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对Fe74Al4Sn2P10C2B4Si4非晶磁粉芯退火温度进行了研究,发现采用60min的退火时间,随着退火温度的变化,磁粉芯电感及品质因数在不同温度阶段表现出各自的特性.从室温至300℃之间,磁粉芯性能随着温度的升高缓慢改善,在此区间磁粉芯磁导率提高约47%;当温度在300~400℃之间,磁粉芯性能随着退火温度的升高显著改善,在此区间磁粉芯磁导率提高76%;当退火温度在400~440℃之间,磁粉芯磁导率及1MHz以下品质因数达到最大值;当退火温度接近初始晶化温度468℃时,磁粉芯在1MHz以上具有较好的综合性能. 相似文献
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对Fe74A14Sn2P10C2B4Si。非晶磁粉芯退火温度进行了研究,发现采用60min的退火时间,随着退火温度的变化,磁粉芯电感及品质因数在不同温度阶段表现出各自的特性。从室温至300℃之间,磁粉芯件能随着温度的升高缓慢改善,在此区间磁粉芯磁导串提高约47%;当温度在300~400℃之间,磁粉芯性能随着遐火温度的升高显著改善,在此区间磁粉芯磁导率提高76%;当退火温度在400~44012之间,磁粉芯磁导率及1M比以下品质因数达到最大值;当退火温度接近初始品化温度468℃时,磁粉芯住1MHz以上具有较好的综合性能。 相似文献
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采用高压水雾化方法制备了成分为(Fe0.76Si0.09B0.10P0.05)98C2的非晶粉末,由该成分非晶粉末制备出的磁粉芯具有较高的抗直流偏置性能及优异的损耗特性.研究了制备工艺对样品磁性能的影响.研究结果表明,非晶磁粉芯压制后的去应力退火处理能够有效的提高磁导率和降低损耗,过高的热处理温度会使非晶粉末晶化,导致涡流损耗急剧升高,恶化磁性能,最佳的退火温度为693K,绝缘包覆是制备高性能磁粉芯的必备工艺,通过最优化工艺制备的磁粉芯,其损耗为Pcv =320 kW/m3(f=100 kHz,Bm=0.1 T),抗直流偏置性能为:在H=100 Oe(1 Oe=7.9578×10A/m)外加磁场下,磁导率μa=60的磁粉芯样品对应电感下降为原感值的60%.通过与同规格其他类型磁粉芯的对比,发现FeSiBPC非晶磁粉芯具有极低的损耗及优异的高频磁性能. 相似文献
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利用单辊法制备了Fe74 Al4Sn2M2P10Si4B4(M为Nb、Mo、V)、Fe74 Al4SnzMo2P8Si4B4C2和Fe75Al4Sn2Mo2Nd1P8Si4B4非晶合金薄带,并测试了该非晶合金系的差示扫描量热曲线和动、静态软磁性能.结果表明,Fe74Al4Sn2NbzP10Si4B4非晶合金具有相对较宽的超冷液相区,其△Tx=51.41 K;而Fe74Al4Sn2MozP10Si4B4非晶合金具有较好的软磁性能,其最大磁导率μm=53.5×104,μe(1 kHz)=7.02×104,损耗P1.1T/50Hz=0.096 W/kg;Fe74Al4Sn2Mo2P8Si4B4C2非晶合金具有宽的超冷液相区和良好的软磁性能,其超冷液相区的宽度△Tx=48.81 K,μm=23.3×104,P1 1T/50 Hz=0.153 W/kg;Fe75Al4SnzMozNd1P8Si4B4非晶合金具有很宽的超冷液相区,其△Tx=60.06 K. 相似文献
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通过水雾化法制备了Fe74Cr1Si9B10P4C2非晶合金粉末,该成分合金过冷液相区可达35 K,具有良好的大块非晶形成能力,粒径在100 μm左右的粉末依然为非晶态.同时该成分非晶合金还具有优异的软磁性能,其饱和磁感Bs可达1.3T,矫顽力Hc=4.6 A/m.通过对非晶粉末表面进行钝化绝缘处理可极大提高非晶磁粉芯的高频特性,粉芯磁导率在10 MHz左右依然保持稳定,同时磁心损耗也极大降低,在Bm=100 mT,f=100 kHz测试条件下,其损耗Pcv=592.9 kW/m3. 相似文献
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通过铝热反应熔化法制备纯纳米晶Fe3Al材料以及添加质量分数分别为10%Ni,10%Cr,10% Mn,15% Mo,5% Cu和10%Cu合金元素的6种块体纳米晶Fe3Al材料;对含10% Ni的纳米晶Fe3Al材料分别进行600 ℃、1000℃,8h的等温处理.采用质量损耗法测定不同纳米晶Fe3Al材料在质量分数为5% H2SO4溶液中的均匀腐蚀速率;并研究各纳米晶Fe3Al材料在1200℃空气中的高温氧化性能.结果表明:添加15%Mo和添加10%Cu的纳米晶Fe3Al材料较纯纳米晶Fe3Al材料抗腐蚀性能提高明显;含10% Ni的纳米晶Fe3Al材料经过600℃ 等温处理后的腐蚀速率略高于未等温处理的材料,而经1000℃等温处理后腐蚀速率明显下降;随着合金元素Ni、Mn、Cr、Cu的加入,纳米晶Fe3Al材料的氧化速度增大,抗氧化性能降低. 相似文献
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新型(Fe,Co)-Zr-RE-B非晶合金的热稳定性和磁性 总被引:1,自引:0,他引:1
利用旋铸技术制备了一种新型的含稀土元素的铁基非晶合金。研究了Nd含量对Fe70Co8Zr7-xNdxB15(x=0~6%原子数分数)合金的非晶形成能力、热稳定性和磁性能的影响。当该合金系的Nd含量在0~6%(原子数分数)变化时,其饱和磁感应强度(Js)在1.10T~1.37T范围内变化,矫顽力(Hc)在2.28A/m~8.15A/m范围内变化。Js随Nd含量的增加而增加,当Nd含量为2%和3%时,其Hc值均在3A/m以下,且在Nd含量为2%时,具有最高的非晶形成能力(glassformationability简称GFA)即大的ΔTx(达61K);同时又有良好的软磁性能,其Js和Hc值分别为1.25T和2.28A/m。经对比得出,Fe70Co8Zr5RE2B15(RE=Ce、Pr、Gd和Tb)合金与Fe70Co8Zr5Nd2B15具有相近的非晶形成能力和磁性能。 相似文献
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Magnetic Properties of FeSiBC Amorphous Alloy Powder Cores Using Mechanical-crushed Powder 总被引:1,自引:0,他引:1
The FeSiBC amorphous powder cores were fabricated using powders of the FeSiBC amorphous ribbons which were mechanically crushed for a short time, and the relationship between magnetic properties and powder particle sizes was evaluated. The saturation magnetization Bs of the amorphous Fe82Si2B15C1 alloy was 1.62 T, which provided a superior dc-bias property for the powder cores. Meanwhile, a stable permeability up to high frequency range over 10 MHz and the low core loss of 400 kW/ma at f=50 kHz and Bm =0.1 T were obtained. These excellent high-frequency magnetic properties of the FeSiBC amorphous powder cores could be attributed to the effective electrical insulation between the FeSiBC amorphous powders made by mechanical crushing. 相似文献
