Linear and Nonlinear Drying Behavior in Tuberous Crop Slices

Understanding drying physics is a complex task because interactions between phases and variations in thermal properties change over time. In this investigation we used two models to simulate the drying of potatoes slices. Drying kinetics were modeled by both the drying characteristic curve (DCC) method and by a mechanistic approach implemented in COMSOL Multiphysics. The DCC was developed on the basis of experimental data and a referential drying rate, which for potatoes is the maximum evaporation rate during the process. The surface thermal evolution was considered to estimate the drying rate curve and the drying stages. The phenomenological model considers both the transport of free water and water vapor by applying a mechanistic approach. In order to simulate free water transport we took into account the capillary diffusivity term, and to simulate water vapor evacuation we considered the desorption isotherm. Two drying conditions were analyzed, 1.0 and 2.2 m/s of air flow with 60°C and 30% relative humidity (RH). The mechanistic model solves the primary unknown's moisture content, temperature, and dry air density. Both models were compared against experimental data. The simulation correctly describes the drying kinetics for the trial at 2.2 m/s and fails to simulate the phenomena at 1.0 m/s. Two different drying behaviors influenced by air flow speed were identified by following the evolution of surface temperature and mass flux. The dependence of mass flux on the difference in temperature (T_air?T_surface) shows that the area of exchange is a very important parameter to be considered in simulations, because both linear and nonlinear behaviors are manifested.     

Drying kinetics of cork planks in a cork pile in the field

Moisture content is one important parameter in the trading of raw cork planks after harvesting. This study presents a mathematical modeling of the drying curve of raw cork planks in a cork pile in the field, under natural sun drying conditions. Experimental data were obtained by following the water loss (i.e. by daily weighing) of 97 cork planks positioned in nine points within a cork pile. Immediately after harvesting, the raw cork planks had a mean moisture content in a dry basis of 40.4% and after 20-day drying 16.6%. The drying process of the cork planks showed three phases: drying was very fast in the first 2 days; in the next 2–15 days there was a decreasing drying rate; and a final phase, after 15 days in the cork pile, with a slightly decreasing drying rate. Mathematical modeling provided a direct relation between moisture content and drying time. After comparing sixteen empirical drying models, the Modified Henderson and Pabis model showed the best fit. According to this model, the cork planks are commercial dry (14% moisture content in a wet basis) 15 days after harvest.     

COMBINED CONVECTIVE-MICROWAVE DRYING OF AGAR GELS: INFLUENCE OF MICROWAVE POWER ON DRYING KINETICS

The use of microwave energy in the drying of deformable material such as gel considerably reduces drying time and enables the control of retraction in the sample. A further advantage is that no hot spots are produced, allowing a dry product of superior quality to be obtained.The aim of this work has been to determine the kinetics of the convective-microwave drying process of agar gel plates. For this purpose, we developed a pilot closed loop, computer-controlled apparatus of convective-microwave drying, that enables the drying air conditions to be changed and the microwave power to be supplied over a wide value range. The equipment also records the sample surface temperature by means of an infrared thermometer. The drying curves obtained for plane geometry present four different drying phases: an initial phase where a rapid increase in the drying rate and in the surface temperature can be observed, as well as a constant rate phase that ends in the so-called convective critical moisture content, a first falling rate phase that concludes in the microwave critical moisture point, and finally a second falling rate phase. Combined convective-microwave drying enables a considerable reduction in drying time compared to convective drying, the time required being inversely proportional to the microwave power supplied. The empirical equation that best represents the kinetics is of the Page type. The absorbed volumetric power in terms of the moisture content was experimentally estimated, with the experimental data fitting an empirical equation.     

COMBINED CONVECTIVE-MICROWAVE DRYING OF AGAR GELS: INFLUENCE OF MICROWAVE POWER ON DRYING KINETICS

ABSTRACT

The use of microwave energy in the drying of deformable material such as gel considerably reduces drying time and enables the control of retraction in the sample. A further advantage is that no hot spots are produced, allowing a dry product of superior quality to be obtained.The aim of this work has been to determine the kinetics of the convective-microwave drying process of agar gel plates. For this purpose, we developed a pilot closed loop, computer-controlled apparatus of convective-microwave drying, that enables the drying air conditions to be changed and the microwave power to be supplied over a wide value range. The equipment also records the sample surface temperature by means of an infrared thermometer. The drying curves obtained for plane geometry present four different drying phases: an initial phase where a rapid increase in the drying rate and in the surface temperature can be observed, as well as a constant rate phase that ends in the so-called convective critical moisture content, a first falling rate phase that concludes in the microwave critical moisture point, and finally a second falling rate phase. Combined convective-microwave drying enables a considerable reduction in drying time compared to convective drying, the time required being inversely proportional to the microwave power supplied. The empirical equation that best represents the kinetics is of the Page type. The absorbed volumetric power in terms of the moisture content was experimentally estimated, with the experimental data fitting an empirical equation.     

