Effect of Intermetallic Compound Phases on the Mechanical Properties of the Dissimilar Al/Cu Friction Stir Welded Joints

Types and distribution of intermetallic compound phases and their effects on the mechanical properties of dissimilar Al/Cu friction stir welded joints were investigated. Three different rotation speeds of 1000, 1200 and 1400 rpm were used with two welding speeds of 20 and 50 mm/min. The results show that the microstructures inside the stir zone were greatly affected by the rotation speed. Complex layered structures that containing intermetallic compound phases such as CuAl₂, Al₄Cu₉ were formed in the stir zone. Their amount found to be increased with increasing rotation speed. However, the increasing of the rotation speed slightly lowered the hardness of the stir zone. Many sharp hardness peaks in the stir zones were found as a result of the intermetallic compounds formed, and the highest peaks of 420 Hv were observed at a rotation speed of 1400 rpm. The joints ultimate tensile strength reached a maximum value of 105 MPa at the rotation speed of 1200 rpm and travel speed of 20 mm/min with the joint efficiency ranged between 88 and 96% of the aluminum base metal. At the travel speed of 50 mm/min, the maximum value of the ultimate tensile strength was 96 MPa at rotation speed of 1400 rpm with the joint efficiency ranged between 79 and 90%. The fracture surfaces of tensile test specimens showed no evidence for the effect of the brittle intermetallic compounds in the stir zones on the tensile strength of the joints.     

Effect of Tool Rotation Rate on Microstructure and Mechanical Behavior of Friction Stir Spot-Welded Al/Cu Composite

In this study, the friction stir spot welding of Al/Cu composite produced by accumulative roll-bonding process was performed using a triangular pin with no features. The influence of tool rotation rate on the microstructure, surface hardness, and tensile shear strength was examined. The results indicated that the weld made at lower tool rotation rate was not bonded because there was no intermixing between the upper and lower sheets. The maximum shear failure load increased with the increasing tool rotation rate, and reached a maximum value at 1400 rpm, which can be ascribed to the increasing area and effective length (d) of stir zone (SZ). The experimental observations showed the presence of the intermetallic compounds (Al₂Cu and AlCu₃) in the SZ. It was concluded that the intermetallic compounds, accompanied by the material crushing, increased the hardness of the SZ.     

Theoretical and experimental studies on fabrication of two-layer aluminum−copper pipe by friction stir additive manufacturing

Using a friction stir additive manufacturing (FSAM) process, the fabrication of a two-layer aluminum−copperpipe was studied experimentally and numerically. For this purpose, by presenting a 3D thermo-mechanical model in ABAQUS software, the temperature and strain distributions during the process were studied. The simulation results show that, although the rotational-to-traverse speed ratio with a good approximation can predict the heat input during welding, it is not a precise measure to predict the occurrence of defects in the weld cross-section. There is a good agreement between the predicted and experimental thermal results, and the maximum relative error is 4.1% in estimating the maximum temperature during welding. Due to heat and severe plastic deformationin the stir zone, the aluminum−copper intermetallic compounds (CuAl₂ and Cu₉Al₄) are formed. The maximum hardness in the stir zone is 301.4 HV_0.1in sample welded with an overlap of −0.5 mm.The ultimate tensile strength and elongation of the two-layer pipe fabricated by friction stir additive manufacturingare(319.52±2.31) MPa and 19.47%, respectively.     

异种搅拌摩擦焊制备铜铝合金双金属纳米复合材料

对纯铜与AA5754合金进行对接搅拌摩擦焊接.为了降低金属间化合物的有害影响,在搅拌摩擦焊(FSW)接头中添加纳米SiC强化颗粒.采用拉伸试验、显微硬度试验、扫描电镜和X射线衍射分析方法研究焊接接头的性能.结果显示,当焊接速度为50 mm/min、转速为1000 r/min时接头的性能最好.纳米SiC颗粒的存在使搅拌区...     

