Fretting Fatigue Behavior of Cavitation Shotless Peened Ti–6Al–4V

Fretting fatigue behavior of cavitation shotless peened (CSP) titanium alloy, Ti–6Al–4V was investigated. Constant amplitude fretting fatigue tests were conducted at several maximum stress levels, σ_max, ranging from 400 to 555 MPa with a stress ratio of 0.1. Test results showed that the fretting fatigue life was enhanced by CSP treatment as compared to the unpeened specimen, but the enhancement was not as large as that from the shot-peening treatment. Residual stress measurements by X-ray diffraction method before and after fretting test showed that residual compressive stress was relaxed during fretting fatigue. Before fretting, CSP specimen had higher compressive residual stress on the surface than the shot-peened specimen. However, greater residual stress relaxation occurred in CSP specimen such that the relaxed compressive residual stress profile near the contact surface of CSP specimen was lower than that of shot-peened specimen. This lower compressive residual stress from fretting fatigue was the reason for shorter fretting fatigue life of CSP specimen as compared to shot-peened specimen at the applied stress level.     

Influence of Calf Serum on Fretting Behaviors of Ti–6Al–4V and Diamond-Like Carbon Coating for Neck Adapter–Femoral Stem Contact

Influences of newborn calf serum on the fretting behaviors of Ti–6Al–4V and diamond-like carbon coating were investigated using a fretting-wear test rig with a cylinder-on-flat contact. The results indicated that, for the Ti–6Al–4V/Ti–6Al–4V contact, the friction coefficients were high (0.8–1.2) and the wear volumes presented an increase with the increase in the displacement amplitude under dry laboratory air conditions. Under serum-liquid conditions, the Ti–6Al–4V/Ti–6Al–4V contact presented significantly larger wear volumes under the displacement of ±?40 µm; however, it presented significantly lower friction coefficients (0.25–0.35) and significantly smaller wear volumes under the displacement of ±?70 µm. For the DLC coating/Ti–6Al–4V contact, the coating response wear maps could be divided into two areas: the coating working area (low normal force conditions) and the coating failure area (high normal force conditions). In the coating working area, the DLC coating could protect the substrate with low friction, low wear volume, and mild damage in the coating. The presence of serum had a positive influence on the tribological performance of the DLC coating. Furthermore, the positive influence was more significant under larger displacement amplitudes condition.     

Effect of Plasma Nitriding Environment and Time on Plain Fatigue and Fretting Fatigue Behavior of Ti–6Al–4V

Plasma nitriding was performed on Ti–6Al–4V fatigue test samples at 520°C in two environments (nitrogen and nitrogen–hydrogen mixture in a ratio of 3:1) for two time periods (4 and 18 h). Plain fatigue and fretting fatigue tests were conducted on unnitrided and plasma nitrided samples. Plasma nitriding degraded lives under both plain fatigue and fretting fatigue loadings. The samples nitrided in nitrogen exhibited superior lives compared with the samples nitrided in the nitrogen–hydrogen mixture, possibly due to the relatively higher hardness (and presumably lower toughness) of the nitrided layer of the samples nitrided in the nitrogen–hydrogen mixture environment. For those samples nitrided in the nitrogen–hydrogen mixture, those nitrided for 18 h exhibited superior lives compared with those nitrided for 4 h. This trend was observed for samples nitrided in nitrogen gas at lower stress levels only; the converse was true at higher stress levels of 550 MPa and 700 MPa under plain fatigue loading. However, under fretting fatigue loading, the plasma nitriding time did not influence the lives significantly.     

Tribological Behaviour of SiC Particle Reinforced Al–Si Alloy

The purpose of this study is to explore the effect of SiC reinforcement along with immiscible element addition in spray formed Al–Si base alloy. The investigation is done for four different compositions, i.e., Al–Si base alloy, Al–Si/SiC, Al–Si–5Sn/SiC and Al–Si–10Sn/SiC composite. The dry sliding wear properties of base alloy and composites were investigated against EN 31 steel at five different normal loads (14.7, 24.5, 34.3, 44.1 and 53.9 N). The tests were carried out in dry sliding conditions with a sliding speed of 1.6 ms⁻¹ over pin-on-disc tribometer. Each composition is tested at four different temperatures 50, 75, 100 and 150 °C. To determine the wear mechanism, the worn surfaces of the samples were examined using scanning electron microscope (SEM). The composites emerge to be better wear resistant material than base alloy especially at higher loads. The optimum wear reduction was obtained in Al–Si–10Sn/SiC composite at all the different normal loads and temperatures.     

