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精炼餐饮业地沟油挥发性危害成分的GC/MS静态顶空分析
引用本文:全常春,尹平河,赵玲,单习章,张璇,余汉豪.精炼餐饮业地沟油挥发性危害成分的GC/MS静态顶空分析[J].食品科学,2004,25(4):128-134.
作者姓名:全常春  尹平河  赵玲  单习章  张璇  余汉豪
作者单位:1. 暨南大学生命科学技术学院,广东,广州,510632
2. 广州越秀区环境保护局,广东,广州,510045
基金项目:国家自然科学基金项目(20277016)
摘    要:精炼地沟油就是从餐饮业下水道隔油池中捞取的废油酯,经过一系列的工艺加工处理而得到的油脂。由于经过了多次的使用和复杂环境条件的影响,油脂会发生变质或者引入一些有害成分。在暴利的驱使下,不法分子将其回流到食用油市场中,给人们的健康带来极大的危害。本文应用气质联用的静态顶空方法,对精炼地沟油的易挥发成分进行了检测,实验结果表明,该样品油中含有大量的烷烃(从C9到C14)和油脂氧化变质的二级产物—己醛。

关 键 词:餐饮业  废油酯  精炼地沟油  挥发性成分  有害成分  GC/MS静态顶空法
文章编号:1002-6630(2004)04-0128-07

Assay on the Harmful Volatile Components of the Refined Waste Edible Oil Gained from the Restaurant Sewer by Static Headspace and Gas Chromatography/Mass Spectrometry
QUAN Chang-chun,YIN Ping-he,ZHAO Ling,SHAN Xi-zhang,ZHANG Xuan,YU Han-hao.Assay on the Harmful Volatile Components of the Refined Waste Edible Oil Gained from the Restaurant Sewer by Static Headspace and Gas Chromatography/Mass Spectrometry[J].Food Science,2004,25(4):128-134.
Authors:QUAN Chang-chun  YIN Ping-he  ZHAO Ling  SHAN Xi-zhang  ZHANG Xuan  YU Han-hao
Affiliation:QUAN Chang-chun1,YIN Ping-he1*,ZHAO Ling1,SHAN Xi-zhang2,ZHANG Xuan2,YU Han-hao2
Abstract:The refined oil gained from the waste edible oil sewer collected from the waste edible oil pool of restaurants wasconducted by a series of refining methods. For being used repeatedly many times and influenced by the complex environmentalconditions, the refined oil would deteriorate or be introduced with some harmful component. If unlawfully sold in the edible oilmarket, it would do much harm to human health. This paper described a qualitative assay method of the volatile compounds ofthe refined edible oil gained from the sewer by static headspace and gas chromatography/mass spectrometry. Alarge amount ofalkane, from n-C9 to n-C14, and the second grade production of the deteriorated oil hexanal were identified in this experiment.
Keywords:static headspace  GC-MS  waste edible oil  oil gained from the sewer  volatile compound
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