Manufacturing and mechanical characterization of Al<Subscript>2</Subscript>O<Subscript>3</Subscript>/β-TCP/TiO<Subscript>2</Subscript> biocomposite as a potential bone substitute

This paper focuses on the mechanical characterization of a bioceramic based on commercial alumina (Al₂O₃) mixed with synthesized tricalcium phosphate (β-TCP) and commercial titania powder (TiO₂). The effect of β-TCP and TiO₂ addition on the mechanical performance was investigated. After a sintering process at 1600 °C for 1 h, various mechanical properties of the samples have been studied, such as compressive strength, flexural strength, tensile strength, elastic modulus, and fracture toughness. The measurements of the elastic modulus (E) and the tensile strength (σ _t ) were conducted using the modified Brazilian test while the compressive strength (σ _c ) was determined through a compression test. Also, semi-circular bending (SCB) specimens were used to evaluate the flexural strength (σ _f ) and the opening mode fracture toughness (K _IC). From the main results, it was found that the best mechanical performance is obtained with the addition of 10 wt.% TCP and 5 wt.% TiO₂. Alumina/10 wt.% tricalcium phosphate/5 wt.% titania composites displayed the highest values of mechanical properties and a good combination of compressive strength (σ _c ?≈?352 MPa), flexural strength (σ _f ?≈?98 MPa), tensile strength (σ _t ?≈?86.65 MPa), and fracture toughness (K _IC?≈?13 MPa m^1/2).     

Big data analysis of a mini three-axis CNC machine tool based on the tuning operation of controller parameters

The characteristic responses of a mini three-axis computer numerical control (CNC) machine tool based on the controller tuning operation were investigated for big data estimation. The major tuning parameters included the position control gains K _p, the position feed-forward control gains K _f, the speed control gains K _v, and the gain ratios K _g of the position and speed control values in manufacturing industries. K _p gains of 10, 30, 50, 80, 100, 200, 300, and 400 rad/s, K _f gains of 0, 30, 50, 60, 80, and 100 %, K _v gains of 30, 50, 70, 100, 300, 900, 2000, and 3000 rad/s, and K _g ratios of (1:1), (3:1), (5:1), and (7:1) were analyzed for smart productivity. The results show that the settling times at different K _p values were almost constant when the K _p gain was over 200 rad/s. The maximum overshoots, when the feed-forward gain is over 60 %, almost increased with increasing feed-forward gains. However, the overshoot of the three-axis CNC machine tool decreased as the K _v gain increased until the K _v gain reached 70 rad/s. The settling times at a constant K _g ratio decreased with an increase in the K _p and K _v gains. The characteristic responses of the tuning operations were enabled with connectivity to a cloud network to share the big data, to support decision making, and to adjust operations in real time.     

Effect of Oxygen on the Self-formation of Carbonaceous Tribo-layer with Carbon Nitride Coatings under a Nitrogen Atmosphere

The ball-on-disk friction and wear tests of CN _X coatings (CN _X /CN _X ) were conducted under a nitrogen atmosphere with controlled relative humidity (RH) (3.4–40.0%RH) and oxygen concentration (100–21 × 10⁴ ppm) in this study. We found that the specific wear rate of CN _X coating on ball (W _b), which could give stable and low friction coefficient (<0.05), was below 3.0 × 10^?8 mm³/Nm. Average friction coefficients (µ _a) and W _b of CN _X /CN _X increased (µ _a: 0.02–0.33, W _b: 1.6 × 10^?8–2.4 × 10^?7 mm³/Nm) with increasing oxygen concentration (230–211,000 ppm) as well as RH (4.7–21.1%RH) under a nitrogen atmosphere. However, the W _b remained low value below 2.3 × 10^?8 mm³/Nm regardless of oxygen concentration (100–207,000 ppm) of a nitrogen atmosphere (3.4–3.9%RH) when CN _X -coated balls were slid against a hydrogenated CN _X (CN _X :H) coatings (CN _X /CN _X :H). Besides, the CN _X /CN _X :H achieved low and stable friction coefficient below 0.05 under a nitrogen atmosphere (10,000 ppmO₂) regardless of increasing RH up to 20%RH. Raman analysis indicated that the structure of carbon on the top surface of CN _X coating was changed from as-deposited CN _X coating in the case of low friction coefficient (<0.05). Furthermore, TOF-SIMS analysis provided the evidence that the carbon derived from CN _X -coated disk was considered to diffuse into the ball surface, and it mixed with the carbon derived from CN _X -coated ball on the wear scar, which formed the chemically bonded carbon tribo-layer. Low friction coefficient (<0.05) with CN _X coatings under a nitrogen atmosphere was achieved due to self-formation of the carbon tribo-layer.     