微波干燥工艺参数对玉米爆腰率的影响

玉米收获后需干燥至安全水分后储藏,干燥方式及合理的工艺过程对干燥品质有很大的影响,玉米干燥后的爆腰率是其品质的重要指标。利用自制的微波干燥试验测试系统对玉米进行干燥试验,得出了玉米微波干燥的特征曲线及干燥温度特性,探讨了三个主要工艺参数单位功率、干燥最高温度、平均失水率对爆腰率的影响。实验结果表明,玉米微波干燥中按失水率的变化可以分为预热、恒速、降速三个阶段,预热段较长,水分主要在恒速段排出;温度经历了上升和趋于稳定的过程;爆腰率随各参数的增大而升高。得到的初步结论是：玉米微波干燥最好在单位干燥功率0.3W／g以下、干燥最高温度不超过70℃、平均失水率不大于0.2％／min的条件下进行。     

SIMULATION OF PLUM DRYING IN DEEP BED

Thin layer air drying of plum was studied. The drying conditions in this study are : dry bulb temperature ranging from 60 to 100 °C, air moisture content ranging from 0.008 to 0.089 kg water/kg dry air and air velocity ranging from 0.5 to 2 1x11s. An exponential model was used to describe the drying curve. The heat and moisture balances on the air were used to calculate the outlet air temperature and its moisture content. The heat balance on the product was used to calculate the product temperature. These equations were used to predict the drying of plum in deep bed. A good agreement between the experimental and calculated product moisture content, the product temperature and the outlet air temperature were obtained     

SIMULATION OF PLUM DRYING IN DEEP BED

Thin layer air drying of plum was studied. The drying conditions in this study are : dry bulb temperature ranging from 60 to 100 °C, air moisture content ranging from 0.008 to 0.089 kg water/kg dry air and air velocity ranging from 0.5 to 2 1x11s. An exponential model was used to describe the drying curve. The heat and moisture balances on the air were used to calculate the outlet air temperature and its moisture content. The heat balance on the product was used to calculate the product temperature. These equations were used to predict the drying of plum in deep bed. A good agreement between the experimental and calculated product moisture content, the product temperature and the outlet air temperature were obtained     

热泵干燥怀山药片的工艺研究

以提高怀山药干燥效率和产品品质为目标,本文利用热泵干燥方法,研究了热泵温度,风速,怀山药切片厚度对干燥曲线,L值,以及干制品复水率的影响。试验表明,热泵温度,风速及切片厚度都对怀山药片的干燥速率有显著影响。怀山药片热泵干燥的最佳工艺参数为：热泵温度40℃,风速1．0m/s,切片厚度5mm,干燥后怀山药片的L值和复水率分别为82．07和85．08％。     

Drying Kinetics of Some Building Materials

Abstract

Moisture is one of the most deteriorating factors of buildings. The deteriorating effect of moisture occurs mainly during the drying phase, not in the wetting phase. Environmental factors, such as air temperature, air humidity, and air velocity affect drying. An experimental air dryer of controlled drying air conditions was used to investigate the drying performance of 4 stone materials, 2 bricks, and 6 plasters. Drying kinetics was examined at 3 air temperatures, 5 air humidities, and 3 air velocities. A first-order kinetics model was obtained in which the drying time constant was a function of the drying conditions, and the equilibrium material moisture content was described by the modified Oswin equation. The parameters of the proposed model were found to be affected strongly by the material characteristics.     