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Tarek Bachaga Rakia Daly Lusia Escoda Joan Josep Suñol Mohamed Khitouni 《Metallurgical and Materials Transactions A》2013,44(10):4718-4724
An amorphous Al50(Fe2B)30Nb20 powder mixture was prepared by mechanical alloying in a high-energy planetary ball-mill under argon atmosphere. Morphologic, microstructural, and structural changes during the milling process were followed by scanning electron microscopy and X-ray diffraction. Rietveld analysis of X-ray diffraction patterns was used to follow the solid-state amorphization transformation during the milling process of the prepared powder. The reaction between elemental Al, Fe2B, and Nb powders leads to the formation of the Al(Fe,B) and Al(Fe,Nb,B) solid solutions after 4 and 6 hours of milling, respectively. An amorphous structure is achieved after 20 of milling. These amorphous powders are crystallized on further milling time (36 hours). The observation by scanning electron microscope shows a phenomenon of fracturing followed by compaction of the powder particles. 相似文献
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通过实验研究了Nd2Fe14B/Fe3B双相纳米复合磁粉分别与几种不同性能的磁粉复合成粘结磁体后磁性能的变化。通过对复合磁体的理论分析得知,由Nd2Fe14B/Fe3B与RE2Fe14B或铁氧体磁粉复合成的粘结磁体中,成分间并未发生化学反应。以Nd2Fe14B/Fe3B铁氧体复合粘结磁体为例,根据理论分析推出的剩磁Br-成分含量关系曲线与实际曲线吻合得很好,表明剩磁与成分含量间存在着近似的线性关系,从而可通过数学手段建立磁性能参数与成分含量的函数关系式,用于简化混粉工艺。另外,添加铁氧体可对该复合磁体较差的热稳定性起到补偿作用,并减少了磁不可逆损失。 相似文献
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Melt-spun Nd8Fe78B6Co4 magnetic powders and their bonded magnets were prepared with the optimization of compositions and preparation techniques. The microstructure change of alloy NdFeB and the relation between microstructure and heat-treatment were studied. The heat-treatment temperature is 200~700 ℃. The as-cast structure of the alloy is typically amorphous. Different melt-spun speed and different heat treatment could result in different magnetic properties of NdFeB magnets. Magnetic properties of NdFeB increase with the addition of element Co. The magnetic properties of magnet alloy get the best when the melt-spun speed reaches 23~26 m·s-1, heat treatment temperature is 690 ℃ and time is 30 min. 相似文献
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Junji Saida Akihisa Inoue Tsuyoshi Masumoto 《Metallurgical and Materials Transactions A》1991,22(9):2125-2132
Amorphous ultrafine powders in (Fe, Co, Ni)-B binary systems were prepared in different reduction conditions of metal ions
in an aqueous solution by use of KBH4, with the aim of clarifying the effect of reaction conditions on the composition, thermal stability, and magnetic properties
of the resultant amorphous powders. As the mol ratio of KBH4 to metal ions decreases, the structure of the ultrafine powders changes from amorphous to crystalline phase. The morphology
of these powders is in a nearly spherical shape with a particle size of about 20 nm for the amorphous phase and changes to
the chain-like or net-like shape for the crystalline phase. The B content in the Fe-B amorphous powder decreases with a decrease
of the ratio of KBH4 to metal ions, and the powder size decreases with an increase of the reduction temperature. 相似文献
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