| 在线凝胶渗透色谱-串联气质联用法测定植物油和猪肉中55 种农药残留 |
| |
| 引用本文： | 吴卫东,吴凤琪,万志刚,靳保辉,陈 波,沈金灿,吕 杰,叶 英.在线凝胶渗透色谱-串联气质联用法测定植物油和猪肉中55 种农药残留[J].食品安全质量检测技术,2014,5(11):3400-3409. |
| |
| 作者姓名： | 吴卫东 吴凤琪 万志刚 靳保辉 陈 波 沈金灿 吕 杰 叶 英 |
| |
| 作者单位： | 深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,深圳出入境检验检疫局食品检验检疫技术中心,岛津企业管理中国有限公司 |
| |
| 基金项目： | 质检总局科技计划项目（2012IK188，2014IK118），深圳市基础研究计划（JC201105190972A） |
| |
| 摘 要： | 目的 建立植物油和动物组织中55种农药残留的快速检测方法。 方法 样品用经改进的QuEChERS方法提取净化,提取液采用在线GPC/GC-MS检测。结果 在0.01~0.20 mg/L范围内各农药组分具有良好的线性关系,相关系数均在0.992以上。方法的加标回收率在60%~130%之间。55种农药定量下限范围为0.005~0.03 mg/kg。结论 该方法操作简便、快速、灵敏、准确,适合于植物油和动物组织中55种农药残留的测定。
|
| 关 键 词： | 在线凝胶渗透色谱气相色谱质谱联用法 植物油 动物组织 农药残留 |
| 收稿时间： | 2014/10/15 0:00:00 |
| 修稿时间： | 2014/11/5 0:00:00 |
Determination of 55 pesticide residues in vegetable oil and animal tissues using on-line gel permeation chromatography coupled with gas chromatogra-phy-mass spectrometry |
| |
| WU Wei-Dong,WU Feng-Qi,WANG Zhi-Gang,JIN Bao-Hui,CHEN Bo,SHEN Jin-Can,LV Jie and YE Ying.Determination of 55 pesticide residues in vegetable oil and animal tissues using on-line gel permeation chromatography coupled with gas chromatogra-phy-mass spectrometry[J].Food Safety and Quality Detection Technology,2014,5(11):3400-3409. |
| |
| Authors: | WU Wei-Dong WU Feng-Qi WANG Zhi-Gang JIN Bao-Hui CHEN Bo SHEN Jin-Can LV Jie and YE Ying |
| |
| Affiliation: | Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shenzhen Key Laboratory of Detection Technology R D on Food Safety,Food Inspection and Quarantine Center,Shenzhen Entry-Exit Inspection and Quarantine Bureau,Shimadzu ChinaCo,LTD,Guang Zhou |
| |
| Abstract: | Objective To establish a method for the simultaneous determination of 55 pesticide residues in vegetable oil and animal tissues . Methods The samples were extracted and purified by a modified QuEChERS method,and then the supernatant was analyzed by on-line GPC/GC-MS system. Results The calibration curves of 55 pesticide residues were linear in the range of 0.01~0.20 mg/L with good correlation coefficients more than 0.992. The recoveries of the method ranged from 60% to 130%.The limits of quantification were 0.005~0.03mg/kg. Conclusions The method was simple,rapid and reliable, and could meet the requirement the simultaneous determination and analysis of 55 pesticide residues in vegetable oil and animal tissues. |
| |
| Keywords: | on-line GPC/GC-MS system vegetable oil animal tissues pesticides |
|
| 点击此处可从《食品安全质量检测技术》浏览原始摘要信息 |
|
点击此处可从《食品安全质量检测技术》下载全文 |
|
