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低温碱法脱酯制取低酯果胶的研究
引用本文:雷激,马力,赵义梅,邹立,许杰. 低温碱法脱酯制取低酯果胶的研究[J]. 食品与发酵工业, 2006, 32(1): 45-48
作者姓名:雷激  马力  赵义梅  邹立  许杰
作者单位:西华大学生物工程学院,成都,610039
基金项目:四川省科技厅资助项目;四川省科技厅资助项目;四川省教育厅资助项目
摘    要:以商品柑橘高酯果胶为原料,重点探讨了低温碱法脱酯对果胶质量的影响。以果胶的半乳糖醛酸含量、酯化度(DE值)、特性粘度等指标为考察依据。结果表明,低温下(5℃)碱法脱酯可将影响果胶品质的β-消去反应控制在较小程度,所得产品特性粘度能最大程度保持。柑橘高酯果胶碱法脱酯的最佳工艺条件为:pH 9.0,控制5℃低温处理30 min,该条件所得果胶半乳糖醛酸含量为81.387%,DE值为38.95%,指标达到低酯果胶产品的标准。

关 键 词:低酯果胶  碱法脱酯  β-消去反应
收稿时间:2005-09-26
修稿时间:2005-12-15

Study on the Low Ester Pectin Made by Base Catalysed De-esterification of High Ester Citrus Pectin
Lei Ji,Ma Li,Zhao Yimei,Zou Li,Xu Jie. Study on the Low Ester Pectin Made by Base Catalysed De-esterification of High Ester Citrus Pectin[J]. Food and Fermentation Industries, 2006, 32(1): 45-48
Authors:Lei Ji  Ma Li  Zhao Yimei  Zou Li  Xu Jie
Affiliation:Bioteehnology College, Xihua University, Chengdu 610039, China
Abstract:High ester(methyl) citrus pectin(HM-pectin) was used to produce a low ester pectin under low temperature.Parameters such as galacturonic acid contents,degree of esterification(DE) and specific viscosity of the pectin were tested.The results indicated that de-esterification at low temperature(5℃) gave lessβ-elimination reaction,with better specific viscosity retained.Under this temperature,with the esterification time of 30 min and the pH maintained to 9.0,a low ester pectin product with DE of 38.95%,galacturonic acid of 81.387% and specific viscosity of 2.177 was produced,which met the low pectin requirements of Eruopean Union standard.
Keywords:low ester pectin  base catalysed de-esterification  β-elimination
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