Analysis of Fretting Fatigue of Cavitation Shotless Peened Ti–6Al–4V

Fretting fatigue behavior of cavitation shotless peened titanium alloy, Ti–6Al–4V coupons was investigated using finite element method and a critical plane-based multi-axial fatigue parameter. Cavitation shotless peening (CSP)-induced compressive residual stress, which was larger at the contact surface than its counterpart from the shot peening (SP). However, compressive residual stress decreased more sharply with distance from the contact surface in CSP than in SP. Analysis using a critical plane-based multi-axial fatigue parameter demonstrated that the crack initiation would occur inside the cavitation shotless peened specimen which matched with the experimental observations. On the other hand, crack initiation would occur on the contact surface in the shot peened specimen which again was in agreement with experiments. The analysis also showed that the crack propagation part of the total fretting fatigue life was longer in the shot peened specimen than in the cavitation shotless peened specimen while the crack initiation part was almost equal from both peening methods. Therefore, CSP could not improve the fretting fatigue life/strength as much as the SP did but it improved relative to the un-peened specimen.     

Tribological behaviors of Ti–6Al–4V modified by chemical methods

In order to improve the tribological properties of titanium-based implants, sodium hydroxide (NaOH), hydrogen peroxide (H₂O₂) solutions, sol–gel hydroxyapatite (HA) film, thermal treatment and combined methods of NaOH solution/HA film, H₂O₂ solution/HA film are used to modify the surfaces of Ti–6Al–4V (coded TC4). The chemical states of some typical elements in the modified surfaces were detected by means of X-ray photoelectron spectroscopy (XPS). The tribological properties of modified surfaces sliding against an AISI52100 steel ball were evaluated on a reciprocating friction and wear tester. As the results, complex surfaces with varied components are obtained. All the methods are effective in improving the wear resistance of Ti–6Al–4V in different degrees. Among all, the surface modified by the combined method of NaOH solution/HA film gives the best tribological performances. The friction coefficient is also greatly reduced by the modification of NaOH solution. The order of the wear resistance under 3 N is as following: Ti–NaOH–HA>Ti–NaOH>Ti–HA>Ti–H₂O₂–HA>Ti–H₂O₂ >Ti–500; under 1 N is Ti–HA, Ti–NaOH–HA>Ti–NaOH. For Ti–H₂O₂, a very low friction coefficient and long wear life over 2000 passes is obtained under 1 N. SEM observation of the morphologies of worn surfaces indicates that the wear of TC4 is characteristic of abrasive wear. Differently, abrasion, plastic deformation and micro–crack dominate the wear of Ti–HA; slight abrasive wear dominate the wear mechanism of Ti–NaOH and microfracture and abrasive wear for Ti–NaOH–HA and Ti–H₂O₂–HA, while the sample modified by thermal treatment is characterized by sever fracture. The superior friction reduction and wear resistance of HA films are greatly attributed to the slight plastic deformation of the film. NaOH solution is superior in improving the wear resistance and decreasing the friction coefficient under relative higher load (3 N) and H₂O₂ is helpful to reduce friction and wear under relatively lower load (1 N). Combined method of Ti–NaOH–HA is suggested to improve the wear resistance of Ti–6Al–4V for medial applications under fretting situations.     

Fretting corrosion behaviour of Ti–6Al–4V/PMMA contact in simulated body fluid

Abstract

The fretting corrosion of a Ti–6Al–4V flat in contact with a poly(methyl methacrylate) (PMMA) ball in 0·9 wt-% NaCl solution was investigated using a fretting rig operating under electrochemical control. The effect of potential and of normal load on friction, wear and electrochemical response was studied under gross slip regime. No noticeable mechanical deterioration of the Ti–6Al–4V surface could be observed. At anodic potential, alloy corrosion was only slightly enhanced by fretting. Wear of PMMA was large and controlled by third body formation. A correlation between PMMA wear coefficient and thickness of third body was observed.     

