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热处理对热电Bi2Te2.7Se0.3“纳米花”材料形貌的影响
引用本文:李晓龙,周春生,杨超普,李哲建,邸友莹,李峰,王晴玉,郭明.热处理对热电Bi2Te2.7Se0.3“纳米花”材料形貌的影响[J].稀有金属材料与工程,2021,50(11):3966-3970.
作者姓名:李晓龙  周春生  杨超普  李哲建  邸友莹  李峰  王晴玉  郭明
作者单位:商洛学院,商洛学院,商洛学院,商洛学院,商洛学院,商洛学院,商洛学院,西安建筑科技大学环境与市政工程学院
基金项目:国家自然科学基金资助(项目号No.21873063)和商洛学院科研基金资助(项目号:19SKY001)
摘    要:采用bottom-up制备纳米材料技术,在ITO导电玻璃上电化学恒电位沉积制备了一种由纳米线变异为纳米带,进而构成的“纳米花”形貌的热电材料。采用FE-SEM技术手段对纳米花形貌进行研究,探讨了热电纳米花材料的形成机理,模拟了纳米花形成过程。结果分析表明,纳米花是经过两个阶段形成的:首先是纳米线在热处理过程逐渐形成纳米带,然后,由纳米带收缩形成纳米花;热处理条件对纳米花的形成起到决定性的作用。

关 键 词:纳米花  机理  热处理  热电材料
收稿时间:2020/11/8 0:00:00
修稿时间:2020/11/28 0:00:00

The Effect of Thermal Treatment on the Morphology of Flower-shaped Thermoelectric Bi2Te2.7Se0.3 Materials
Li Xiaolong,Zhou Chunsheng,Yang Chaopu,Li Zhejian,Di Youying,Li Feng,Wang Qingyu and Guo Ming.The Effect of Thermal Treatment on the Morphology of Flower-shaped Thermoelectric Bi2Te2.7Se0.3 Materials[J].Rare Metal Materials and Engineering,2021,50(11):3966-3970.
Authors:Li Xiaolong  Zhou Chunsheng  Yang Chaopu  Li Zhejian  Di Youying  Li Feng  Wang Qingyu and Guo Ming
Abstract:Following the bottom-up technology, the flower-shaped nanomaterials consisted of nanobelts and nanowirs were fabricated on ITO-coated glass substrate by electrodeposition. The morphology of the as-prepared nano-flower was analized by FE-SEM. Moreover, the forming process was simulated. The results showed that the nano-flowers were fabricated through the two steps: first, nanowires formed gradually into nanobelts during the couse of thermal treatment; second, nanobelts contracted into nano-flowers. In addition, the conditions of thermal treatment played the determined role on the flower-shaped Bi2Te2.7Se0.3thermoelectric materials.
Keywords:Nano-flower  Mechanism  Thermal treatment  Thermoelectric materials
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