Effect of Shoulder Size on Weld Properties of Dissimilar Metal Friction Stir Welds

This article reports a research study that shows the effect of shoulder diameter size on the resulting weld properties of dissimilar friction stir welds between 5754 aluminum alloy (AA) and C11000 copper (Cu). Welds were produced using three different shoulder diameter tools: 15, 18, and 25?mm by varying the rotational speed between 600 and 1200?rpm and the traverse speed between 50 and 300?mm/min to achieve the best result. Each parameter combination was chosen to represent different heat input conditions (low, intermediates and high). The welds were characterized through microstructural evaluation, tensile testing, microhardness measurements, x-ray diffraction analysis, and electrical resistivity. Microstructural evaluation of the welds revealed that the welds produced consisted of all the friction stir welding (FSW) microstructure zones with organized flow lines comprising mixture layers of aluminum (Al) and copper (Cu) at the Stir Zones. The average Ultimate Tensile Strength (UTS) of the welds considered ranged from 178 to 208?MPa. Higher Vickers microhardness values were measured at the joint interfaces of all the welds because of the presence of intermetallic compounds in these regions. The x-ray diffraction analysis revealed the presence of Al₄Cu₉ and Al₂Cu intermetallics at the interfacial regions, and low electrical resistivities were obtained at the joint interfaces. An optimized parameter setting for FSW of Al and Cu was obtained at the weld produced at 950?rpm and 50?mm/min with the 18-mm shoulder diameter tool.     

Microstructural and mechanical properties of friction stir welded aluminum/copper lap joints

This paper focuses on the microstructural and mechanical properties of the friction stir welding (FSW) of 1060 aluminum alloy to a commercially pure copper. A number of FSW experiments were carried out to obtain the optimum mechanical properties by adjusting the rotational speed and welding speed in the range of 750–1500 rpm and 30–375 mm/min, respectively. Various microstructures with different morphologies and properties were observed in the stir zone. The results indicated that Al₄Cu₉, AlCu and Al₂Cu are the main intermetallic compounds formed in the interfacial region. The effect of formation of hard and brittle intermetallic phase at the interface of the joints on the shear strength of the joint is discussed.     

7075铝合金与H68黄铜的搅拌摩擦焊组织分析

采用金相显微镜对7075铝合金与H68黄铜异种材料搅拌摩擦焊接头组织进行观察、采用X射线衍射仪（XRD）对焊接接头中相结构进行分析,并采用显微硬度计对焊接接头硬度分布进行测试.结果表明,搅拌针的旋转频率为1 100 r/min,焊接速度为80 mm/min时,焊接接头未形成金属间化合物,焊核区晶粒细化,且显微硬度值增加...     

Investigation of microstructure and mechanical properties of friction stir lap jointed Monel 400 and Inconel 600

This study was conducted to investigate the microstructure and mechanical properties of friction stir lap joints. Monel 400 and Inconel 600 were selected as the experimental materials, and friction stir welding was carried out at a tool rotation speed of 200 rpm and welding speed of 100 mm/min. The application of friction stir welding to Monel 400 effectively reduced the grain size in the stir zone; the average grain size of Monel 400 was reduced from 11.9 μm in the base material to 4.2 μm in the stir zone, which resulted in an improvement in the mechanical properties of the stir zone. The joint interface between Monel 400 and Inconel 600 showed a relatively sound weld without grooves or cracks, and only a small amount of voids with a size of 0.5 μm; however, no intermetallic compounds were observed in the lap jointed interface. Moreover, the hook on the advancing side of Monel 400 was formed from Inconel 600, which contributed to maintenance of the tensile strength. The evolution of microstructures and mechanical properties of friction stir lap jointed Monel 400 and Inconel 600 are also discussed herein.     

Influence of tool pin design on properties of dissimilar copper to aluminum friction stir welding

Dissimilar friction stir welding (FSW) of copper and aluminum was investigated by nine different tool designs, while the rest of the process parameters were kept constant. Mechanical and metallurgical tests such as macrostructure, microstructure, tensile test, hardness, scanning electron microscope and electron X-ray spectrographs were performed to assess the properties of dissimilar joints. The results exhibited that, the maximum joint strength was achieved by the tool of cylindrical pin profile having 8 mm pin diameter. Besides, the fragmental defects increased as the number of polygonal edges decreased, hence the polygonal pin profiles were unsuitable for dissimilar FSW butt joints. Furthermore, the tensile strength increased as the number of polygonal edges increased. Stir zone of polygonal pin profiles was hard and brittle relative to cylindrical tool pin profiles for same shoulder surface. Maximum hardness of HV 283 was obtained at weld made by the polygonal square pin profile. The hard and brittle intermetallic compounds (IMCs) were prominently presented in the stir zone. Phases of IMCs such as CuAl, CuAl₂, Cu₃Al and Cu₉Al₄ were presented in the stir zone of dissimilar Cu–Al joints.     

