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Nb-Ti-Si 合金表面辉光离子渗 Mo / 包埋渗 Si制备 MoSi2 涂层的研究
引用本文:曹正,田晓东,李宁,王利捷,吕娜.Nb-Ti-Si 合金表面辉光离子渗 Mo / 包埋渗 Si制备 MoSi2 涂层的研究[J].表面技术,2015,44(1):68-71.
作者姓名:曹正  田晓东  李宁  王利捷  吕娜
作者单位:长安大学 材料学院,西安,710064
基金项目:国家自然科学基金项目,陕西省大学生创新创业训练计划项目(201410710112)Fund:Supported by the National Natural Science Foundation of China,Shaanxi Provincial College Students'Innovation and Entrepreneurship Training Program
摘    要:目的在Nb-Ti-Si合金表面制备MoSi2涂层。方法先进行辉光离子渗Mo,再进行包埋渗Si。分析温度对渗Mo层表面形貌、厚度、元素互扩散的影响,以及渗Si后涂层的表面形貌和结构。结果在1100℃进行辉光离子渗Mo,渗Mo层与基体形成了显著的互扩散。对渗Mo层进行包埋渗Si后,所形成的涂层组织致密,具有多层结构,由外向内依次为MoSi2层、NbSi2层和Nb5Si3层,在MoSi2和NbSi2层之间存在(Mo,Nb)Si2互扩散区。结论通过辉光离子渗/包埋渗的方法,可以在Nb-Ti-Si合金表面制备Mo Si2涂层,且涂层与基体呈冶金结合,结合较好。

关 键 词:Nb-Ti-Si合金  辉光离子渗  包埋渗  MoSi2涂层
收稿时间:8/3/2014 12:00:00 AM
修稿时间:2015/1/20 0:00:00

Preparation of MoSi2 Coating on Nb-Ti-Si Alloy by Glow Plasma Deposition of Mo / Pack Cementation of Si
CAO Zheng,TIAN Xiao-dong,LI Ning,WANG Li-jie and LYU Na.Preparation of MoSi2 Coating on Nb-Ti-Si Alloy by Glow Plasma Deposition of Mo / Pack Cementation of Si[J].Surface Technology,2015,44(1):68-71.
Authors:CAO Zheng  TIAN Xiao-dong  LI Ning  WANG Li-jie and LYU Na
Affiliation:School of Materials, Chang'an University, Xi'an 710064, China,School of Materials, Chang'an University, Xi'an 710064, China,School of Materials, Chang'an University, Xi'an 710064, China,School of Materials, Chang'an University, Xi'an 710064, China and School of Materials, Chang'an University, Xi'an 710064, China
Abstract:ABSTRACT:Objective To prepare the MoSi2 coating on the surface of Nb-Ti-Si alloy. Methods The coating was prepared through glow plasma deposition of Mo and pack siliconization. The effects of temperature on the microstructure, thickness and ele-ment distribution of the deposited Mo layer were analyzed, and the coating structure of the Mo layer after siliconization was investi-gated. Results Elements inter-diffusion between the glow plasma deposited Mo layer and the substrate was significant at 1100 °;after siliconization, dense MoSi2 coating was formed on the substrate. The MoSi2 coating had a multi-layer structure. From the sur-face to the substrate, the MoSi2 coating was consisted of the MoSi2 layer, the NbSi2 layer and the Nb5 Si3 layer;a ( Mo,Nb) Si2 in-ter-diffusion zone was formed between the MoSi2 layer and the NbSi2 layer. Conclusion The MoSi2 coating could be prepared on the surface of the Nb-Ti-Si alloy through glow plasma deposition of Mo/pack siliconization. The coating had metallurgical bonding with the substrate.
Keywords:Nb-Ti-Si alloy  glow plasma deposition  pack cementation  MoSi2 coating
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