用高露点空气干燥小木块时挥发性有机物的释放

Emission of volatile organic compounds (VOCs) during drying of wood particles for particleboard manufacture, or for production of refined biofuels, is a potential environmental problem. The aim of this work is to study the emissions of VOCs during drying, and the influence on the emissions by different drying parameters. The experiments have mainly been done in a batch fluidized bed dryer, but measurements have also been done in a, pilot scale, continuous fluidized bed dryer. The parameters studied are air flow rate through the bed, air temperature, air dewpoint, and bed height. Since the present trend in biofuels and particle drying is towards very high dewpoints during drying, some measurements have been made at dewpoints up to 95℃, corresponding to a water content of 3.2 kg water per kilogram dry air. The emissions have been measured in two different ways, online during drying with a flame ionization detector and through wood analyses of the terpene content in the wood particles before and after dryi     

Enthalpy-Entropy Compensation for Water Loss of Vegetable Tissues during Air Drying

Transition state theory was used to study enthalpy-entropy compensation for water loss during air drying of potato and apple slices. Slices of either potato or apple of 4-mm thickness, 40 mm diameter and air drying temperatures of 323, 333, 343, and 353 K were employed in the experiments. Moisture content and internal potato and apple slice temperatures were recorded during the drying runs. Water loss during drying was described by the unsteady-state Fick's equation and moisture diffusivity evolution was established by applying the method of the slopes. Thus, the experimental drying curve was compared to the theoretical diffusion curve, and the slope of the two curves were estimated at the same moisture content to in order give the corresponding value of diffusivity. During drying, the moisture diffusivity reached a maximum value as the water content of potato and apple slice was around 1 kg water/kg dry solid, regardless of the air temperature. The isokinetic temperature was found to be 320.2 and 312.8 K for potato and apple tissues, respectively. These values were greater than the experimental harmonic mean temperature, which was found to be 307.4 and 308.3 K for potato and apple tissues, respectively. Thus, it was concluded that the water loss process is enthalpy controlled.     

The Drying Kinetics and Equilibrium Moisture Content of MDF Fibers

An experimental device was constructed to study the drying kinetics of wood fibers under controlled conditions. The device consisted of a drying chamber in which a net basket filled with the fiber material was connected to a load cell. The drying medium was then forced through the basket at controlled levels of humidity and temperature.

Experiments were performed with spruce fibers and the drying medium at varying temperature (50–170°C) and relative humidity (1–86%). In general, the drying rate increased with increasing temperature and decreasing relative humidity. A constant drying rate period was observed in all cases. The critical moisture content was approximately 1.25. The characteristic drying curve has a slight downward concave shape. The equilibrium moisture contents obtained at ambient temperature agree well with data in the literature.     

Experimental Study and Mathematical Modeling of Green Pea Drying in a Spouted Bed

In this study, green pea drying is investigated experimentally in a laboratory-scale spouted bed dryer. A mathematical model is also developed to investigate the effect of operating conditions on the performance of the system. The effect of operating parameters such as inlet air temperature, particle size, and flow rate of the drying air on the performance of the dryer are studied experimentally. In order to build the process model, it is necessary to analyze the transport in both solid and gas phases. A complete set of equations with no adjustable parameters is derived for existing zones in the spouted bed dryer in order to predict variations in the temperature and moisture content of the solid and gas phases with time for batch drying conditions. Model results are compared with corresponding experimental data. Agreement between the model results and experimental data is good.     

Combined Convective and Microwave Drying of Agglomerated Sand: Internal Transfer Modeling with the Gas Pressure Effect

In order to improve the industrial drying (hot air and microwave) of inserts made of agglomerated sand, a comprehensive internal heat and water transfer model has been proposed. In this model, the internal gas phase pressure effect was made perfectly explicit, especially the phenomena of liquid and vapour transfer by filtration and of liquid expulsion at the surface. This model was validated on the basis of the experimental mean water content and core temperature curves for drying trials at different microwave powers. Then, it was used for comparing the drying time and the internal pressure level calculated for four particular processes: a standard process with high temperature air applied all over the time, a strong process with high power microwaves applied all over, and two processes which alternate the two heating modes. It was demonstrated that the combined and alternative processes provide a real possibility for faster drying with less internal pressure and thus with less cracking risk. The microwaves should be applied only in the first hour of the process and with decreasing power. The decrease of the drying time was around 30% with regard to the hot air standard process.     

Numerical Simulation of Vacuum Drying by Luikov's Equations

A two-dimensional mathematical model was developed to simulate coupled heat and mass transfer in apple under vacuum drying. Luikov's equations are the governing equations in analyzing heat and mass diffusion problems for capillary-porous bodies. The model considers temperature- and moisture-dependent material properties. The aim of this study is to analyze the influence of some of the most important operating variables, in particular, pressure and temperature of drying air, on the drying of apple. The resulting system of unsteady-state partial differential equations has been solved by a commercial finite element method (FEM) package called FEMLAB (COMSOL AB, Stockholm, Sweden). Simulations, carried out in different drying conditions, showed that temperature is more effective than air pressure in determining the drying rate. A parametric study was also carried out to determine the effects of heat and mass transfer coefficients on temperature and moisture content distributions inside apple during vacuum drying. A comparison between the theoretical predictions and a set of experimental results reported in the literature showed very good agreement, especially during the first 4,200 s, when experimental data and theoretical predictions overlapped and relative errors never exceeded 2%.     

