| 气相色谱法测定鲜枸杞中氧乐果农药残留量的不确定度评定 |
| |
| 引用本文： | 郭军霞,成 娟,雷 茜,何智宏,王永兰,郭明玲,卜金忠.气相色谱法测定鲜枸杞中氧乐果农药残留量的不确定度评定[J].食品安全质量检测技术,2020,11(20):7570-7575. |
| |
| 作者姓名： | 郭军霞 成 娟 雷 茜 何智宏 王永兰 郭明玲 卜金忠 |
| |
| 作者单位： | 甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心,甘肃省林业科技推广总站，国家林业和草原局经济林产品质量检验检测中心（兰州），甘肃省林果产品质量监督检验检测中心 |
| |
| 基金项目： | 甘肃省林业和草原局2019年林业科技创新与国际合作省级财政资金计划项目《甘肃枸杞质量安全监测与风险评估研究》 |
| |
| 摘 要： | 目的 评定气相色谱法测定鲜枸杞中氧乐果含量的不确定度。方法 参考JJF 1059.1-2012《测量不确定度评定与表示》,应用国家农业行业标准NY/T 761-2008《蔬菜和水果中有机磷、有机氯、拟除虫菊酯和氨基甲酸酯类农药多残留的测定》对鲜枸杞中氧乐果农药残留进行检测,并对其测定过程的不确定度进行了评定和分析。结果 在鲜枸杞中的氧乐果含量测定中,当样品的氧乐果含量为0.045 mg/kg时,其扩展不确定度为0.006 mg/kg(k=2),结果表示为(0.045±0.006)mg/kg。结论 鲜枸杞中氧乐果农药残留测量结果的主要不确定度来自样品重复测量,标准溶液配制,样品前处理、定容,标准溶液重复测定,样品称量5个因素,其中样品重复测量引入的相对标准不确定度分量贡献最大,而由样品称量引入的相对标准不确定度分量最小。
|
| 关 键 词： | 鲜枸杞 气相色谱法 氧乐果 不确定度 |
| 收稿时间： | 2020/6/8 0:00:00 |
| 修稿时间： | 2020/10/14 0:00:00 |
Evaluation of uncertainty in determination of omethoate pesticide residues in fresh wolfberry by gas chromatography |
| |
| GUO Jun-Xi,CHENG Juan,LEI Xi,HE Zhi-Hong,WANG Yong-Lan,GUO Ming-Ling,PU Jin-Zhong.Evaluation of uncertainty in determination of omethoate pesticide residues in fresh wolfberry by gas chromatography[J].Food Safety and Quality Detection Technology,2020,11(20):7570-7575. |
| |
| Authors: | GUO Jun-Xi CHENG Juan LEI Xi HE Zhi-Hong WANG Yong-Lan GUO Ming-Ling PU Jin-Zhong |
| |
| Affiliation: | Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province,Forestry Sci-tech Extension Station of Gansu Province,National Forestry and Grassland Administration Economic Forest Products Quality Inspection and Testing Center Lanzhou,Forestry and Fruit Products Quality Supervision and Inspection Center of Gansu Province |
| |
| Abstract: | |
| |
| Keywords: | Fresh wolfberry Gas chromatography Omethoate Uncertainty |
|
| 点击此处可从《食品安全质量检测技术》浏览原始摘要信息 |
|
点击此处可从《食品安全质量检测技术》下载全文 |
|
