Residual toughness of poly(acrylonitrile-butadiene-styrene) (ABS) after fatigue loading—effect of uniaxial fatigue loading

Toughness variation of non-notched poly(acrylonitrile-butadiene-styrene) (ABS) subjected to uniaxial fatigue loading was investigated. The experiments were conducted by applying fatigue loading to strip specimens first, from which dog-bone specimens were machined. The dog-bone specimens were tested to measure the strain for the on-set of fracture, named cracking strain here, thus to monitor the toughness change due to the fatigue loading.The test results showed that the fatigue loading caused the toughness drop in ABS, even before any visible crack was developed. Damage development and fracture behavior were then analyzed using scanning electron microscopy (SEM). The SEM analysis revealed that damage zones, not cracks, were initiated during the fatigue loading, and were the main cause of the toughness drop. Mechanisms for the damage initiation include matrix crazing and debonding of small rubber particles; however, large rubber particles remained intact. Based on the results, a deformation model is proposed for the damage zone initiation, which provides an explanation for the toughness change under the fatigue loading.     

Some Peculiarities of Fatigue Crack Growth at Various Stages of Its Development

The author considers some peculiarities of fatigue crack growth in metals at the stages of its initiation and initial development, and stable and unstable growth that precedes final fracture. It is shown that at the stage of initial growth of fatigue cracks, the stress state, nonlocalized fatigue damage that precedes initiation of the main fatigue crack, residual surface stresses, surface manufacturing and in-service defects, and contact interactions are the factors that determine the crack paths. Stable growth of a fatigue crack is primarily determined by the stress-strain state of a structure as a whole and by the stress-strain state at the crack tip with allowance for its variation due to crack propagation, which is evaluated by the criteria of fracture mechanics. The author also studied peculiarities of fatigue crack development in compressor blades of marine gas turbines. It is shown that for embrittled steels, when fatigue cracks develop under plane strain conditions, final fracture occurs at very small crack sizes. In this case, the characteristics of fatigue fracture toughness are appreciably lower than the static values. The paper also considers peculiarities of unstable fatigue crack propagation.     

Fatigue and fracture of a Ni–P amorphous alloy thin film on the micrometer scale

Fracture and fatigue tests have been performed on micro‐sized specimens for microelectromechanical systems (MEMS) or micro system technology (MST) applications. Cantilever beam type specimens with dimensions of 10 × 12 × 50 μm³, approximately 1/1000th the size of ordinary‐sized specimens, were prepared from a Ni–P amorphous thin film by focused ion beam machining. Fatigue crack growth and fracture toughness tests were carried out in air at room temperature, using a mechanical testing machine developed for micro‐sized specimens. In fracture toughness tests, fatigue pre‐cracks were introduced ahead of the notches. Fatigue crack growth resistance curves were obtained from the measurement of striation spacing on the fatigue surface, with closure effects on the fatigue crack growth also being observed for micro‐sized specimens. Once fatigue crack growth occurs, the specimens fail within one thousand cycles. This indicates that the fatigue life of micro‐sized specimens is mainly dominated by a crack initiation process, also suggesting that even a micro‐sized surface flaw may be an initiation site for fatigue cracks which will shorten the fatigue life of micro‐sized specimens. As a result of fracture toughness tests, the values of plane strain fracture toughness, K_IC, were not obtained because the criteria of plane strain were not satisfied by this specimen size. As the plane strain requirements are determined by the stress intensity, K, and by the yield stress of the material, it is difficult for micro‐sized specimens to satisfy these requirements. Plane‐stress‐ and plane‐strain‐dominated regions were clearly observed on the fracture surfaces and their sizes were consistent with those estimated by fracture mechanics calculations. This indicates that fracture mechanics is still valid for such micro‐sized specimens. The results obtained in this investigation should be considered when designing actual MEMS/MST devices.     

