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干法制备氧化淀粉的工艺研究
引用本文:刘冠军,董海洲,侯汉学,邱立忠,王希功.干法制备氧化淀粉的工艺研究[J].食品与发酵工业,2005,31(11):71-74.
作者姓名:刘冠军  董海洲  侯汉学  邱立忠  王希功
作者单位:1. 山东农业大学食品科学与工程学院,泰安,271018
2. 山东诸城兴贸玉米开发有限公司,诸城,262200
摘    要:以H_2O_2为氧化剂,在碱催化剂存在的条件下干法制备出氧化淀粉。并对反应温度、反应时间、反应体系水的质量分数、NaOH与淀粉的摩尔比和H_2O_2与淀粉的摩尔比对氧化淀粉羧基含量的影响进行了研究。在固定反应时间3h,以及H_2O_2与淀粉的摩尔比0.225的条件下,选择反应温度、反应体系水的含量、NaOH与淀粉的摩尔比为三因素,采用正交实验,确定出制备氧化淀粉的最佳工艺参数为:反应温度60℃、反应体系水的质量分数为26.5%、NaOH与淀粉的摩尔比为0.135。

关 键 词:氧化淀粉  双氧水  羧基含量  干法工艺
收稿时间:06 20 2005 12:00AM
修稿时间:09 27 2005 12:00AM

Studies on Dry Preparation of Oxidized Starch
Liu Guanjun,Dong Haizhou,Hou Hanxue,Qiu Lizhong,Wang Xigong.Studies on Dry Preparation of Oxidized Starch[J].Food and Fermentation Industries,2005,31(11):71-74.
Authors:Liu Guanjun  Dong Haizhou  Hou Hanxue  Qiu Lizhong  Wang Xigong
Affiliation:1.College of Food Science and Engineering, Shandong Agriculture University, Taian, 271018, China; 2.Zhucheng Xingmao Corn Developing Co. , LTD, Zhucheng, 262200, China
Abstract:The Oxidized starch was prepared by dry method with Hydrogen-peroxide. The effect of reaction temperature, reaction time, the mole of sodium hydroxide/starch ratio, water content and the mole of Hydrogenperoxide/starch ratio on the carboxyl content were studied. The reaction temperature, water content and the mole of sodium hydroxide/starch ratio were selected as three factors with the reaction time (3h) and the mole of Hydrogen-peroxide/starch ratio(0.226) fixed. The optimum conditions were obtained by orthogonal design as followings: reaction temperature 60℃, the water content is 26.5%, the mole of sodium hydroxide/starch ratio 0.135.
Keywords:oxidized starch  hydrogen-peroxide  carboxyl content  dry preparation
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