Fluorescence decay characteristic of Tm-doped YAG crystal fiber for sensor applications, investigated from room temperature to 1400/spl deg/C

An yttrium aluminum garnet (YAG) crystal fiber with a thulium-doped end tip was specially grown by means of the laser heated pedestal growth approach and designed to be incorporated in a fiber-optic temperature probe. The fluorescence decay characteristics of the crystal fiber, including the temperature dependence of both the fluorescence lifetime and intensity, were comprehensively investigated. Experimental results indicated that the crystal fiber showed a monotonic relationship between the fluorescence lifetime and temperature with an average lifetime sensitivity of 3 /spl mu/s /spl deg/C over a wide temperature range, taking measurement from room temperature to 1200/spl deg/C. Good stability (up to 1400/spl deg/C) was observed with high repeatability of the fluorescence lifetime during the annealing process carried out on the fiber over this temperature range. The fiber was found to be an excellent candidate material to be used as a fluorescence decay-based fiber thermometer probe and the results are presented on its performance.     

Strain and temperature sensors using multimode optical fiber Bragg gratings and correlation signal processing

Multimode fiber optic Bragg grating sensors for strain and temperature measurements using correlation signal processing methods have been developed. Two multimode Bragg grating sensors were fabricated in 62/125 /spl mu/m graded-index silica multimode fiber; the first sensor was produced by the holographic method and the second sensor by the phase mask technique. The sensors have signal reflectivity of approximately 35% at peak wavelengths of 835 nm and 859 nm, respectively. Strain testing of both sensors has been done from 0 to 1000 /spl mu//spl epsiv/ and the temperature testing from -40 to 80/spl deg/C. Strain and temperature sensitivity values are 0.55 pm//spl mu//spl epsi/ and 6 pm//spl deg/C, respectively. The sensors are being applied in a power-by-light hydraulic valve monitoring system.     

Harsh environments minimally invasive optical sensor using free-space targeted single-crystal silicon carbide

To the best of our knowledge, for the first time, a single-crystal silicon carbide (SiC)-based minimally invasive smart optical sensor suited for harsh environments has been designed and demonstrated. The novel sensor design is based on an agile wavelength source, instantaneous single-wavelength strong two-beam interferometry, full optical power cycle data acquisition, free-space targeted laser beams, multiple single-crystal-thick SiC optical front-end chips, and multiwavelength signal processing for unambiguous temperature measurements to form a fast and distributed smart optical sensor system. Experiments conducted using a 1550-nm eye-safe band-tunable laser and a 300-/spl mu/m coating-free thick SiC chip demonstrate temperature sensing from room temperature to 1000/spl deg/C with an estimated average 1.3/spl deg/C resolution. Applications for the proposed sensor include use in fossil fuel-based power systems, aerospace/aircraft systems, satellite systems, deep-space exploration systems, and drilling and oil mining industries.     

CMOS monolithic metal-oxide sensor system comprising a microhotplate and associated circuitry

A gas sensor system fabricated in industrial CMOS technology is presented, which includes, for the first time, a microhotplate and the necessary driving and control circuitry on a single chip. Post-complementary-metal-oxide-semiconductor (CMOS) fabrication steps, such as micromachining of the membrane structure, the deposition of noble metal on the electrodes, and the processing of the sensitive metal-oxide layer, have been developed to be fully compatible with the industrial CMOS process. Temperatures up to 350/spl deg/C were reached on the hotplates using a low-voltage power supply (5 V). A symmetric hotplate design with a temperature homogeneity of better than 2% in the heated area was realized. The integrated temperature controller regulates the membrane temperature with a resolution of /spl plusmn/0.3/spl deg/C in the tracking mode. The temperature increase on the bulk chip owing to heat transfer through the membrane is less than 2% of the respective membrane operation temperature (6/spl deg/C at 350/spl deg/C membrane temperature). The gas sensing performance of the sensor was assessed by test measurements with carbon monoxide (CO). The gas tests evidenced a limit of detection of less than 5 ppm CO.     

Capacitive sensor for active tip clearance control in a palm-sized gas turbine generator

The efficiency of a gas turbine has an inverse relationship to the clearance between the rotor blades and the casing. Recent efforts in miniaturization of micro gas turbine engines have created a new challenge in blade tip clearance measurement. This paper describes the development of a capacitive tip clearance measurement system, based on a synchronous detection of a phase-modulated signal, for a palm-sized gas turbine engine with an integral ceramic rotor piece. A surface modification of the ceramic compressor and rotor with conductive coating is utilized to create a novel configuration of a tip clearance probe. The probe capacitance varies by approximately 120 fF for a 100-/spl mu/m blade displacement. Periodic autocalibration is used to reduce the effects of temperature drift on the sensor output. The remaining measurement error drift of 1.5 fF//spl deg/C was caused by the temperature drift of the probe parasitic capacitor. The random uncertainty was between 1.9 and 6.9 /spl mu/m depending on the tip clearance gap.     

