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Energy filtering transmission electron microscopy using the new JEM-2010FEF
Authors:TOMOKIYO  MATSUMURA  & MANABE
Affiliation:Department of Materials Science and Engineering,;Department of Applied Quantum Physics and Nuclear Engineering,;Research Laboratory for High Voltage Electron Microscopy, Kyushu University, Fukuoka 812-8581, Japan
Abstract:The new JEM-2010FEF electron microscope provides useful techniques based on energy filtering as an omega-type energy filter is integrated into a thermal field-emission 200 kV transmission electron microscope. For example, the zero-loss imaging improves the contrast of high resolution lattice images as well as images of precipitates or lattice defects in alloys. The acquisition time for elemental mapping with core-loss electrons is one order in magnitude shorter than with energy-dispersive X-ray spectroscopy. The removal of inelastically scattered electrons enables us to observe weak lines in convergent-beam electron diffraction patterns from a thicker specimen with a probe size 1–2 nm in diameter. A combination of the field emission gun and sensitive recording media such as an imaging plate and a slow-scan CCD camera makes the energy filtering more powerful.
Keywords:convergent-beam electron diffraction  electron spectroscopic diffraction  electron spectroscopic imaging  elemental mapping  energy filtering  field emission gun  higher order Laue zone  imaging filter  imaging plate  omega-filter  transmission electron microscopy  zero-loss image  
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