Sensing of Ellipsoidal Inclusions in a Biomedical Ti–6Al–4V Alloy by Magnetic Means

Russian Journal of Nondestructive Testing - In this work, we conducted an experimental research to verify a developed analytical model based on the magnetic sensing of thermoelectric currents...     

Tribological Behavior of Micrometer- and Submicrometer-Size Cenosphere Particulate-Filled Glass Fiber–Reinforced Vinylester Composites Under Dry and Water-Lubricated Sliding Conditions

In this work, the tribological behavior of micrometer and submicrometer cenosphere particulate–filled E-glass fiber–reinforced vinylester composites have been investigated on a pin-on-disc tester under dry sliding and water-lubricated sliding conditions. Three different uniform sizes of cenosphere particles (2 μm, 900 nm, 400 nm) were used as fillers in the glass fiber–reinforced vinylester composites. The weight fraction of cenosphere particles has been varied in the ranges from 5, 10, 15, to 20 wt%. The experimental results show that all of the composites exhibited lower coefficient of friction and lower wear resistance under water-lubricated sliding conditions than under dry sliding. It has been noted that the submicrometer size (400 nm) cenosphere particulates as fillers contributed significantly to improve the wear resistance. It has also been noted that 10 wt% of the cenosphere particles is the most effective in reducing the wear rate and coefficient of friction. Effects of various wear parameters such as applied normal loads, sliding speeds, particle size, and particle content on the tribological behavior were also discussed. In order to understand the wear mechanism, the morphologies of the worn surface were analyzed by means of scanning electron microscopy (SEM) for composite specimens under both dry and water-lubricated sliding conditions.     

Production and Heat Treatment of Ti6–Al5.5–V–1.8Sn Powder Titanium Alloy

The mechanical properties of Ti6–Al5.5–V–1.8Sn powder titanium alloy are investigated as a function of its structure, which, in turn, depends on its production and heat treatment (quenching and aging).     

Tribo-layer and its role in dry sliding wear of Ti–6Al–4V alloy

Dry sliding wear tests were performed for Ti–6Al–4V alloy under a load of 50–250 N at 25–500 °C on a pin-on-disk elevated temperature tester. Worn surfaces and subsurfaces were thoroughly investigated for the morphology, composition and structure of tribo-layers. Ti–6Al–4V alloy could not be considered to possess poor wear resistance at all times, and presented a substantially higher wear resistance at 400–500 °C than at 25–200 °C. The tribo-layer, a mechanical mixing layer, was noticed to exist on worn surfaces under various conditions. High wear rate at 25–200 °C was ascribed to no protective tribo-layer containing no or trace tribo-oxides. As more oxides appeared in the tribo-layers, they presented an obviously protective role due to their high hardness, thus giving a reasonable explanation for high wear resistance of Ti–6Al–4V alloy at 400–500 °C.     

Minimal quantity lubrication-MQL in grinding of Ti–6Al–4V titanium alloy

Titanium and its alloys are attractive materials due to their unique high strength–weight ratio that is maintained at elevated temperatures and their exceptional corrosion resistance. The major application of titanium has been in the aerospace industry. On the other hand, titanium and its alloys are notorious for their poor thermal properties and are classified as difficult-to-machine materials. The problems that arise during grinding of titanium alloys are attributed to the high specific energy and high grinding zone temperature. Significant progress has been made in dry and semidry machining recently, and minimal quantity lubrication (MQL) machining in particular has been accepted as a successful semidry application because of its environmentally friendly characteristics. A number of studies have shown that MQL machining can show satisfactory performance in practical machining operations. However, there has been few investigation of MQL grinding of special alloys like titanium alloys and the cutting fluids to be used in MQL grinding of these alloys. In this study, vegetable and synthetic esters oil are compared on the basis of the surface quality properties that would be suitable for MQL applications. The cutting performance of fluids is also evaluated using conventional wet (fluid) grinding of Ti–6Al–4V. As a result, synthetic ester oil is found to be optimal cutting fluids for MQL grinding of Ti–6Al–4V.     

