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硅钢水溶性极厚绝缘涂层的热老化行为研究
引用本文:罗勃,储双杰,杨勇杰,黄杰,李登峰,王俊.硅钢水溶性极厚绝缘涂层的热老化行为研究[J].表面技术,2011,40(4):81-84.
作者姓名:罗勃  储双杰  杨勇杰  黄杰  李登峰  王俊
作者单位:上海交通大学材料科学与工程学院,上海,200240;上海交通大学材料科学与工程学院,上海200240;宝山钢铁股份有限公司,上海201900;宝山钢铁股份有限公司,上海,201900
摘    要:对两种硅钢水溶性极厚绝缘涂层进行了不同温度的热老化实验.通过TG-DTA,GDS,FT-IR,SEM和光泽度仪等测试方法对老化的涂层进行分析表征,提出了评估硅钢水溶性极厚绝缘涂层热老化性能的合理温度区间,探讨了涂层热老化行为,并分析了两种涂层热老化性能的差异.结果表明,涂层附着性随着老化时间的延长逐渐下降.FT-IR表...

关 键 词:硅钢  极厚绝缘涂层  热老化

Study on Thermal Aging Behaviors of Water-soluble and Extra-thick Insulation Coating for Silicon Steel
LUO Bo,CHU Shuang-jie,YANG Yong-jie,HUANG Jie,LI Deng-feng,WANG Jun.Study on Thermal Aging Behaviors of Water-soluble and Extra-thick Insulation Coating for Silicon Steel[J].Surface Technology,2011,40(4):81-84.
Authors:LUO Bo  CHU Shuang-jie  YANG Yong-jie  HUANG Jie  LI Deng-feng  WANG Jun
Affiliation:1(1.Institute of Meterial Science and Engineering,Shanghai Jiaotong University,Shanghai 200240,China;2.Baoshan Iron and Steel Co Ltd,Shanghai 201900,China)
Abstract:Thermal aging expriments at different temperature were carried out on two types of water-soluble and extra-thick insulation coatings for non-oriented silicon steel,and a series of test methods such as glossmeters,TG-DTA,FT-IR,GDS,SEM were applied in analysis.For evaluating the thermal aging effect of this kind of insulation coating,the proper temperature range was proposed.The difference of aging performance between two coatings was been investigated and the related behaviors were been discussed.The results indicate that the adhesion of coatings decreases with increasing thermal aging time.During the thermal aging,the fourier transfor infrared studies reveal that the chemical bond created by cross-linking reaction does not break,and the rupture of tridzine ring of amino resin is regarded as the main facor to destroy the three dimensional hydrophobic ploymer network.
Keywords:silicon steel  extra-thick insulation coating  thermal aging
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