| 乙酰丙酮分光光度法检测菌菇类及水产品中甲醛含量的研究 |
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| 引用本文： | 华红慧,岳振峰,郑卫平,林燕奎,韩瑞阳,王耀宇.乙酰丙酮分光光度法检测菌菇类及水产品中甲醛含量的研究[J].食品科学,2007,28(4):273-276. |
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| 作者姓名： | 华红慧 岳振峰 郑卫平 林燕奎 韩瑞阳 王耀宇 |
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| 作者单位： | 深圳出入境检验检疫局食品检验检疫技术中心； 深圳出入境检验检疫局食品检验检疫技术中心 广东 深圳 518067； 广东 深圳 518067； |
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| 摘 要： | 采用乙酰丙酮分光光度法检测菌菇类及水产品中甲醛的含量。本方法采用试样低温浸泡预处理,加磷酸溶液蒸馏提取,且控制冷凝水温≤10℃,然后用分光光度法测定试样中甲醛含量。通过对检测条件的优化,甲醛的测定低限为0．1mg/kg。甲醛的加标回收率可达90%～111%,相对标准偏差为5．6%～8．5%。
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| 关 键 词： | 甲醛 分光光度法 菌菇类 水产品 |
| 文章编号： | 1002-6630（2007）04-0273-04 |
| 修稿时间： | 2006-04-30 |
Study on Determination of Formaldehyde in Mushroom and Aquatic Products by Acetyl-acetone Spectrophotometric Method |
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| HUA Hong-hui,YUE Zhen-feng,ZHENG Wei-ping,LIN Yan-kui,HAN Rui-yang,WANG Yao-yu.Study on Determination of Formaldehyde in Mushroom and Aquatic Products by Acetyl-acetone Spectrophotometric Method[J].Food Science,2007,28(4):273-276. |
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| Authors: | HUA Hong-hui YUE Zhen-feng ZHENG Wei-ping LIN Yan-kui HAN Rui-yang WANG Yao-yu |
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| Affiliation: | Technical Center for Food Inspection and Quarantine,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen 518067,China |
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| Abstract: | Acetyl-acetone spectrophotometric method is adopted to analyze the content of formaldehyde in mushroom and aquatic products.The sample is soaked in water at low temperature before adding phosphoric acid and distilling,and the temperature of cooling water is controlled below 10℃and at last the content of formaldehyde in sample is analyzed by spectrophotometer.Through the opitimization of the analysis conditions,the limit of quantitation is 0.1mg/kg,the recovery is between 90% and 111%,and the relative standard deviation is between 5.6%～8.5%. |
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| Keywords: | formaldehyde spectrophotometric method mushroom aouatic oroduct |
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