Small fatigue crack initiation and growth behavior of high-strength low alloy steel in various environments

Fatigue tests under rotating bending and reversed torsion were carried out in air, distilled water and 3% saltwater, using smooth specimens of high-strength low alloy steel (Cr-Mo steel). The initiation and growth behavior of small fatigue cracks in each environment were evaluated based on detailed observations, and the effects of corrosive environment were also discussed. The fatigue strength decreased with increasing aggressiveness of test environment. The decreases in corrosive environment were due to earlier fatigue crack initiation. From the observed locations at which small fatigue cracks began, it was considered that the crack initiation was primarily governed by hydrogen embrittlement in distilled water and also affected by corrosive dissolution in 3% saltwater. The validity of the application of linear fracture mechanics for small fatigue cracks was established. The growth rates of small fatigue cracks were higher than for large through cracks, and not accelerated by the corrosive environment. Moreover, fatigue life in the corrosive environment was estimated by using the crack growth characteristics in air.     

Characterization and measurement of the mode 1 dynamic initiation of cracks in metals at intermediate strain rates—A review

Dynamic initiation of cracks in metals occurs as a result of impact loading. In general, for the case of small scale yielding, the fracture toughness of the material reduces with elevated strain rate, whereas for large scale yielding fracture toughness increases with strain rate. The review concentrates on the modelling of the crack tip stress field at intermediate strain rates ( <100 s⁻¹) and on the micromechanical causes of the rate dependency of dynamic initiation fracture toughness. The validation of developed fracture criteria requires careful experimental testing, and problems associated with instrumented impact testing are discussed. Some results are given for 150M12 and 817M40/En24 structural steels.     

THE GROWTH OF SMALL FATIGUE CRACKS IN A LOW CARBON STEEL; THE EFFECT OF MICROSTRUCTURE AND LIMITATIONS OF LINEAR ELASTIC FRACTURE MECHANICS

The growth characteristics of small fatigue cracks were studied under rotary bending in a low carbon steel prepared with two ferrite grain sizes of 24 and 84 μm, and were compared with the growth characteristics of large through cracks in fracture mechanics type specimens. The effect of microstructure on crack growth rates and the interaction in growth behaviour between two neighboring small cracks were examined experimentally, and also the critical crack lengths above which linear elastic fracture mechanics (LEFM) is applicable were evaluated for small crack growth and for fatigue crack thresholds. It is found that small cracks grow much faster than large ones and also show growth rate perturbations due to grain boundaries. It is indicated that the critical crack lengths for fatigue crack thresholds are significantly shorter than those for small crack growth.     

Determination of fracture toughness from thin side-grooved specimens

Methods of determining fracture toughness from specimens of thickness lower than that required by ASTM Standard, E399 were studied using aluminum and titanium alloy specimens. In thin specimens in which crack growth initiation is clearly marked by a sudden change in the slope of the load-displacement curve, the stress intensity at the crack growth initiation point was found to be the same as the standard fracture toughness value. Crack growth initiation was more easily identifiable in the aluminum alloys than in the titanium alloy, although the latter was more brittle. Side grooves enable identification of crack growth initiation in thinner specimens, reducing considerably the thickness requirement for fracture toughness testing. A nearly straight crack front was found to be essential for obtaining reproducible results. Sharp and deep side grooves produced fatigue cracks leading at the edges.     

An investigation of the effects of mix strength on the fracture and fatigue behavior of concrete mortar

This paper examines the effects of mix compressive strength (30, 35 and 40 MPa) on the fracture initiation toughness, resistance-curve behavior and fatigue crack growth behavior of concrete mortar. The fracture initiation toughness and the resistance-curve behavior are shown to increase with increasing mix strength. The observed resistance-curve behavior is then attributed largely to the effects of ligament bridging, which are predicted using small- and large-scale bridging models. In contrast, the fatigue crack growth resistance is shown to decrease with increasing mix strength. An extended multiparameter framework was used for the modeling of fatigue crack growth. Finally, the implications of the results are discussed for the design of concrete mixtures with attractive combinations of strength, fracture toughness and fatigue crack growth resistance.     