Ductile fracture locus of Ti–6Al–4V titanium alloy

The simulation of ductile fracture in real components is becoming a strategic issue in numerical simulations. Numerical simulations of crashes, forming processes, impacts and fractures are reliable only if carried out with an accurate material calibration. The topics involved in this kind of simulation require a complete calibration of both the true stress–strain curve and the failure. The focus of this work is the accurate calibration of the constitutive relations of the titanium alloy Ti–6Al–4V. The approach proposed is based on different experimental tests supported by numerical simulations performed by means of detailed FE models. The Bao–Wierzbicki ductile failure criterion is calibrated using a total of 11 specimens. These specimens are tested on a multiaxial test machine to investigate the failure at different stress triaxialities. Furthermore, the sensitivity to the mesh size and the assessment of the calibration accuracy are analysed in detail on different components in order to verify the geometry transferability.     

Chemistry enhanced shear thickening polishing of Ti–6Al–4V

To obtain the great surface quality of Ti–6Al–4V and achieve high efficiency in the polishing process, the chemistry enhanced shear thickening polishing (C-STP) was proposed, and the polishing performance of different pH slurry was studied. The results show that the material removal rate gradually increases as the pH value decreases from 10 to 1, and the best surface quality is obtained at pH 2. The corrosion current density and potential were measured by potentiodynamic polarization under three typical pH values. It is confirmed that the most massive corrosion rate presents at pH 2, and the passive film is most susceptible to be produced at pH 10. The reaction resistance was measured by electrochemical impedance spectroscopy to clarify the polishing mechanism. Under acidic conditions, the chemical reaction product on the surface can be quickly removed by mechanical action of the abrasive. On the contrary, the passive film formed on the surface under the alkaline condition is difficult to be removed. The corrosion reaction products were determined by X-ray photoelectron, and the chemical reaction under acid-base environment was derived. MRR reached 107.3 nm/min under the selected process parameters, and the surface roughness (S_a) is reduced from 124 nm to 8.6 nm within 15 min.     

Tribological Behaviors of Carbon Fiber–Reinforced PEEK Sliding on Ion-Nitrided 2Cr13 Steel Lubricated with Tap Water

Selecting the proper material and surface treatment methods for elements is one of the essential problems when designing water hydraulic components due to the corrosiveness and poor lubricity of water. Experimental investigation was performed to study the tribological properties of ion-nitrided 2Cr13, a kind of martensitic stainless steel, sliding on carbon fiber–reinforced polyetheretherketone (CFRPEEK). The influence of factors such as sliding velocity, load, and lubrication condition were studied through experiments mainly under tap water lubrication. It was found that the friction coefficients are influenced by both the pressure and the sliding velocity. In contrast, the friction coefficients between quenched 2Cr13 and CFRPEEK are much higher. Compared to water lubrication, both the wear rate and friction coefficients increase in the case of dry friction. Wear mainly occurred on the CFRPEEK. By examining the worn surfaces of the specimens, it was found that adhesion was the main form of wear of the PEEK composite.     

Effects of sliding velocity on tribo-oxides and wear behavior of Ti–6Al–4V alloy

Dry sliding wear tests were performed for Ti–6Al–4V alloy on a pin-on-disc wear tester. The wear behavior of Ti–6Al–4V alloy at sliding velocities of 0.5–4 m/s was studied and the tribo-oxides and their function were explored. Ti–6Al–4V alloy presented a marked variation of wear rate as a function of velocity. With the rise and fall of wear rate, Ti–6Al–4V alloy underwent the transitions of wear mechanisms from the combination of delamination wear and oxidative wear at lower speeds to delamination wear at 2.68 m/s, and then to oxidative wear at 4 m/s. These phenomena were attributed to the appearance and disappearance of tribo-oxides. In spite of trace or a small amount, tribo-oxides would change the wear behavior, and even wear mechanism.     

