| 纺织品中6种禁用有机磷阻燃剂的超声萃取—气相色谱法测定 |
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| 引用本文： | 王成云,张伟亚,谢堂堂,褚乃清,李燕华,唐莉纯,张恩颂,沈雅蕾,刘彩明,李丽霞.纺织品中6种禁用有机磷阻燃剂的超声萃取—气相色谱法测定[J].产业用纺织品,2011,29(10):42-46. |
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| 作者姓名： | 王成云 张伟亚 谢堂堂 褚乃清 李燕华 唐莉纯 张恩颂 沈雅蕾 刘彩明 李丽霞 |
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| 作者单位： | 深圳出入境检验检疫局,深圳,518045 |
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| 基金项目： | 深圳出入境检验检疫局科技计划项目(SZ2010014); 认监委制标项目(2011B238k)资助 |
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| 摘 要： | 以丙酮为萃取溶剂,超声萃取阻燃纺织品中的禁用有机磷阻燃剂,采用火焰光度检测器(FPD)进行检测,从而建立了一种气相色谱方法,对阻燃纺织品中6种禁用有机磷阻燃剂进行了同时测定,并对萃取条件进行了优化。该方法简便快速、灵敏度高,6种目标分析物的检出限均低于3.0 ng/mL,方法的加标回收率为81.26%～96.77%,相对标准偏差为3.18%～6.45%。应用该方法对市售的阻燃纺织品中禁用有机磷阻燃剂含量进行了测定,结果发现部分阻燃纺织品中检出高含量的禁用有机磷阻燃剂。
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| 关 键 词： | 超声萃取 GC-FPD 纺织品 禁用有机磷阻燃剂 |
Determination of six kinds of banned organophophrous flame retardants in textiles by gas chromatography combined with ultrasonic extraction |
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| Wang Chengyun,Zhang Weiya,Xie Tangtang,Zhu Naiqing,Li Yanhua,Tang Lichun,Zhang Ensong,Shen Yalei,Liu Caiming,Li Lixia.Determination of six kinds of banned organophophrous flame retardants in textiles by gas chromatography combined with ultrasonic extraction[J].Technical Textiles,2011,29(10):42-46. |
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| Authors: | Wang Chengyun Zhang Weiya Xie Tangtang Zhu Naiqing Li Yanhua Tang Lichun Zhang Ensong Shen Yalei Liu Caiming Li Lixia |
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| Affiliation: | Wang Chengyun,Zhang Weiya,Xie Tangtang,Zhu Naiqing,Li Yanhua,Tang Lichun,Zhang Ensong,Shen Yalei,Liu Caiming,Li Lixia(Shenzhen Entry-Exit Inspection and Quarantine Bureau) |
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| Abstract: | An analytical method based on gas chromatography was established to determine simultaneously the contents of six banned organophophrous flame retardants in textiles.Organophosphrous flame retardants in textiles were first ultrasonically extracted with acetone as the extraction solvent and the extracted analytes were analyzed with flame photometric detector(FPD).The extraction conditions were optimized.The detection limits were all less than 3.0 ng/mL for all six banned organophosphrous flame retardants.The ... |
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| Keywords: | ultrasonic extraction GC-FPD textile banned organophosphrous flame retardant |
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