6063铝合金双轴肩搅拌摩擦焊接头组织性能研究

进行了3 mm厚6063-T4铝合金双轴肩搅拌摩擦焊接。结果表明,当搅拌头转速为600 r/min,焊速在100~300 mm/min的范围内,可获得表面成形美观、内部无缺陷的优质接头。在接头搅拌区内,上、中、下各层硬度分布较为均匀,在热机影响区及热影响区内,上、下层硬度值高于中间层。热机影响区靠近搅拌区的位置以及热机影响区与热影响区的交界处为接头的两个薄弱位置。随着焊接速度的增加,接头各区域硬度值以及抗拉强度有着先增大后减小的趋势,所得最优接头抗拉强度为174 MPa,达到母材的87%,断裂位置位于热影响区。     

旋转速度对镁/铜异种金属搅拌摩擦焊接头成形及拉伸性能的影响

保持95 mm/min焊接速度不变的条件下,通过改变旋转速度研究其对镁/铜异种金属搅拌摩擦焊接头成形和力学性能的影响。结果表明:采用750 r/min搅拌头旋转速度焊接时,焊缝表面出现起皮现象;焊核区底部形成明显的隧道槽缺陷。适当增加搅拌头旋转速度至950 r/min时,焊缝表面变得更光滑;混合区尺寸增大;内部隧道槽缺陷消失;该混合区主要由被搅碎的Mg、Cu合金和少量新生成的Mg₂Cu金属间化合物组成;接头的抗拉性能最好,抗拉强度达81.7 MPa;但是,继续增大搅拌头旋转速度至1180 r/min时,不利于接头成形,混合区底部有细小的孔洞缺陷产生。     

转速对6061铝合金/纯铜异种金属搅拌摩擦焊接头组织与性能的影响

采用搅拌摩擦焊技术对4 mm厚6061-T6铝合金和纯铜进行连接,研究转速对铝铜异种金属接头组织与力学性能的影响。结果表明,当焊接速度为30 mm/min、搅拌头转速在1 200~1 800 r/min的范围内,可以获得表面成形良好、无缺陷的铝铜异种金属接头。大量破碎的铜被搅入焊核区,形成了组织结构复杂的区域。通过EDS和XRD分析,在焊核区内发现了Al_2Cu、Al_4Cu_9和Al Cu金属间化合物。在界面处,铝和铜发生相互扩散形成金属间化合物层,随着转速的提高,化合物层逐渐变厚。由于晶粒细化、固溶强化作用以及金属间化合物的生成,异种接头的焊核区平均显微硬度值高于铝铜两侧平均硬度,并且在焊核区出现硬度峰值点。随着转速的增加,接头抗拉强度呈现先增大后减小的趋势,所得最优接头抗拉强度为183 MPa,达到铜母材的71.8%,断裂位置位于铝侧热影响区,断裂方式为韧性断裂。     

Effect of Temperature on Microstructure and Fracture Mechanisms in Friction Stir Welded Al6061 Joints

Aluminum and its alloys are widely used in different industries due to such attractive properties as adequate strength, ductility, and low density. It is desirable to characterize welds of aluminum alloys obtained using “friction stir welding” at high temperatures. Al-to-Al (both 6061-T6) butt joints are produced by friction stir welding at tool rotation speed of 1600 rpm and four levels of tool advancing speeds: 250, 500, 750, and 1000 mm/min. Microstructural properties of the different welds are investigated. Observed are noticeable differences in microstructure characteristics between the various weld zones. Mechanical properties of these welded joints are characterized under tensile tests at temperatures of 25, 100, 200, and 300 °C, at a constant strain rate of 10^?3/s. The optimum microstructural and mechanical properties were obtained for the samples FS welded with 1600 rpm tool rotation speed at 1000 mm/min tool advancing speed. The studied welds exhibited yield strength, ultimate tensile strength, and strain to failure with values inferior of those of the base material. Observations of postmortem samples revealed that in the temperature range of 25-200 °C the locus of failure originates at the region between the thermo-mechanically affected zone and the heat-affected zones. However, at higher temperatures (300 °C), the failure occurs in the stir zone. A change in the crack initiation mechanism with temperature is suggested to explain this observation.     

