| PET核孔膜制备纳米钯及其形貌观测 |
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| 引用本文： | 周敏兰,傅元勇,刘义保,焦学胜,鞠薇,梁海英,吴振东.PET核孔膜制备纳米钯及其形貌观测[J].原子能科学技术,2016,50(1):178-180. |
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| 作者姓名： | 周敏兰 傅元勇 刘义保 焦学胜 鞠薇 梁海英 吴振东 |
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| 作者单位： | 1.东华理工大学 教育部核技术应用工程研究中心，江西 南昌330013；2.中国原子能科学研究院 核物理研究所，北京102413 |
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| 摘 要： | 采用径迹蚀刻的聚酯（PET）膜制作核孔膜模板，辅助电化学沉积法制备了纳米钯。利用扫描电子显微镜（SEM）和能量色散X射线光谱仪（EDX）对纳米钯的形貌和成分进行了表征。结果显示，在沉积电位为-0.65 V时，此法制备的纳米钯颗粒均匀，且呈阵列分布，长径比分布范围为5～70。
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| 关 键 词： | 聚酯膜 核孔膜模板 电化学沉积 纳米钯 |
Preparation and Morphology Observation of Nano-palladium with PET Nuclear Pore Membrane |
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| ZHOU Min-lan,FU Yuan-yong,LIU Yi-bao,JIAO Xue-sheng,JU Wei,LIANG Hai-ying,WU Zhen-dong.Preparation and Morphology Observation of Nano-palladium with PET Nuclear Pore Membrane[J].Atomic Energy Science and Technology,2016,50(1):178-180. |
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| Authors: | ZHOU Min-lan FU Yuan-yong LIU Yi-bao JIAO Xue-sheng JU Wei LIANG Hai-ying WU Zhen-dong |
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| Affiliation: | 1.Engineering Research Center of Nuclear Technology Application, Ministry of Education, East China Institute of Technology, Nanchang 330013, China; 2.China Institute of Atomic Energy, P. O. Box 275-118, Beijing 102413, China |
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| Abstract: | The nuclear pore membrane template was obtained with the aid of track‐etched polyester (PET) film .The nano‐palladium was produced in the template by elec‐trodeposition .The morphology and composition of the nano‐palladium were character‐ized by scanning electron microscope (SEM ) and energy dispersive X‐ray spectrometer (EDX) respectively .Results show that the nano‐palladium particles by this method are even and distribute in array ,and the ratio of length to diameter ranges from 5 to 70 w hen the deposition potential is -0.65 V . |
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| Keywords: | polyester film nuclear pore membrane template electrodeposition nano-palladium |
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