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Mo-Nb合金单晶晶向测定和表征
引用本文:胡忠武,李中奎,郭林江,殷 涛,郭振祺. Mo-Nb合金单晶晶向测定和表征[J]. 稀有金属材料与工程, 2011, 40(11): 2006-2009
作者姓名:胡忠武  李中奎  郭林江  殷 涛  郭振祺
作者单位:1. 西北有色金属研究院,陕西西安,710016
2. 西安交通大学,陕西西安,710049
摘    要:采用一种金相和RO-XRD相结合的方法,快速、准确地测定Mo-Nb合金单晶的晶向,并对晶向品质做出精确的表征。所测Mo合金单晶,其(111)晶面衍射角的测试值与计算值基本一致,其晶向偏离角分别为0.73o和0.91o,与电子背散射衍射法测试的结果一致,晶向分散度仅为1o左右。

关 键 词:单晶  RO-XRD法  金相  晶向偏离角
收稿时间:2011-03-21

Measurement and Evaluation of Orientation for Mo-Nb Alloy Single Crystal
Hu Zhongwu,Li Zhongkui,Guo Linjiang,Yin Tao and Guo Zhenqi. Measurement and Evaluation of Orientation for Mo-Nb Alloy Single Crystal[J]. Rare Metal Materials and Engineering, 2011, 40(11): 2006-2009
Authors:Hu Zhongwu  Li Zhongkui  Guo Linjiang  Yin Tao  Guo Zhenqi
Affiliation:Hu Zhongwu1,Li Zhongkui1,Guo Linjiang1,Yin Tao1,Guo Zhenqi2(1.Northwest Institute for Nonferrous Metal Research,Xi'an 710016,China)(2.Xi'an Jiaotong University,Xi'an 710049,China)
Abstract:A method combining optical metallograph with rotating orientation X-ray diffraction was applied for the measurement and evaluation of orientation for molybdenum-niobium alloy single crystal quickly and accurately. The diffraction angle of (111) orientation plane measured by this method almost accords with the calculated value. The disorientation angles of the samples are 0.73 o and 0.91o, respectively, which are consistent with the results measured by EBSD. The degree of scatter in the preferred orientation is about 1o
Keywords:single crystal   rotation orientation X-ray diffraction   optical metallograph   disorientation angle
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