Determining electrophysical characteristics of metal-oxide-semiconductor structures from the data of voltage-capacitance analysis of the depletion region of a semiconductor surface

The oxide layer in nanotransistors with metal-oxide-semiconductor (MOS) structures may be as thin as 20Å. The physical diagnostics of such structures via conventional methods of voltage-capacitance characteristics (VFCs) is impossible without taking into account the usually disregarded effects of degeneracy and dimensional quantization of the electron gas. However, as the oxide-layer thickness decreases, these effects make an increasingly substantial contribution to capacitance C of the MOS structure not only at C?C _i (where C _i is the “oxide capacitance”) but also at C < C _i . In this study, we have developed a general method for determining the principal characteristics of MOS structures from the data of analysis of the VFCs in the region of the Schottky depletion layer. The doping level, the surface potential, the semiconductor surface charge, the voltage of “flat bands,” oxide capacitance C _i , the voltage drop across the oxide, and the sign and density of the charge fixed in it can be found at an accuracy of ?0.1% within the framework of a single experiment regardless of the oxide-layer thickness and without using fitting parameters and a priori assumptions concerning the properties of the electron gas in the accumulation and inversion layers. The stages and results of the implementation of this method are demonstrated by the results of experiments performed on an n-Si-based MOS structure with a 171.2 Å-thick oxide layer.     

Data recording system of a dispersion interferometer based on a CO<Subscript>2</Subscript> laser

The data recording system of a multichannel double-pass dispersion interferometer based on a CO₂ laser is described. This system has been designed to record the linear density of plasmas in a real-time mode with a time discreteness of 4 μs and resolution 〈N _e L〉 ～ 0.34 × 10¹³ cm^?2 (N _e is the electron component of the plasma density, and L is the plasma size in the wave propagation direction) in the range of linear density variations of up to 10¹⁷ cm^?2. The system is built from unified recording modules that use fast ADCs to record the shape of photodetector and modulator signals and FPGA-based digital units of dataflow processing to form results of measurements. The single-channel recording module of the dispersion interferometer has been tested under actual experimental conditions of the GDL gas-dynamic trap and the TEXTOR tokamak (Julich, Germany).     

