| 气相色谱-质谱联用法测定食品纸包装材料中的多氯联苯 |
| |
| 引用本文： | 白彦坤,郭丽敏,李强.气相色谱-质谱联用法测定食品纸包装材料中的多氯联苯[J].分析仪器,2011(5):18-21. |
| |
| 作者姓名： | 白彦坤 郭丽敏 李强 |
| |
| 作者单位： | 1. 河北省食品质量监督检验研究院,石家庄,050091
2. 河北省食品安全重点实验室,石家庄,050091;河北省食品质量监督检验研究院,石家庄,050091 |
| |
| 基金项目： | 基金项目：河北省质量技术监督局科技计划项目（No.070105）. |
| |
| 摘 要： | 建立了一种测定食品纸包装材料中多氯联苯的方法。采用超声萃取法提取样品，通过固相萃取柱净化、无水硫酸钠脱水、浓缩后，用气质联用法进行测定。该方法的检出限为10g／kg，回收率为75％～96％，相对标准偏差为2．9％～6．9％。并初步建立了三重串联四极杆气相色谱／质谱／质谱验证方法，该方法的检出限为1μg／kg。
|
| 关 键 词： | 超声萃取 气质联用法 三重串联四极杆气相色谱／质谱 食品纸包装材料 多氯联苯 |
Determination of polychlorinated biphenyle in food packaging paper materials |
| |
| Bai Yankun,Guo Limin,Li Qiang.Determination of polychlorinated biphenyle in food packaging paper materials[J].Analytical Instrumentation,2011(5):18-21. |
| |
| Authors: | Bai Yankun Guo Limin Li Qiang |
| |
| Affiliation: | 1. Hebei Food Safety Key Laboratory, Agriculture University of Hebei , Baoding, 071001; 2. Hebei Institute of Food Quality Supervision and Inspection, Shijiazhuang, 050051) |
| |
| Abstract: | A method for the determination of polychlorinated biphenyls （PCBs） in food packaging papers was establised. The PCSs were extracted by ultrasonic extraction, purified by solid-phase extraction column, and dehydrated by anhydrous sodium sulfate. After being concentrated, the sample was determined by gas chromatography-mass spectrometry. The detection limit was 10gg/kg, the recoveries were 75%-96%, and RSDs were 2.9-6.9%. An authentication method, GC-MS-MS, with the detection limit of 1μg/kg was also established. |
| |
| Keywords: | |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
