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Ni71CrSi中间层钎焊连接C/C复合材料与镍基高温合金GH3044
引用本文:张鑫,史小红,王杰,李贺军,李克智.Ni71CrSi中间层钎焊连接C/C复合材料与镍基高温合金GH3044[J].稀有金属快报,2013(11):665-670,675.
作者姓名:张鑫  史小红  王杰  李贺军  李克智
作者单位:西北工业大学凝同技术国家重点实验室C/C复合材料工程中心,陕西西安710072
摘    要:以Ni71CrSi为中间层存1180℃×30min的钎焊条件下,对C/C复合材料和镍基高温合金进行钎焊试验。,研究了Ni7lCrSi对C/C复合材料和表面SiC改性的C/C复合材料的润湿性。利用扫捕电子显微镜、能谱分析仪、万能试验机和做米压痕仪分别对接头的界面组织、显微硬度和剪圳断裂过程进行了研究。结果表明,表面未改性的C/C复合材料在连接过程中直接失效,而表而SiC改性的C/C复合材料与镍基合金的接头连接良好,且接头剪切强度达到35.08MPa,断裂方式呈假塑性断裂。机理分析表明,镍基钎料较好地润湿表面SiC改性的C/C复合材料,接头的显做硬度分布旱中问高两边低的变化趋势,且形成了表面改性C/C/Ni(s.s)+Cr7C3+Ni3Si/Ni(s.s)+cr3c2+Ni3Si/Ni(s.s)+cr3c2+MC+Ni3Si/Ni3Si+MC+Ni(s.s)/GH3044界面结构。

关 键 词:C  C复合材料  镍基高温合金  钉焊  界面结构  断裂方式

Brazing of C/C Composites and GH3044 Ni-Based Superalloy Using Ni71CrSi as the Interlayer
ZHANG Xin,SHI Xiaohong,WANG Jie,LI Hejun,LI Kezhi.Brazing of C/C Composites and GH3044 Ni-Based Superalloy Using Ni71CrSi as the Interlayer[J].Rare Metals Letters,2013(11):665-670,675.
Authors:ZHANG Xin  SHI Xiaohong  WANG Jie  LI Hejun  LI Kezhi
Affiliation:(C/C Composites Technology Research Center, State Key Laboratory of Solidification Processing Northwestern Polytechnical University, Xi' an 710072, China)
Abstract:C/C composites and Nickle-based superalloy GH3044 were brazed at 1 180 ℃ for 30 rain using the Ni71CrSi filler as interlayer. The wettability of filler on the surface of C/C composites and SiC modified C/C composites was stud- ied. The mierostructure, microhardness and shear fi'acture of the joint between C/C composites and GH3044 were investi- gated by scanning electron microscopy, energy-dispersive spectrometry, material universal testing machine and Micro-in- dentation instrument, respectively. Results showed that the joint without SiC coating got failed during the brazing process. Ni71 CrSi can well braze Niekle-based superalloy and C/C composites with SiC coating. The shear strength of joint with SiC coating at room temperature was up to 35, 08 MPa. The joint exhibited pseudo-plastic fracture behavior. Mechanism analy- sis indicated that this filler could wet modified C/C composites well. The hardness distribution of the joint presented a trend with high value at the middle and low value at the both sides, and the interracial structure of joints was: C/C com- posites with SiC coatingv/Ni( s. s) + CrTC3 + Ni3Si/Ni( s, s) + Cr3C2 + Ni3Si/Ni( s. s) + Cr3C2 + MC + Ni3Si/Ni3Si + MC + Ni( s. s)/GH3044.
Keywords:C/C composites  Nickle-based superalloy  brazing  interracial structure  fracture mechanisms
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