Combined rough and finish machining of Ti–6Al–4V alloy by electrochemical mill-grinding

Abstract

This study proposes a combined method for the electrochemical mill-grinding of Ti–6Al–4V alloy to achieve a high material removal rate, high machining accuracy and good surface quality based on rough and finish machining. In the rough machining stage, a maximum feed rate of 2.7?mm min^?1 and a material removal rate of 248.3?mm³ min^?1 were achieved experimentally at a 10?mm cut depth using an abrasive tool with five rows of tool-sidewall outlet holes. In the finish machining stage, there were almost no overcuts or stray corrosions produced. The sidewall surface roughness and sidewall flatness were Ra = 1.06 and 76.8?μm after the finishing stage, which represent a 68% and 79.2% improvement compared with the rough machining stage, respectively. Finally, we fabricated a 1-mm-thick thin-walled structure using the combined machining operations, in which approximately 96% of the total material removal volume was performed at the rough machining stage.     

An experimental study of process variables in turning operations of Ti–6Al–4V and Cr–Co spherical prostheses

Ti–6Al–4V and Cr–Co alloys are extensively used in manufacturing prostheses due to their biocompatibility, high strength-to-weight ratio and high resistance to corrosion and wear. However, machining operations involving Ti–6Al–4V and Cr–Co alloys face a series of difficulties related to their low machinability which complicate the process of controlling the quality levels required in these parts. The main objective of this paper is to study the influence of cutting parameters, machine tool control accuracy and metrology procedures on surface roughness parameters and form errors in contouring operations of Ti–6Al–4V and Cr–Co workpieces. The machining performance of the two biocompatible materials is compared, focusing the study on part quality at low feed per revolution and the stochastic nature of plastic deformations at this regime. The results showed a better surface roughness control for Ti–6Al–4V, whereas for Cr–Co alloys, the performance presents high variability. In the case of form errors (sphericity), contouring errors and metrology procedures are important factors to be considered for quality assurance. In addition, the study analyses the correlation of the machining performance with different sensor signals acquired from a low cost non-intrusive multi-sensor, showing a high correlation of signals from acoustic emission sensors and accelerometers in the machining of spherical features on Ti–6Al–4V parts. The findings of this research work can be taken into account when designing prostheses components and planning their manufacturing processes.     

In-process prediction of surface roughness in turning of Ti–6Al–4V alloy using cutting parameters and vibration signals

In this work, an attempt has been made to use vibration signals for in-process prediction of surface roughness during turning of Ti–6Al–4V alloy. The investigation was carried out in two stages. In the first stage, only acceleration amplitude of tool vibrations in axial, radial and tangential directions were used to develop multiple regression models for prediction of surface roughness. The first and second order regression models thus developed were not found accurate enough (maximum percentage error close to 24%). In the second stage, initially a correlation analysis was performed to determine the degree of association of cutting speed, feed rate, and depth of cut and the acceleration amplitude of vibrations in axial, radial, and tangential directions with surface roughness. Subsequently, based on this analysis, feed rate and depth of cut were included as input parameters aside from the acceleration amplitude of vibrations in radial and tangential directions to develop a refined first order multiple regression model for surface roughness prediction. This model provided good prediction accuracy (maximum percentage error 7.45%) of surface roughness. Finally, an artificial neural network model was developed as it can be readily integrated into a computer integrated manufacturing environment.     

Failure mechanisms of a PCD tool in high-speed face milling of Ti–6Al–4V alloy

High-speed milling tests were carried out on Ti–6Al–4V titanium alloy with a polycrystalline diamond (PCD) tool. Tool wear morphologies were observed and examined with a digital microscope. The main tool failure mechanisms were discussed and analyzed utilizing scanning electron microscope, and the element distribution of the failed tool surface was detected using energy dispersive spectroscopy. Results showed that tool flank wear rate increased with the increase in cutting speed. The PCD tool is suitable for machining of Ti–6Al–4V titanium alloy with a cutting speed around 250 m/min. The PCD tool exhibited relatively serious chipping and spalling at cutting speed higher than 375 m/min, within further increasing of the cutting speed the flank wear and breakage increased greatly as a result of the enhanced thermal–mechanical impacts. In addition, the PCD tool could hardly work at cutting speed of 1,000 m/min due to the catastrophic fracture of the cutting edge and intense flank wear. There was evidence of workpiece material adhesion on the tool rake face and flank face in very close proximity to the cutting edge rather than on the chipped or flaked surface, which thereby leads to the accelerating flank wear. The failure mechanisms of PCD tool in high-speed wet milling of Ti–6Al–4V titanium alloy were mainly premature breakage and synergistic interaction among adhesive wear and abrasive wear.