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Application of electrophoretic deposition for inner surface coating of porous ceramic tubes
Authors:L Kreethawate  S Larpkiattaworn  L Besra
Affiliation:
  • a Research Unit of Advanced Ceramics, Department of Materials Science, Faculty of Science, Chulalongkorn University, Bangkok 10330, Thailand
  • b National Center of Excellence for Petroleum, Petrochemicals and Advanced Materials, Chulalongkorn University, Bangkok 10330, Thailand
  • c Thailand Institute of Scientific and Technological Research (TISTR), Technopolis, Khlong-Luang, Pathumthani 12120, Thailand
  • d Institute of Minerals and Materials Technology, Bhubaneswar 751 013, Orissa, India
  • e National Institute for Materials Science (NIMS), 1-2-1 Sengen, Tsukuba, Ibaraki 305-0047, Japan
  • Abstract:The direct coating of a nano-porous alumina layer on the inner surface of micro-porous alumina tubes was performed by electrophoretic deposition (EPD). A thin layer of polypyrrole (Ppy) was synthesized on the inside wall of the porous tubes by the chemical polymerization of pyrrole (Py) to give the wall electric conduction for the EPD electrode. The bimodal suspension of alumina powders with 0.6 μm and 30 nm average particle sizes was selected to control the nano-porous structure. The thickness of the coating layer was controlled by altering the applied voltage and deposition time. The interfacial connection of the coated layer and the substrate was observed by SEM before and after sintering. The pore size of the coated layer was characterized by its pore size distribution.
    Keywords:EPD  electrophoretic deposition  Ppy  polypyrrole  Py  pyrrole  APS  ammonium peroxodisulfate  NDA  2-6-naphthalenedisulfonic acid disodium salt
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