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动态真空安定性试验方法研究(Ⅰ)
引用本文:张同来,胡晓春,杨利,李坤远,张建国,王文杰,王丽琼.动态真空安定性试验方法研究(Ⅰ)[J].含能材料,2009,17(5):549-553.
作者姓名:张同来  胡晓春  杨利  李坤远  张建国  王文杰  王丽琼
作者单位:1. 北京理工大学爆炸科学与技术国家重点实验室,北京,100081
2. 北京理工大学爆炸科学与技术国家重点实验室,北京,100081;防化指挥工程学院三系,北京,102205
基金项目:爆炸科学与技术国家重点实验室基金项目 
摘    要:为了研究含能材料的安定性、相容性和长储寿命,在真空和加热条件下测试含能材料的热分解过程,在真空安定性(VST)原理基础上,建立了压力和温度传感器全内置式的动态真空安定性试验(dynamic vacuum stabilitytest,DVST)测试装置及方法,实现了对含能材料真空安定性的实时、在线、连续、直接跟踪测试,为精确研究含能材料的安定性、预估储存寿命提供了一种新方法。

关 键 词:物理化学  动态真空安定性试验(DVST)  相容性  长储寿命  动力学
收稿时间:2009/2/20 0:00:00
修稿时间:2009/6/22 0:00:00

Study on Dynamic Vacuum Stability Test Method (Ⅰ)
ZHANG Tong-lai,HU Xiao-chun,YANG Li,LI Kun-yuan,ZHANG Jian-guo,WANG Wen-jie and WANG Li-qiong.Study on Dynamic Vacuum Stability Test Method (Ⅰ)[J].Chinese Journal of Energetic Materials,2009,17(5):549-553.
Authors:ZHANG Tong-lai  HU Xiao-chun  YANG Li  LI Kun-yuan  ZHANG Jian-guo  WANG Wen-jie and WANG Li-qiong
Affiliation:State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China;The 3rd Department, Institute of Chemical Defense,Beijing 102205,China;State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China;State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China;State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China;State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China;State Key Laboratory of Explosion Science and Technology, Beijing Institute of Technology, Beijing 100081,China
Abstract:In order to study the stability, compatibility, storage life and the decomposition mechanism of the energetic materials, a new test method named dynamic vacuum stability test (DVST) was established based on the principle of vacuum stability test method. The related instrument was set up with all internal-planted pressure sensor and temperature sensor in the test tube. The changes of the pressure and temperature of the tested samples can be detected real-time directly with the instrument. So the materials can be investigated continuously online. It provides a more accurate result of the stability for the tested materials after proper analysis of the acquired data from the instrument.
Keywords:physical chemistry  dynamic vacuum stability test (DVST)  compatibility  storage life  kinetics
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