Lubricity of High Water Content Aqueous Gels

Aqueous gels such as biopolymer gels, mucus, and high water content hydrogels are often qualitatively described as lubricious. In hydrogels, mesh size, ξ, has been found to be a controlling parameter in friction coefficient. In the tribology of aqueous gels, we suggest that the Weissenberg number (Wi) is a useful parameter to define different regimes, and following the original formulations in rheology, Wi is given by the polymer relaxation time (ηξ³/k_BT) multiplied by the shear rate due to fluid shear through a single mesh (V/ξ): Wi?=?ηVξ²/k_BT. At sliding speeds below a Weissenberg number of approximately 0.1, Wi?<?0.1, the friction coefficient is velocity-independent and scales with mesh size to the ??1 power, µ ∝ ξ^?1. De Gennes’ scaling concepts for elastic modulus, E, give a dependence on polymer mesh size to the ??3 power, E ∝ ξ^?3, and following Hertzian contact analysis, the contact area is found to depend on the mesh size squared, A ∝ ξ². Combining these concepts, the shear stress, τ, and therefore the lubricity of aqueous gels, is predicted to be highly dependent on the mesh size, τ ∝ ξ^?3. Studies aimed at elucidating the fundamental mechanism of lubricity in biopolymer gels, mucus, and hydrogels have wrestled with comparisons across mesh size, which can be extremely difficult to accurately quantify. Using scaling concepts relating polymer mesh size to water content reveals that shear stress decreases rapidly with increasing water content, and plots of shear stress as a function of swollen water content are suggested as a useful method to compare aqueous gels of unknown mesh size. As a lower bound, these data are compared against estimates of fluid shear stress for free and bound water flowing through a mesh size estimated by the water content of the gels. The results indicate that the strong dependence on lubricity is likely due to a synergistic combination of a low viscosity solvent (water) coupled to a system that has a decreasing friction coefficient, modulus, and the resulting contact pressure with increasing water content. Although the permeability, K, of aqueous gels increases dramatically with water content (and mesh size), K ? ξ²/η, the stronger decrease of the elastic modulus and subsequent decrease in contact pressure due to an increase in the contact length, predicts that the draining time under contact, t, actually increases strongly with increasing water content and mesh size, t ∝ ξ². Consistent with the finding of extremely high water content aqueous gels on the surfaces of biological tissues, these high water content gels are predicted to be optimal for lubrication as they are both highly lubricious and robust at resisting draining and sustaining hydration.     

Nonparametric estimation of a probability density function and its derivatives. <Emphasis Type="Italic">C</Emphasis>-approach

Nonparametric (kernel) estimation of a probability density function f(x) for a sample of finite size is considered using the C-approach. The smoothness parameter β of the estimated probability density is introduced. For the case β > 2, it is shown that the convergence of the density estimate f _n (x) to the function f(x) can be improved by using alternating-sign weight functions (higher-order weight functions). Estimation of the derivatives of a function is briefly considered using the same approach.     

A Dispersion Interferometer Based on a CO<Subscript>2</Subscript> Laser

A double-pass dispersion interferometer based on a 9.6-μm CO₂ laser with a sensitivity of 〈 n _e l〉_min ∼ 1 × 10¹³ cm⁻² and a temporal resolution of ∼50 μ s, designed to measure linear plasma density, is described. A ZnGeP₂ nonlinear crystal is used as the frequency doubler. The main advantages of the interferometer are its compactness and a low sensitivity to vibrations of optical elements. The interferometer requires no special vibration isolation. Its main components are arranged compactly on an optical bench outside the apparatus, except for a window for radiation injection and a retroreflector; these are mounted on the wall of the experimental facility's vacuum chamber. The advantages of the dispersion interferometer have been demonstrated in an experiment with a gas-dynamic trap. __________ Translated from Pribory i Tekhnika Eksperimenta, No. 5, 2005, pp. 96–106. Original Russian Text Copyright ? 2005 by Solomakhin, Bagryanskii, Voskoboinikov, Zubarev, Kvashnin, Lizunov, Maksimov, Khil'chenko.     

High-power sources of ultra-wideband radiation with subnanosecond pulse lengths

Sources of high-power ultra-wideband electromagnetic pulses of nanosecond duration are described. A bipolar voltage pulse with a length of 0.5 ns and an amplitude of ～200 kV is fed to the input of a radiating system (a 16-element array antenna or a single antenna). The values of the effective radiation potential E _p R = 260 kV for a source with a single antenna and E _p R = 690 kV for a source with a 16-element antenna array were obtained at a pulse repetition frequency of 100 Hz.     

