| 3-氨基4-(叠氮乙酰胺基)呋咱合成 |
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| 引用本文： | 李战雄,唐松青,刘金涛,钱国兴.3-氨基4-(叠氮乙酰胺基)呋咱合成[J].含能材料,2002,10(3):112-113. |
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| 作者姓名： | 李战雄 唐松青 刘金涛 钱国兴 |
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| 作者单位： | 中国科学院上海有机化学研究所,上海,200032 |
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| 摘 要： | 以3，4－二氨基呋咱（DAF）分别和氯乙酰氯、溴乙酰缩合得到了单取代乙酰化产物，进一步叠氮化得到的3－氨基－4－（叠氮乙酰胺基）呋咱为高氮含量的呋咱含能衍生物。
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| 关 键 词： | 3 4二氨基呋咱 叠氮乙酰胺基 DAF 乙酰化 叠氮化 炸药 |
| 文章编号： | 1006-9941(2002)03-0112-02 |
| 收稿时间： | 2002/4/17 0:00:00 |
| 修稿时间： | 2002年4月17日 |
Synthesis of 3-Amino-4-(azidoacetamido)Furazan |
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| LI Zhan-xiong,TANG Song-qing,LIU Jin-tao and QIAN Guo-xing.Synthesis of 3-Amino-4-(azidoacetamido)Furazan[J].Chinese Journal of Energetic Materials,2002,10(3):112-113. |
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| Authors: | LI Zhan-xiong TANG Song-qing LIU Jin-tao and QIAN Guo-xing |
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| Affiliation: | Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032,China;Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032,China;Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032,China;Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, Shanghai 200032,China |
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| Abstract: | The acetylation of 3,4-diaminofurazan (DAF) was studied in this paper. By the reaction of DAF with chloroacetyl chloride and bromoacetyl bromide respectively, the substituted acetyl furazano derivatives were obtained. Then 3-amino-4-(azidoacetamido)furazan was obtained as an high nitrogen content furazano energetic derivative by treating these two intermediates with sodium azide. |
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| Keywords: | 3 4-diaminofurazan acetylation azidation |
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