-ray peak profile analysis of dislocation type,density and crystallite size distribution in cold deformed Pb-Ca-Sn alloys

The density,nature of the dislocations and distribution of the domain sizes in cold-deformed Pb-Ca-Sn solid solution were determined by X-ray diffraction profile analysis.The dislocation densities are of the order of 1010 cm-2.The strain broadening of diffraction profiles was accounted for by dislocation contrast factor.The coherent domain size was determined by the recently developed PM2K software package.Assuming that the domain size distribution is log-normal,the distribution function(median μ and variance σ) was calculated from the size parameters determined from X-ray diffraction profile analysis.