Interaction between tensile strength failure and mixed mode crack propagation in concrete

Crack size and structure size transitions are illustrated which connect the two limit-cases of ultimate tensile strength failure (small cracks and small structures) and mixed-mode crack propagation (large cracks and large structures). The problem of mixed-mode crack propagation in concrete is then faced. By increasing the size-scale of the element the influences of heterogeneity and cohesive crack tip forces disappear and crack branching is governed only by the linear elastic stress-singularity in the crack tip region. It is proved in this way that the fracture toughness of the material is measured by a unique parameter (G_IF, G_IC or K_IC) even for the mixed-mode condition. The ratio of the sliding or Mode II fracture toughness (G_IIF, G_IIC or K_IIC) to the opening or Mode I fracture toughness depends only on the crack branching criterion adopted and not on the material features. Eventually, very controversial experimental results recently obtained on the shear fracture of concrete are explained on the basis of the above-mentioned size-scale transition.     

THE SIZE OF PLASTIC ZONES AND FATIGUE CRACK GROWTH BEHAVIOUR OF THREE FORMS OF A Ti–6Al–2.5Mo–1.5Cr ALLOY

The effect of microstructure on the fatigue properties of Ti–6Al–2.5Mo–1.5Cr alloy was investigated. The experimental results for both the fatigue crack initiation and propagation behaviour, as well as the dynamic fracture toughness ( K _Id ) showed clearly that a lamellar microstructure is superior to two other structures. It was found that, as in the case of steels, the initiation and subsequent growth of cracks in the titanium specimens with a sharp notch may also occur on loading levels below the threshold values of the K factor (Δ K _th ) determined for long fatigue cracks. In addition, measurements by interferential-contrast of the plastic zone size on the surface of specimens revealed that the different rate of crack growth at identical values of Δ K in individual structural states can roughly be correlated with the size of the plastic zone. A general relationship between the fatigue crack growth rate and plastic zone size, the modulus of elasticity and the role of crack tip shielding is discussed.     

Growth behaviour of small surface fatigue cracks in AISI 304 stainless steel

A series of axial tensile fatigue tests (R = 0.1) was carried out to investigate the initiation and the growth behaviours of very small surface fatigue cracks under two different surface conditions (viz. smooth and pitted surfaces) of AISI 304 stainless steel at room temperature. This paper deals with both of the two approaches regarding the analysis of fatigue: the approach based on the concept of fracture mechanics and low cycle fatigue. In particular, both the initiation and growth of cracks and the coalescence of small cracks by fatigue in the specimen have been investigated by the methods of surface replicas and photomicrographs. Quantitative information such as the initiation period, growth and coalescence behaviours of small cracks, and crack growth properties were systematically obtained. The results show that the accurate determination of these parameters is critical for the application of fracture mechanics to fatigue life assessment.     

The effect of initial notch shape of compact specimen on fatigue pre-cracking and fracture toughness testing

The circular notched compact specimens, along with standard specimens having straight or chevron notch are provided for fatigue and fracture toughness testings in order to study the crack observation capability during fatigue pre-cracking, skewness of the crack front, and the resulting fracture toughness K_Q. The test results indicated that circular notched specimens significantly facilitate the crack observation during fatigue testing as the cracks initiate on both surfaces of the specimen. No remarkable differences were observed on geometries of the fatigue crack front obtained and the resulting fracture toughness among these three types of specimen. The macroscopic observation of beach marks on the fracture surfaces revealed that, in the present material Ti-6Al-4V (ELI), the advance of only 1.3% of the whole crack length corresponded to the load level at which fracture toughness K_Q was evaluated.     

Weld tool travel speed effects on fatigue life of friction stir welds in 5083 aluminium

This paper reports the results of a study into the influence of weld tool travel speed (in the range 80–200 mm/min) on the occurrence of ‘onion-skin’ forging-type defects (similar to the root defects known as ‘kissing bonds’) in single pass friction stir (SP FS) welds, and on the effect of these defects on fatigue crack initiation and overall life. Results indicate that such defects are generally not associated with fatigue crack initiation, but may act to reduce fatigue life by providing easy linking paths between two fatigue cracks. It is likely that their influence on fracture toughness of SP FS welds would be higher, as they occur more readily when growth rates and levels of plastic deformation are higher.     

