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氮掺杂石墨烯/氧化亚铜复合凝胶的制备与性能
引用本文:李亮,陈海春,邱唯楚,申小松,喻航达,喻湘华. 氮掺杂石墨烯/氧化亚铜复合凝胶的制备与性能[J]. 武汉工程大学学报, 2018, 40(4): 410-414
作者姓名:李亮  陈海春  邱唯楚  申小松  喻航达  喻湘华
作者单位:武汉工程大学材料科学与工程学院,湖北 武汉 430205
摘    要:为了拓展石墨烯凝胶材料在污水处理领域的应用,以氧化石墨烯与氢氧化铜为前驱物,氨水为氮源,葡萄糖为还原剂,利用一步水热法制备了氮掺杂石墨烯/氧化亚铜(NG/Cu2O)复合凝胶材料。采用X射线衍射仪、扫描电子显微镜表征产物的微观形貌与结构,通过紫外-可见分光光度计测试NG/Cu2O复合材料在不同的光照环境下对罗丹明B(RhB)染料所表现出的吸附降解性能。实验结果表明,与NG凝胶相比,NG/Cu2O复合凝胶材料表现出更好的吸附与催化降解能力,且在紫外光的光照环境下对RhB染料的吸附降解性能最佳。

关 键 词:氮掺杂石墨烯  氧化亚铜  复合材料  凝胶

Synthesis of Nitrogen-Doped Graphene/Cuprous Oxide Composite Hydrogels and Their Performance
LI Liang,CHEN Haichun,QIU Weichu,SHEN Xiaosong,YU Hangda,YU Xianghua. Synthesis of Nitrogen-Doped Graphene/Cuprous Oxide Composite Hydrogels and Their Performance[J]. Journal of Wuhan Institute of Chemical Technology, 2018, 40(4): 410-414
Authors:LI Liang  CHEN Haichun  QIU Weichu  SHEN Xiaosong  YU Hangda  YU Xianghua
Affiliation:School of Materials Science and Engineering,Wuhan Institute of Technology,Wuhan 430205, China
Abstract:
To expand the application of graphene hydrogel in waste water treatment,an efficient one-step hydrothermal method was developed for the synthesis of nitrogen-doped graphene/cuprous oxide (NG/Cu2O) composite hydrogel using graphene oxide and Cu(OH)2 as the precursors,ammonia as the nitrogen source,glucose as the reducing agent. Scanning electron microscopy and X-ray diffraction were conducted to characterize the morphology and structure of the composites. The adsorption/degradation properties for Rhodamine B(RhB) of NG/Cu2O composite hydrogel were evaluated by ultraviolet-visible spectrophotometer. The experimental results showed that compared with NG hydrogel,the NG/Cu2O composite hydrogel possessed better adsorption/degradation ability for RhB,especially under UV light irradiation.
Keywords:nitrogen-doped graphene  cuprous oxide  composite  hydrogel
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