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苍耳子风湿药酒的研制与检测
引用本文:戚颖欣,曹柏营,寇莹,昌友权. 苍耳子风湿药酒的研制与检测[J]. 食品科学, 2007, 28(9): 481-484
作者姓名:戚颖欣  曹柏营  寇莹  昌友权
作者单位:吉林工程技术师范学院生物与食品工程学院; 吉林工程技术师范学院生物与食品工程学院 吉林长春130052; 吉林长春130052;
基金项目:吉林工程技术师范学院大学生创新基金
摘    要:实验确定了回流提取法为苍耳子药酒生产的最佳工艺,建立苍耳子风湿药酒的质量标准,利用高效液相色谱法检测苍耳子有效成分绿原酸。绿原酸进样量在0.315~1.575μg范围内呈良好的线性关系,回归方程为Y=1857900X+7575.80,r=0.999985(n=5),平均加样回收率为99.22%,RSD值为1.38%(n=6)。结果表明本方法简便、快速、灵敏、准确、重复性好,可以控制苍耳子风湿药酒的质量。

关 键 词:苍耳子   风湿药酒   高效液相色谱  
文章编号:1002-6630(2007)09-0481-04
修稿时间:2007-08-08

Development and Determination of Fengshi Medical Wine of Fructus xanthii
QI Ying-xin,CAO Bai-ying,KOU Ying,CHANG You-quan. Development and Determination of Fengshi Medical Wine of Fructus xanthii[J]. Food Science, 2007, 28(9): 481-484
Authors:QI Ying-xin  CAO Bai-ying  KOU Ying  CHANG You-quan
Affiliation:College of Biology and Food Engineering,Jilin Teacher’s Institute of Engineering and Techology,Changchun 130052,China
Abstract:Experimentntal results inchicated that the optimal production method of Fengshi medical wine of Fructus xanthii was circumfluence extraction.An RP-HPLC method was established for determination of chloralgenic acid in Fengshi medical wine of Fructus xanthii.The calibration curve was in good linearity over the range of 0.315~1.575μg with the regression equation Y=1857900X+7575.80,r=0.999985(n=5).The average recovery was 99.22% with RSD=1.38%(n=6).The method appeared to be simple,accurate,reproducible and could be used to control the quality of Fengshi medical wine of Fructus xanthii.
Keywords:Fructus xanthii   Fengshi medical wine   HPLC
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