Temperature Characteristics of Pharmaceutical Powders During Microwave Drying

The internal temperature of wetted pharmaceutical powder samples dried in an experimental microwave system were monitored. In general, the temperature profile consisted of three distinct stages: short preheating stage, constant temperature period, and decreasing temperature phase. Approaching the end of the constant rate period, a local maximum in the temperature curve was observed. The development of the internal temperature profile was observed to be material dependent, with the dielectric, physical, and thermal properties of the powder and solvent being contributory factors. The characteristics were also dependent on bed dimensions (surface area and depth), with an increase in surface area and decrease in depth providing lower product temperatures. The surface temperature remained lower than the center temperature throughout the drying process, with the differential through the sample depth increasing on reducing the moisture content. A nonuniform temperature distribution developed across the sample cross section. Sample agitation was found to aid temperature leveling.     

Temperature Characteristics of Pharmaceutical Powders During Microwave Drying

The internal temperature of wetted pharmaceutical powder samples dried in an experimental microwave system were monitored. In general, the temperature profile consisted of three distinct stages: short preheating stage, constant temperature period, and decreasing temperature phase. Approaching the end of the constant rate period, a local maximum in the temperature curve was observed. The development of the internal temperature profile was observed to be material dependent, with the dielectric, physical, and thermal properties of the powder and solvent being contributory factors. The characteristics were also dependent on bed dimensions (surface area and depth), with an increase in surface area and decrease in depth providing lower product temperatures. The surface temperature remained lower than the center temperature throughout the drying process, with the differential through the sample depth increasing on reducing the moisture content. A nonuniform temperature distribution developed across the sample cross section. Sample agitation was found to aid temperature leveling.     

Drying Kinetics and Antioxidant Phytochemicals Retention of Salak Fruit under Different Drying and Pretreatment Conditions

Kinetics of hot air drying and heat pump drying were studied by performing various drying trials on salak slices. Isothermal drying trials were conducted in hot air drying and heat pump drying at a temperature range of 40–90°C and 26–37°C, respectively. Intermittent drying trials were carried out in heat pump drying with two different modes: periodic heat air flow supply and step-up air temperature. It was observed that the effects of relative humidity and air velocity on drying rate were significant when moisture content in salak slices was high, whereas the effects of temperature prevailed when the moisture content was low. As such, it was proposed that drying conditions should be manipulated according to the moisture transport mechanisms at different stages of drying in order to optimize the intermittent drying and improve the product quality. Generally, loss of ascorbic acid during drying was attributed to thermal degradation and enzymatic oxidation, whereas the loss of phenolic compounds was mainly due to thermal degradation. Experimental results showed that heat pump drying with low-temperature dehumidified air not only enhanced the drying kinetics but produced a stable final product. Heat pump–dried samples retained a high concentration of ascorbic acid and total phenolic compounds when an appropriate drying mode was selected.     

Combined Crystallization and Drying in a Pilot-Scale Spray Dryer

Combined crystallization and drying of lactose solutions was performed in a pilot-scale spray dryer over a wide range of operating conditions. The effect of different parameters, including temperature, moisture content, atomizing air flow rate, liquid feed rate, main drying air flow rate, and particle size, on the degree of crystallinity of the spray-dried powders was analyzed. Water-induced crystallization (WIC) and modulated differential scanning calorimetry (MDSC) were used to assess the effect of these parameters on the degree of crystallinity of the spray-dried powders. The particles were characterized in terms of the final moisture content using WIC and distinctive differences in the peak heights, which are indicative of the particle crystallinity, were found for spray-dried particles using different drying conditions, supporting the results from MDSC. MDSC showed that decreasing the inlet air temperature by 40°C increased the degree of crystallinity in the particles threefold from 22 to 72%. A decrease in the inlet air temperature may decrease the particle temperature, resulting in wetter particles, and a lower temperature meant a longer particle drying time and allowed the particles to rearrange themselves into a more crystalline form. Up to 72% crystallinity is achievable in a pilot-scale spray dryer by suitable adjustment of the operating conditions. The results suggest differences in the rate of crystallization and particle size between small and pilot-scale spray dryers.