2219铝合金TIG和FSW接头力学及疲劳性能

目的 研究钨极氩弧焊(TIG)和搅拌摩擦焊(FSW)对2219铝合金(母材)力学及疲劳性能的影响。方法 通过拉伸试验,得到了母材、TIG和FSW接头的抗拉强度和伸长率;通过疲劳性能试验测试了母材、TIG和FSW接头在不同应力下相应的疲劳寿命,根据疲劳试验结果绘制了其试样的S-N曲线;使用扫描电子显微镜观察并分析了疲劳断口的形貌特征。结果 未焊接的铝合金母材抗拉强度和伸长率最高,分别为506 MPa和15.92%;TIG接头抗拉强度和伸长率分别为330 MPa和7.65%,FSW接头抗拉强度和伸长率分别为310 MPa和8.74%。母材、TIG和FSW接头等3种疲劳试样在2×10⁶次循环下的疲劳强度分别为129、108、115 MPa,其疲劳断口均可分为裂纹源区、裂纹扩展区和瞬间断裂区,疲劳裂纹分别起始于试样表面的局部变形区、第二相夹杂物和“吻接”缺陷。疲劳裂纹扩展区的主要形貌为疲劳辉纹和二次裂纹,瞬间断裂区以脆性断裂为主。结论 TIG和FSW等2种焊接工艺均导致了2219铝合金的强度、塑韧性和疲劳性能降低,其接头表面的第二相夹杂物和“吻接”缺陷促进了疲劳裂纹的萌生。     

FATIGUE BEHAVIOUR OF STEEL CASTINGS CONTAINING NEAR-SURFACE DEFECTS

Manufacturing defects in the near-surface region of 2¼% Cr 1% Mo castings were investigated in a joint research programme. After ultrasonic testing and X-ray inspection, large push-pull specimens (cross section 1000 mm²) were taken from castings in regions with indications of defects and tested under fully reversed loading in the elastic and elastic plastic region up to predetermined levels of defect growth. The defects are micropores, pin holes, slag and oxide layers or inclusions, hot tears and small micro cracks in welds. The initiation of crack growth was analysed by two methods, namely (a) the local strain concept with idealization of defects as three-dimensional elliptical notches and (b) by the fracture mechanics concept with idealization of defects as two-dimensional elliptical cracks. The main results can be summarized as follows: 1. The local strain concept describes the crack initiation potential of the defects more accurately than the fracture mechanics concept. 2. Interpretation of casting defects as cracks produces very conservative estimates in many cases. 3. Analytical evaluation of crack growth behaviour using the fracture mechanics approach for defects experiencing crack growth of at least 1 mm is much more accurate than when defects having a smaller extent of crack growth are included in the analysis. Additional evaluations of crack growth behaviour of hot tears by fracture mechanics show that crack growth starting from open and partially closed hot tears must be subjected to a larger number of cycles than normal fatigue cracks of sound material. Partially closed hot tears in the vicinity of the crack front additionally delay crack propagation.     

钛合金双片层组织对性能的影响

研究了通过热处理制度调整,在合金α片层之间形成细小的条状次生α相,形成一种新型的钛合金显微组织——双片层组织.通过对比等轴组织、双态组织、片层组织和双片层组织的性能,结果表明,在合金的强度和塑性不损失的条件下,双片层组织进一步提高了裂纹在合金中的扩展阻抗,使得合金的断裂韧性得到改善,疲劳裂纹扩展速率得到降低.双片层组织...     

