共查询到18条相似文献,搜索用时 15 毫秒
1.
Wei Wang Zhiwu Wang Wensheng Li Jing Tian Wanli Zhong Jiedong Lin 《Materials at High Temperatures》2013,30(3):276-282
The evolution of the morphology, composition, and particle size of the M23C6 phase in HR3C steel aged at 650 °C was analysed, by means of metallographic microscopy, scanning electron microscopy, and transmission electron microscopy. The results showed that the Cr/Fe ratio in the M23C6 phase, in the form of irregular square and long strip, increased with the ageing time. Fe was gradually replaced by Cr in the M23C6 lattice. The M23C6 phase gradually evolved and then became stable after ageing for 2000 h. 相似文献
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Cyclic behavior of 9–12% Cr steel under both stress and strain control modes was investigated at 873 K. Significant asymmetric deformation and cyclic softening were observed for both modes. Under the strain-controlled fatigue, a strain level-independent softening factor (SF) was observed. The SF was dependent on applied stress under the stress-controlled fatigue. For the strain-controlled fatigue, the magnitude of cyclic asymmetry decreases with the increase of strain amplitude, while under the stress-controlled fatigue, the asymmetry increases with the increase of stress amplitude. The anomalous ratcheting strain resulted from the asymmetry under the stress-controlled mode has a detrimental effect on fatigue life. 相似文献
3.
A PLA/calcium phosphate degradable composite material for bone tissue engineering: an in vitro study
Charles-Harris M Koch MA Navarro M Lacroix D Engel E Planell JA 《Journal of materials science. Materials in medicine》2008,19(4):1503-1513
Biodegradable polymers reinforced with an inorganic phase such as calcium phosphate glasses may be a promising approach to
fulfil the challenging requirements presented by 3D porous scaffolds for tissue engineering. Scaffolds’ success depends mainly
on their biological behaviour. This work is aimed to the in vitro study of polylactic acid (PLA)/CaP glass 3D porous constructs
for bone regeneration. The scaffolds were elaborated using two different techniques, namely solvent-casting and phase-separation.
The effect of scaffolds’ micro and macrostructure on the biological response of these scaffolds was assayed. Cell proliferation,
differentiation and morphology within the scaffolds were studied. Furthermore, polymer/glass scaffolds were seeded under dynamic
conditions in a custom-made perfusion bioreactor. Results indicate that the final architecture of the solvent-cast or phase
separated scaffolds have a significant effect on cells’ behaviour. Solvent-cast scaffolds seem to be the best candidates for
bone tissue engineering. Besides, dynamic seeding yielded a higher seeding efficiency in comparison with the static method. 相似文献
4.
Heimann RB Schürmann N Müller RT 《Journal of materials science. Materials in medicine》2004,15(9):1045-1052
To evaluate the in vivo performance of "duplex" hydroxylapatite top coat/TiO(2) bond coat systems, cylindrical Ti6Al4V rods of 130 mm in length and 11-13 mm in diameter were coated by atmospheric plasma spray (APS) technique with both a standard hydroxylapatite (HAp) layer and a HAp+TiO(2) bond coat "duplex" layer. In this pilot study coated and uncoated rods serving as controls were implanted into the femur of sheep so that their distal ends were freely suspended in the medulla of the femur. After an observation time of six months it was found that bone apposition and bone ingrowth were considerably increased in the presence of a osteoconductive coating. In particular, in vivo spalling and delamination frequently observed with HAp coatings was virtually absent in duplex coatings owing to the strong adhesion of the bond coat to the HAp top coat that anchored the latter solidly to the metallic surface of the implant. Some tentative mechanisms leading to this improved coating adhesion will be discussed. 相似文献
5.
The chemical vapour deposition of MoSi2 on plane substrates (graphite or sintered-SiC) and ceramic fibres has been studied from MoCl4–SiCl4–H2–Ar gas mixtures at 900相似文献
6.
Guantong Chen Weidong Zhuang Yunsheng Hu Yuanhong Liu Ronghui Liu Huaqiang He 《Journal of Materials Science: Materials in Electronics》2013,24(6):2176-2181
Green emitting Eu2+-doped Ba3Si6O12?δ N2+2/3δ phosphors with δ value varying in the range of ?0.6 to 1.8 were synthesized by firing the raw materials of α-Si3N4, SiO2, BaCO3 and Eu2O3 at 1,350 °C for 12 h under a N2/H2 atmosphere. The solid-solution and luminescence properties of as-prepared Ba3Si6O12?δ N2+2/3δ :Eu2+ phosphors were investigated by XRD, O/N automatic analyzer and UV–Vis spectrophotometer. The composition-dependent solid solution of Ba3Si6O12?δ N2+2/3δ with small range of δ is established. The emission wavelength with a range of 522–545 nm by varying δ value as a function of dopant Eu2+ is observed in this phosphor. The emission band shows a shift to higher energy and a diverse quenching concentration with an increase of N/O ratio in Ba3Si6O12?δ N2+2/3δ :Eu2+ phosphors. The measured results suggest that Ba3Si6O12?δ N2+2/3δ :Eu2+ possesses broad applications as an effective green phosphor in producing white light-emitting diodes. 相似文献
7.
Alireza Abrishamchian Tabassom Hooshmand Mohammadreza Mohammadi Farhood Najafi 《Materials science & engineering. C, Materials for biological applications》2013,33(4):2002-2010
In the present research, the introduction of multi-walled carbon nanotubes (MWCNTs) into the hydroxyapatite (HA) matrix and dip coating of nanocomposite on titanium alloy (Ti–6Al–4V) plate was conducted in order to improve the performance of the HA-coated implant via the sol–gel method. The structural characterization and electron microscopy results confirmed well crystallized HA–MWCNT coating and homogenous dispersion of carbon nanotubes in the ceramic matrix at temperatures as low as 500 °C. The evaluation of the mechanical properties of HA and HA/MWCNT composite coatings with different weight percentages of MWCNTs showed that the addition of low concentrations of MWCNTs (0.5 and 1 wt.%) had improved effect on the mechanical properties of nanocomposite coatings. Moreover, this in vitro study ascertained the biocompatibility of the prepared sol–gel-derived HA/MWCNT composite coatings. 相似文献
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