| 松香基咪唑啉的合成及其性能的研究 |
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| 引用本文： | 何文深,谢晖,周永红.松香基咪唑啉的合成及其性能的研究[J].腐蚀科学与防护技术,2004,16(4):247-249. |
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| 作者姓名： | 何文深 谢晖 周永红 |
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| 作者单位： | 1. 南京工业大学,化工学院,南京,210009
2. 中国林业科学研究院,林产化工研究所,南京,210042 |
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| 摘 要： |
以松香和多乙烯多胺为原料合成了松香基咪唑啉(ORI)。并通过正交实验，对影响反应的各个因数进行模拟回归，得出适宜的反应条件：反应温度在230℃～240℃，二乙烯三胺和松香的摩尔用量比为1.6∶1，反应时间为5小时，体系的真空度2.67 kPa～5.33 kPa.
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| 关 键 词： | 松香 咪唑啉 合成 |
| 文章编号： | 1002-6495(2004)04-0247-03 |
| 收稿时间： | 2003-11-04 |
| 修稿时间： | 2003年11月4日 |
SYNTHESIS AND PROPERTIES OF ROSIN- BASED IMIDAZOLINE |
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| HE Wen-shen ,XIE Hui ,ZHOU Yong-hong .Nanjing University of Technology,Nanjing.SYNTHESIS AND PROPERTIES OF ROSIN- BASED IMIDAZOLINE[J].Corrosion Science and Protection Technology,2004,16(4):247-249. |
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| Authors: | HE Wen-shen XIE Hui ZHOU Yong-hong Nanjing University of Technology Nanjing |
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| Affiliation: | HE Wen-shen 1,XIE Hui 1,ZHOU Yong-hong 2 1.Nanjing University of Technology,Nanjing 210009, 2.Institute of Chemical Industry of Forest Products,CAF Nanjing 210042 |
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| Abstract: | SYNTHESIS AND PROPERTIES OF ROSIN-BASED IMIDAZOLINE
HE Wen-shen(1)，XIE Hu(1)，ZHOU Yong-hong(2)
1.Nanjing University of Technology；
2.Institute of Chemical Industry of Forest Products,CAF
A series of oil-soluble rosin-based imidazoline (ORI) were synthesized.The influence of some factors on the synthesis process of rosin-based imidazoline were studied.The optimal processing parameters were obtained through fractional factorial test: Reaction temperature was 230 ℃～240 ℃;the molar ratio of diethylene triamine (DETA) to rosin was 1.6∶1;reaction time was 5 h;and the reaction pressure was 2.67 kPa～5.33 kPa.
rosin；
imidazoline；
synthesis |
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| Keywords: | rosin imidazoline synthesis |
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