Mechanical properties of Al–Li alloys Part 2 Fatigue crack propagation

Abstract

Mechanisms influencing the ambient temperature mechanical properties of commercial Al–Li alloys 2090, 2091, 8090, and 8091 are examined, with specific emphasis on the role of microstructure. In Part 2, results on fatigue crack propagation behaviour are presented for both ‘long’ (≥ 5 mm) and ‘microstructurally small’ (~1–1000 μm) cracks and compared with behaviour in traditional high strength aluminium alloys. In general, it is found that the growth rates of long fatigue cracks in Al–Li alloys are up to two to three orders of magnitude lower than in traditional 7000 and 2000 series alloys, when compared at an equivalent stress intensity range ?K. By contrast, corresponding growth rates of microstructurally small fatigue cracks were up to two to three orders of magnitude higher than the long crack results. Such observations are attributed to the prominent role of crack tip shielding in Al–Li alloys resulting from the tortuous and deflected nature of the crack paths which results in a reduced crack tip ‘driving force’ from crack deflection and, more importantly, from the consequent crack closure induced by the wedging of fracture surface asperities. Since microstructurally small cracks are unable to develop the same level of shielding from crack closure by virtue of their limited wake, small crack growth rates are significantly accelerated. Unlike fracture toughness behaviour, artificial aging of commercial Al–Li alloys to peak strength has a mixed influence on the (long crack) resistance. Although behaviour at higher growth rates is relatively unaffected, in 2091 nominal threshold ?K_TH values are increased by 17%, whereas in 8090 and 8091 they are decreased by 16–17%. However, all alloys show reduced effective fatigue thresholds at peak strength after correcting for crack closure.

MST/926b     

表面裂纹弹塑性起裂的V准则

本文提出了一个新的断裂准则——裂纹咀张开位移率准则及新的材料断裂韧性参量V(?),并用实验验证了该准则的有效性。该准则特别适用于表面裂纹弹塑性起裂载荷的确定。V(?)可以用单试件法测定,并给出了 V_(1c)与 K_(1(?)),σ_c,J(?)的相互换算关系式。     

The effect of material defects on the fatigue behaviour and the fracture strain of ABS

The structural integrity and durability of a construction are highly dependent on the material quality. Poly(Acrylonitrile-Butadiene-Styrene) Copolymer (ABS) is a material which is preferably chosen for high performance products, because of its superior toughness. The toughness of ABS is revealed by its high fracture strain in a tensile test, and high notched Izod impact fracture energy. However, the fatigue resistance of ABS is less favourable. This investigation is mainly devoted to the fatigue behaviour of ABS and to the fracture strain and the notched Izod fracture energy. Various mechanical tests, performed in conjunction with scanning electron microscope investigations of the fracture surfaces, demonstrate that fracture initiates from small defects which are abundantly present in the material. Especially the fatigue fracture surfaces show numerous cracks which had initiated from the defects. The fracture strain in tensile tests is high, but shows a large scatter. It is demonstrated that the fracture strain is also related to the presence of defects. A pre-fatigue load up to 40% of the anticipated fatigue life, followed by a tension test shows a significant reduction of the fracture strain as compared with a tension test on non damaged as-moulded material. Microscopic investigations show that this fracture strain reduction is caused by the presence of small cracks which initiated from the defects, during the preceding fatigue load. A similar but much smaller effect of pre-fatigue was observed for notched Izod tests. Finally it is concluded that the fatigue behaviour of ABS is dominated by the growth live of microscopic small cracks from material defects.     

Effects of microstructural through‐thickness non‐uniformity and crack size on fatigue crack propagation and fracture of rolled Al‐7075 alloy

Some of the fatigue tests performed using the standard compact tension (CT) and a non‐standard specimen made of rolled 7075 aluminium alloy exhibit fatigue crack growth (FCG) lagging in a small region along the crack front. Through‐thickness microstructural evaluation shows that material grains in this region did not flatten as much as other regions. In the non‐standard specimen, surface cracks are either grown under fatigue loading or broken under monotonically increasing quasi‐static loads at different crack sizes. The aforementioned lagging also exists in a narrow region of 3‐D FCG for specimens with microstructural through‐thickness non‐uniformity. A more important feature for this type of specimen with surface crack is the deflection of fast fracture direction into the grain interfaces, namely from L‐T orientation to S‐L and S‐T directions. It is proved that this is due to significant levels of second principal stresses near the free surface for small cracks and lower fracture toughness of the material in S‐L and S‐T directions.