Influence of Processing Parameters on Induced Energy, Mechanical and Corrosion Properties of FSW Butt Joint of 7475 AA

Friction stir welding (FSW), a promising solid state joining process invented at TWI in 1991, was used to join 9?mm thick 7475 aluminum alloy which is considered essentially unweldable by fusion processes. In the present work, the process parameters such as tool rotational speed were varied from 300 to 1000?rpm for a travel speed of 50?mm/min and the influence of process parameters in terms of energy input on microstructure, hardness, tensile strength, and the corrosion property of 7475 aluminum joints was evaluated and analyzed. The maximum tensile strength of FSW joints was obtained at rotational speed of 400?rpm and traverse speed of 50?mm/min (59.2?kJ) which attributed maximum stirred zone area and maximum hardness. The maximum corrosion resistance properties of weld in 3.5% NaCl solution, however, were obtained at rotational speed of 1000?rpm and traverse speed of 50?mm/min. Furthermore, for a given weld, stirred zone showed improved corrosion properties than TMAZ.     

基于CuSi3焊丝的激光熔钎焊钢/铝异种金属工艺分析

采用直径1.6 mm的CuSi3焊丝对钢/铝异种金属进行激光填丝熔钎焊.使用光学显微镜观察了焊缝宏观成形,利用SEM,EDS,XRD分析了接头微观组织,通过原位纳米压痕仪和拉伸试验机测试了接头力学性能.结果表明,采用CuSi3焊丝实现了6061铝合金和镀锌板的激光搭接熔钎焊,优化了工艺参数,获得了成形良好的焊缝.焊缝呈现三个特征区:钢侧界面区、焊缝中心区和铜焊丝/铝过渡区.进一步研究表明,铜焊丝/铝过渡区组织包含Cu₉Al₄和CuAl₂金属间化合物,呈现带状、粗大骨架状、细小骨架状夹杂层片状和树枝状四种形貌.铜焊丝/铝过渡区硬度远高于相邻区域,粗大骨架状区域硬度最高达到9.97 GPa,拉伸断裂于粗大骨架状区域,断口呈现脆性断裂.     

Microstructural characterization and mechanical properties of aluminum 6061-T6 plates welded with copper insert plate (Al/Cu/Al) using friction stir welding

Friction stir welding was used to join two aluminum 6061-T6 plates with an insert of a pure copper plate (Al/Cu/Al), and then the influence of the copper insert on the joint performance was studied. The dissimilar welding results were also compared with AA 6061 friction stir welds produced without copper insert (Al/Al). Optical and scanning electron microscopes were used for the microstructural observations of the welded samples. X-ray diffraction analysis was used to analyze phase component of the Al/Cu/Al specimen. A defect-free joint was observed for the Al/Cu/Al joint at a rotational speed of 950 r/min and a welding speed of 50 mm/min. Microstructural observation of the weld nugget zone (WNZ) demonstrates the formation of composite-like structure which promotes metallurgical bonding of aluminum and copper. XRD results show the formation of intermetallic compounds (IMCs), such as Al₄Cu₉ and Al₂Cu. Furthermore, it was observed that the hardness of the weld with the Cu insert plate is higher than that of other samples due to more dislocation density and a distinct rise in hardness values was observed due to the presence of IMCs. The ultimate tensile strength of the joint with copper insert plate is higher than that of the other sample due to the strong metallurgical bonding between Al and Cu.     