Improvement of AA5052 sheet properties by electromagnetic twin-roll casting

Although servo scanning 3D micro electro discharge machining (SS-3D MEDM) can achieve a high discharge ratio, the processing efficiency is still lower than expected because the discharge area at micro-electrode tip is much smaller than the area to machine. In particular, for 3D micro cavities, the processing efficiency and the machining accuracy inherently contradict each other. In this paper, an on-machine process of rough-and-finishing SS-3D MEDM is proposed with consideration that most cavity material cannot affect the dimensional accuracy. In the rough machining process, technological measures such as high discharge energy and large-diameter tool electrodes are applied to maximize processing efficiency. In the finishing machining process, a small amount of material is removed for dimensional accuracy, smooth surface, and clear edges-and-corners by changing multi-factors of machining parameters. The research is concentrated on two key techniques: rough-and-finishing border strategy and micro tool-electrode precision measurement for the process transformation from rough to finishing. Moreover, an online measurement method is proposed by the point electric contact between a micro electrode and a standard thin-rod, and the measurement accuracy was up to ±1 µm in our experimental system. Machining experiments of 3D micro cavities < 800 µm verified the proposed methods and the processes including 3D model design, rough-machining, micro-electrode measurement and fabrication, and finishing machining. The experimental results were successfully achieved as follows: the dimensional accuracy < 5 µm, surface roughness Sa0.38 µm, and the processing efficiency being improved to 2.4 times.     

Fast-response thermistors made of synthetic single-crystal diamonds

Miniature thermistors are produced from boron-doped synthetic single-crystal diamonds grown under pressure using the thermal gradient method. It is shown that heavily doped diamonds with a boron concentration of 10¹⁹ cm^?3 or higher are most suitable for this purpose. In the temperature range of 300–700 K, coefficient β = ln(R ₁/R ₂)/(1/T ₁ ? 1/T ₂) is 2500 K. The characteristic response time of temperature-sensitive elements based on crystals with dimensions of 1 × 1 × 0.3 mm is ～100 µs; i.e., they can be used in monitoring systems with a response speed of up to 10 kHz.     

A Josephson Voltage Calibrator

An automatic voltage calibrator for voltages ranging from ?1 V to +1 V is described. The device is based on a Josephson array with Nb-AlO _x -Al-AlO _x -Nb junctions. Being illuminated by microwave radiation with a frequency of 65.2 GHz, the array, in which the operating supply currents of three junction sections are set by a multichannel digital source controlled by a personal computer, generates 21 voltage values quantized with steps of 51.5, 86.6, and 138 mV. The capabilities of this device are demonstrated by studying the deviation from linearity of a seven-digit digital nanovoltmeter with a measurement uncertainty of below 1 × 10^?7. By calibrating a precision Zener-diode voltage standard, it is shown that the uncertainty of this calibrator is no more than 20–50 nV at a voltage level of 1 V.     

Optimization of flux-cored arc welding process parameters by using genetic algorithm

The effect of flux-cored arc welding (FCAW) process parameters on the quality of the super duplex stainless steel (SDSS) claddings can be studied using Taguchi L9 design of experiments. In this experimental investigation, deposits were made with 30 % bead overlap. Establishing the optimum combination of process parameters is required to ensure better bead geometry and desired properties. The above objectives can be achieved by identifying the significant input process parameters as input to the mathematical models like welding voltage (X ₁), wire feed rate (X ₂), welding speed (X ₃), and nozzle-to-plate distance (X ₄). The identified responses governing the bead geometry are bead width (W) and height of the reinforcement (H). The mathematical models were constructed using the data collected from the experiments based on Taguchi L9 orthogonal array. Then, the responses were optimized using non-traditional nature-inspired technique like genetic algorithm (GA).     

Taguchi-based grey relational analysis for modeling and optimizing machining parameters through dry turning of Incoloy 800H

The present research focused on the optimization of machining parameters and their effects by dry-turning an incoloy 800H on the basis of Taguchi-based grey relational analysis. Surface roughness (Ra, Rq and Rz), cutting force (Fz), and cutting power (P) were minimized, whereas Material removal rate (MRR) was maximized. An L ₂₇ orthogonal array was used in the experiments, which were conducted in a computerized and numerical-controlled turning machine. Cutting speed, feed rate, and cut depth were set as controllable machining variables, and analysis of variance was performed to determine the contribution of each variable. We then developed regression models, which ultimately conformed to investigational and predicted values. The combinational parameters for the multiperformance optimization were V = 35 m/min, f = 0.06 mm/rev and a = 1 mm, which altogether correspond to approximately 48.98 % of the improvement. The chip morphology of the incoloy 800H was also studied and reported.     

