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实验是通过以橄榄油为原料,四氢呋喃作共溶剂,NaOH为催化剂制备生物柴油。用气相色谱分析方法,通过对反应温度、醇油摩尔比、催化剂的量、反应时间的研究,得出在各自的最优化条件下橄榄油、为97.3%。 相似文献
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茶油的精制方法及应用 总被引:9,自引:0,他引:9
茶油具有"东方橄榄油"的美称,其物理化学性质与橄榄油相似,其脂肪酸组成和甘油三酯结构与橄榄油相同,还含有橄榄油所没有的特定生理活性物质如山茶苷、山茶皂苷、茶多酚等性质,具有丰富的营养价值和应用价值.本文主要介绍了茶油的精制方法、应用及其发展前景. 相似文献
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采用超声波喷雾干燥方法对橄榄油进行微胶囊化研究,探讨进风温度对橄榄油微胶囊含水量及包埋率的影响,进而评价微胶囊化橄榄油的存储稳定性。橄榄油的超声波喷雾微胶囊化研究结果显示:进风温度过高造成橄榄油微胶囊色泽加深,油脂析出,包埋率降低;进风温度过低导致橄榄油微胶囊干燥不充分,含水量较高。对喷雾干燥条件进行优化后获得橄榄油超声波喷雾微胶囊化条件:进风温度180℃,进料速率6 r/min。此条件下制备的橄榄油微胶囊包埋率可达98.2%。存储稳定性研究结果表明:橄榄油在不同光照、温度和湿度等条件下存储至30 d时,光照下微胶囊化橄榄油的过氧化值约是未包埋橄榄油的1/5,酸值约是未包埋橄榄油的1/3;避光下微胶囊化橄榄油过氧化值及酸值约是未包埋橄榄油的2/3;因温度升高,未包埋橄榄油氧化值增加1倍左右,酸值最大值可增加77.8%,而微胶囊化橄榄油过氧化值增加仅15%,酸值最大增加40.5%。微胶囊化橄榄油的过氧化值及酸值均低于未包埋橄榄油,微胶囊对橄榄油起到延缓氧化的作用,提高了橄榄油的存储稳定性。 相似文献
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介绍希腊橄榄油加工和市场现状,关键技术及其特征,主要设备,橄榄油的等级、质量指标和感官评价,化学组成及分析方法,影响橄榄油质量的因素,废水和果渣的组成及其副产物的开发利用以及橄榄油的食用及药用功能等,提出油橄榄的综合利用和加工方向。 相似文献
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The purpose of the work to study biodiesel production by transesterification of Jatropha oil with methanol in a heterogeneous system, using alumina loaded with potassium nitrate as a solid base catalyst. Followed by calcination, the dependence of the conversion of Jatropha oil on the reaction variables such as the catalyst loading, the molar ratio of methanol to oil, reaction temperature, agitation speed and the reaction time was studied. The conversion was over 84% under the conditions of 70 °C, methanol/oil mole ratio of 12:1, reaction time 6 h, agitation speed 600 rpm and catalyst amount (catalyst/oil) of 6% (w). Kinetic study of reaction was also done. 相似文献
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以大豆油、甲醇为原料,研究了通过白云石催化酯交换反应制取生物柴油的工艺的条件。用气相色谱-质谱分析法,并对反应温度、醇油摩尔比、反应时间、催化剂的用量及催化剂粒径进行考察,得出最佳合成条件为:反应温度65℃、反应时间2h、醇油摩尔比7:1,催化剂用量2%,催化剂粒径为80~150目,在此条件下得到生物柴油转化率为77.36%。 相似文献
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Optimization of the production of biodiesel from soybean oil by ultrasound assisted methanolysis 总被引:1,自引:0,他引:1
This paper evaluates and optimizes the production of biodiesel from soybean oil and methanol using sodium hydroxide as catalyst. The study and optimization was carried out at low catalyst concentration (0.2 to 0.6 w/w). The reaction was carried out with application of low-frequency high-intensity ultrasound under atmospheric pressure and ambient temperature in a batch reactor. Response surface methodology (RSM) was used to evaluate the influence of methanol to oil ratio and catalyst concentration on soybean oil conversion into biodiesel. Analysis of the operating conditions by RSM showed that the most important operating condition affecting the reaction was the methanol to oil ratio, while catalyst amount showed little significance in the transesterification reaction. Total consumption of oil was obtained when alcohol to oil ratio of 9:1 and catalyst concentration of 0.2 w/w were applied. 相似文献
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大麻籽油和甲醇经NaOH/PAM催化合成生物柴油,本实验在醇油比固定的情况下考察了催化剂的碱含量、催化剂用量对酯交换转化率的影响、碱量及反应时间分别对转化率和皂化百分数的影响,采用红外光谱技术对催化剂进行分析,确定了较适宜的反应条件.结果表明:实际碱量随NaOH添加量的增加而增加;催化剂用量增加,原料油转化率增加;反应时间的增加,原料油转化率曲线增加到一定水平后趋于平缓;较适宜的反应条件为PN-4催化剂用量3%,反应时间为60 min. 相似文献
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Lin Liu Ding Ma Huiying Chen Heng Zheng Mojie Cheng Yide Xu Xinhe Bao 《Catalysis Letters》2006,107(1-2):25-30
Zn/I2 was found to be a practical and effective catalyst for the transesterification of soybean oil with methanol. A study for
optimizing the reaction conditions such as the molar ratio of methanol to oil, the reaction time and the catalyst amount,
was performed. The highest conversion of 96% was obtained under the optimum conditions. Further, the effect of free fatty
acids and water in the soybean oil on the catalytic activity of the catalysts was also investigated. 相似文献
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Effect of Different Cosolvents on Transesterification of Waste Cooking Oil in a Microreactor 下载免费PDF全文
Biodiesel was prepared from waste cooking oil combined with methanol. The process was performed via transesterification in a microreactor using kettle limescale as a heterogeneous catalyst and various cosolvents under different conditions. n‐Hexane and tetrahydrofuran were selected as cosolvents to investigate fatty acid methyl esters (FAMEs). To optimize the reaction conditions, the main parameters affecting FAME% including reaction temperature, catalyst concentration, oil‐to‐methanol volumetric ratio, and cosolvent‐to‐methanol volumetric ratio were studied via response surface methodology. Under optimal reaction conditions and in the presence of the cosolvents n‐hexane and tetrahydrofuran, high FAME purities were achieved. Considering the experimental results, the limescale catalyst is a unique material, and the cosolvent method can reduce significantly the reaction time and biodiesel production cost. 相似文献