搅拌摩擦焊接工艺参数对AA6061-B4C焊接接头抗拉强度的影响（英文）

搅拌摩擦焊(FSW)是一种固态连接技术,可用来连接高强度铝合金及多种陶瓷颗粒增强金属基复合材料(MMCs)。搅拌摩擦焊获得的陶瓷增强金属基复合材料焊缝优良,在增强体与基体间没有发生有害反应。对搅拌摩擦焊接工艺参数对AA6061-B4C焊接接头抗拉强度的影响进行研究。采用4因素5水平的中心复合设计来控制实验的次数。构建一数学模型来分析搅拌摩擦焊工艺参数对接头抗拉强度的影响。结果表明,在旋转速度1000r/min、焊接速度1.3mm/s、轴向力10kN、增强相含量12%的条件下,搅拌摩擦焊得到的焊接接头的抗拉强度最大。根据构建的模型采用广义简约梯度算法进行优化以得到最大的抗拉强度。金相分析表明,在焊接接头中出现了多种区域,如焊合区、热力影响区和热影响区。在焊合区观察到大量的被细化的铝基体晶粒以及粒径明显减小的B4C颗粒。在热力影响区出现塑性变形、热影响和被拉长的铝晶粒。     

Dissimilar Joining of Pure Copper to Aluminum Alloy via Friction Stir Welding

In this study, the dissimilar friction stir welding(FSW) butt joints between aluminum alloy 5754-H114 and commercially pure copper were investigated. The thickness of welded plates was 4 mm and the aluminum plate was placed on the advancing side. In order to obtain a suitable flow and a better material mixing, a 1-mm offset was considered for the aluminum plate, toward the butt centerline. For investigating the microstructure and mechanical properties of FSWed joints, optical microscopy and mechanical tests(i.e., uniaxial tensile test and microhardness) were used, respectively.Furthermore, the analysis of intermetallic compounds and fracture surface was examined by scanning electron microscopy and X-ray diffraction. The effect of heat generation on the mechanical properties and microstructure of the FSWed joints was investigated. The results showed that there is an optimum amount of heat input. The intermetallic compounds formed in FSWed joints were Al4Cu9 and Al2Cu. The best results were found in joints with 1000 rpm rotational speed and100 mm/min travel speed. The tensile strength was found as 219 MPa, which reached 84% of the aluminum base strength.Moreover, maximum value of the microhardness of the stir zone(SZ) was attained as about 120 HV, which was greatly depended on the grain size, intermetallic compounds and copper pieces in SZ.     

Microstructure and mechanical properties of friction stir weld of dissimilar AZ31-O magnesium alloy to 6061-T6 aluminum alloy

Dissimilar friction stir welding between AZ31-O Mg and 6061-T6 Al alloys was investigated. 3 mm thick plates of aluminum and magnesium were used. Friction stir welding operations were performed at different rotation and travel speeds. The rotation speeds varied from 600 to 1400 r/min, and the travel speed varied from 20 to 60 mm/min. Defect-free weld was obtained with a rotation speed of 1000 r/min and travel speed of 40 mm/min. Metallographic studies showed that the grain size in the stir zone is much finer than that in the base metals. Complex flow pattern was formed in the stir zone. Microhardness measurement revealed an uneven distribution in the stir zone. Tensile test results indicated that the tensile strength of the welded specimen is about 76% of AZ31 Mg alloy and 60% of the 6061 Al alloy in tensile strength. SEM fracture surface image of the welded specimen indicated that the welded specimen failed through brittle-mode fracture.     

镍中间层对铝/镁异种金属搅拌摩擦焊接头微观组织的影响

采用搅拌摩擦焊(friction stir welding, FSW),引入厚度为0.05 mm镍箔作为中间层,在焊接速度不变条件下,采用不同转速对厚度为4 mm的6061铝合金和AZ31镁合金进行平板对接,对接头进行系列微观组织表征及力学性能测试,探讨转速对接头中镍颗粒分布状态,金属间化合物(intermetallic compounds, IMCs)种类与分布及接头强度的影响规律. 研究结果表明:与未引入中间层接头相比,引入镍改变了铝/镁异种金属FSW接头焊核区(weld nugget zone, WNZ)中IMCs种类及分布,WNZ存在明显的镁合金与铝合金相间的带状组织,其上分布着絮状Al₁₂Mg₁₇、颗粒状Mg₂Ni、层状Al₃Mg₂及大小不一的镍箔颗粒;随着转速增加,镍箔颗粒分布愈加均匀,Al₃Mg₂数量相对减少,且脆性Al₃Mg₂由连续分布逐渐演变为断续分布;当转速为750 r/min时,接头抗拉强度达到最大值,与未引入中间层接头相比,引入镍中间层接头抗拉强度提高了56 MPa,达到镁合金的56.9%.