Adatom concentration distribution on an extrawide Si(111) terrace during sublimation

The formation of an adsorption layer on the Si(111) surface during sublimation at temperatures of 1000–1100 °C and subsequent quenching at T = 750 °C is studied by methods of in situ ultrahigh-vacuum reflection electron microscopy and ex situ atomic force microscopy. The adatom concentration distribution on an extrawide (~60 μm) atomically flat terrace is determined for the first time, and the diffusion length x_s = 31±2 μm at T = 1000 °C is obtained. The analysis of the temperature dependence of the equilibrium concentration of adatoms near a monatomic step allows pioneering measurements of the energy necessary for adatom detachment from the step and attachment to the terrace E _ad ≈ 0.68 eV. Based on these results, the energy parameters for some atomic processes on the Si(111) surface are estimated.     

Vibration response analysis caused by rubbing between rotating blade and casing

Two types of blade-tip rubbing due to the static misalignment of the bladed-disk center and casing center and casing deformation are simulated. By applying aerodynamic load in the blade lateral/flexural direction, vibration responses due to blade-casing rubbing are analyzed under the run-up process with constant angular acceleration and the steady-state process at 10000 rev/min. The effects of some parameters, such as the static misalignment e _c, casing stiffness k _c and casing deformation n _p, on the system vibration responses are also illustrated by spectrum cascades, time-domain waveforms of displacement, normal rubbing forces, amplitude spectra and the impulse P in a single blade-casing rubbing period. The results show that blade-tip rubbing will cause amplitude amplification and harmonic resonance phenomena when the multiple frequencies (nf _r) of rotational frequency (f _r) coincide with the first three flexural dynamic frequencies of the blade (f _n1, f _n2 and f _n3). For example, the displacement amplitudes at 3f _r, 14f _r and 38f _r are large and the vibration is dominant near f _n1. In addition, the casing deformation mainly excites the dominant Blade passing frequency (BPF), which is related to the casing deformation coefficient n _p. By comparing these impulse values, for the selected parameters in this paper, the casing stiffness has a greater effect on impulse than the static misalignment and casing deformation coefficient. The impulse shows a linear increase trend with the increasing static misalignment, and it decreases under the large n _p because the contact time decreases with the increase of n _p.     

The use of new resonance integrals for determining the parameters of the epithermal neutron spectrum

A simple method for determining parameters α and b in the presentation of the epithermal neutron spectrum in the form of φ_epi(E) = b/E ^{1 + α} using expansion of function φ_epi(E) in Taylor series with respect to parameter α is described. The problem of determining the parameters is reduced to finding a solution to a system of algebraic equations. The approximation used describes the spectrum with an adequate accuracy up to energies of ～1–50 keV, depending on value α ～ 0.2?0.1, with the help of the first two or three expansion terms (resonance integrals), respectively. The first two resonance integrals for reactions ¹⁹⁷Au(n, γ)¹⁹⁸Au and ⁵⁵Mn(n, γ)⁵⁶Mn are estimated. The measured rates of the appropriate reactions and the values of parameters α and b for the case of an assembly with a graphite moderator are presented.     

Numerical and experimental investigation on the diffuser optimization of a reactor coolant pump with orthogonal test approach

The diffuser of a reactor coolant pump was optimized using an orthogonal approach with numerical simulation to improve the pump hydraulic performance. Steady simulation was conducted by solving Reynolds-averaged Naiver-Stokes equations with the SST k-ω turbulence model using CFX code. The influence of the diffuser geometric parameters, namely, S, φ, α ₄, b ₄, δ ₂, R _t and R ₄, on the pump performance were determined. L₁₈ (3⁷) orthogonal table was chosen for the optimization process. Best indicators were determined, and range analysis of energy losses, head, and efficiency at the rated condition was performed. Optimal parameters of the diffuser were S = 490 mm, φ = 36°, α ₄ = 30°, b ₄ = 200 mm, δ ₂ = 20 mm, R _t = 5 mm and R ₄ = 565 mm. The final design was experimentally tested. Simulation results showed more remarkable performance than the experimental result. However, the numerical predictions and experimental results were consistent, validating the design procedure. Loading of the impeller and diffuser blades was analyzed to investigate the direct impact on the hydrodynamic flow field. The head was 14.74 m, efficiency was 79.6 %, and efficiency of the prototype pump was 83.3 % when the model pump functioned at the rated conditions. Optimization results showed that efficiency and head were improved at the design condition.     

Numerical and experimental investigation into the dynamic response of a floating wind turbine spar array platform

The station keeping ability of a platform is the most fundamental guarantee to securing the dynamic stability of a Floating offshore wind turbine (FOWT) when being subjected to complex marine environment. These are usually evaluated in terms of rigid body dynamic response of a floating platform which supports whole FOWT. To investigate the dynamic response of array of FOWT, we put forward the concept of a large FOWT farm which consists of nine spar-type wind turbine array and meanwhile shares mooring line system by connecting those FOWT to one another. The whole FOWT is established based on OC3-Hywind spar buoy platform with NREL 5MW wind turbine. Considering effects of wind, wave and current loads, the dynamic response of the proposed FOWT was conducted based on FEM software ANSYS AQWA under both operational condition and survival condition. Besides, comparisons of dynamic response between the original single FOWT and the proposed FOWT farm were also made. Several interesting conclusions were gained through the investigation. For the original single FOWT, RAO in surge, heave and pitch are concentrated in low frequency, while the peak value of frequency is about 0.2 rad/s. In addition, FOWT (P1, P3, P7 and P9) located on the four vertices of 3×3 have higher sway motion which range from about -0.15 m~ 0.15 m, while sway motion of the rest can be neglected. With the worsening of environmental condition, surge motion of the original single FOWT increases significantly, while it’s not significant for the proposed FOWT farm. At the same time, statistic values of pitch motion of the proposed FOWT farm are quite close to those of the original single FOWT. While, under the survival condition, range of pitch motion of the proposed FOWT farm is significantly smaller than that of the original single FOWT. In all, the results verify the effectiveness of the proposed FOWT farm.     

Calculation of negative-pressure chip in suction-type internal chip removal system and analysis of influencing factors

Compacted graphite iron (CGI) is considered as the ideal material to make modern fuel-efficient diesel engine. Due to the vermicular or worm-like graphite distributed among the ferrite/pearlite matrix, CGI behaves better physical and mechanical properties in comparison with gray cast iron (GCI) and spherical graphite spheroidal cast iron (SGI). However, these good properties bring about the machining challenges. So it is important to appropriately select cutting parameters to machine this material with economy and efficiency. The present study investigated the influence of cutting parameters, such as cutting speed V, feed rate f, and exit angle Ψ, on workpiece material removal volume Q and cutting burr height on the entrance side H₁ and on the exit side H₂ during high-speed milling of CGI by the coated carbide tools_. On this basis, the relatively optimum high-speed cutting parameters were selected under the research condition. Cutting tool failure mechanism was also investigated with the aid of scanning electronic microscope (SEM) and energy-dispersive system (EDS) (SUPRA55, Germany) analysis. The results showed that Q, H₁, H₂, and the type of cutting burr on the exit side of the machined surface could be influenced by the cutting parameters. And the relatively optimum cutting parameters are V = 800 m/min, f = 0.25 mm/rev, and Ψ = 60°. Adhesive wear and thermal cracks which were perpendicular to the cutting edge were common wear mechanisms during the cutting process. However, with an increase in feed rate, mechanical cracks which were parallel to the cutting edge could be found on the flank face of the cutting tool.