Simultaneous measurement of humidity and temperature by combining a reflective intensity-based optical fiber sensor and a fiber Bragg grating

A novel sensor capable of simultaneously measuring temperature and humidity has been fabricated and demonstrated using optical fiber waveguides. The sensor head is composed of a fiber Bragg grating and a low-finesse Fabry-Perot interferometric cavity. The Fabry-Perot cavity was fabricated using the electrostatic self-assembled monolayer process for the molecular-level deposition of materials of different thicknesses that form a humidity-sensitive coating on the end of the fiber, while the in-line Bragg grating fiber element is used to monitor temperature. Experimental results for a humidity range from 11% to 97% RH and for a temperature range from 10/spl deg/C to 85/spl deg/C are shown.     

Fiber-based UV laser-diode fluorescence sensor for commercial gasolines

We report on an optical fiber probe, coupled to a 404-nm laser diode, as a fluorescence sensor for monitoring of commercial gasolines. The principle of operation of the sensor is based on quantifying the intensity of the Stokes-shifted fluorescence from some of the heavier polycyclic aromatic hydrocarbons C/sub x/H/sub y/,(x,y) /spl ges/ (14,10) present in gasolines as minor constituents. The normalized efficiency of the optical fiber probe, as a function of its geometry, is calculated in the cases of single-fiber and parallel dual-fiber designs. The spatial and temporal resolutions achievable by the sensor are discussed as a function of design parameters The performance of the sensor is investigated experimentally for commercial gasolines in the liquid and gas phase. The optimal excitation wavelength for such sensors is investigated in the range of 350-400 nm. The linear sensitivity to vapor concentrations of retail gasoline fuel is demonstrated in the range of 4%-125% of combustion stoichiometry at 10 bar and 180/spl deg/C. Statistical processing of the data from the sensor allows distinction to be made between different forecourt gasoline suppliers, as well as fuel varieties (unleaded, low sulfur, etc.).     

Simple fiber-optic-based sensors for process monitoring: an application in wine quality control monitoring

The goal of this research was to develop a simple and economical fiber-optic sensor technology for agrifood process monitoring. Toward this end, two fiber-optic sensors were developed to be used in combination: a single reflection V-bend sensor and a single fiber air-gap probe. The former is designed to be sensitive toward refractive index and the latter towards absorption. Experiments indicate that the micromachined V-bend fiber refractometer is most sensitive when the bend angle is centered around 140 degrees, at which angle the sensor may resolve changes in refractive index as small as 0.00015. Additionally, the V-bend sensor was found to be non-responsive toward sample absorption even in extremely absorbing solutions. The air-gap design absorption sensor, most commonly used for measurements in highly colored media, was found to be slightly sensitive towards refractive index. When the two sensors are used together, the response of the absorption sensor may be corrected for. This sensor combination is able to provide accurate measurements in situations where Beer's law is not obeyed. Results are presented that show that the sensor pair was successfully used to monitor wine sugar content (Brix), and color density and hue, parameters related to the age of the wine.     

Ceramic temperature sensors for harsh environments

A ceramic thermocouple based on indium-tin-oxide (ITO) thin films is being developed to measure the surface temperature of gas turbine engine components employed in power and propulsion systems that operate at temperatures in excess of 1500/spl deg/C. By fabricating ITO elements with substantially different charge carrier concentrations, it was possible to construct a robust ceramic thermocouple. A thermoelectric power of 6.0 /spl mu/V//spl deg/C, over the temperature range 25-1250/spl deg/C, was realized for an unoptimized ITO ceramic thermocouple. The charge carrier concentration difference in the legs of the ITO thermocouple was established by r.f. sputtering in oxygen-rich and nitrogen-rich plasmas. SEM micrographs revealed that after high-temperature exposure, the surfaces of the nitrogen prepared ITO films exhibited a partially sintered microstructure with a contiguous network of ITO nanoparticles. Thermal cycling of ITO films in various oxygen partial pressures showed that the temperature coefficient of resistance was nearly independent of oxygen partial pressure at temperatures above 800/spl deg/C and eventually became independent of oxygen partial pressure after repeated thermal cycling below 800/spl deg/C. Based on these results, a versatile ceramic sensor system has been envisioned where a ceramic thermocouple and strain sensor can be combined to yield a multifunctional ceramic sensor array.     

High temperature circular position sensor based on a giant magnetoresistance nanogranular Ag/sub x/Co/sub 1-x/ alloy

A new circular position sensor based on giant magnetoresistances has been developed. The sensing film is an AgCo nanogranular thin film patterned in a circular Wheatstone bridge configuration. This alloy shows a high magnetoresistance (8%) at room temperature within the field generated by an NdFeB permanent magnet that provides a sensitivity of 440 /spl mu/V/V/(/spl deg/). The operational temperature range of this sensor is -40/spl deg/C/+120/spl deg/C, although the magnetic film tolerates higher temperatures up to 200/spl deg/C. These parameters and the contactless way of sensing make this device appropriate for automotive applications. The developed sensor presents excellent characteristics for life, since it is not sensitive to pollution; it is frictionless and does not present any type of electrical noise generated by contacts.     

Development of a new millimeter-wave integrated-circuit sensor for surface and subsurface sensing

A new millimeter-wave sensor employing the stepped-frequency radar technique has been developed using microwave and millimeter-wave integrated circuits and demonstrated for surface and subsurface sensing. The sensor is based on the coherent super-heterodyne scheme and operated from 29.72-37.7GHz. It has been used to profile the surface of a sample with range accuracy within /spl plusmn/0.1 cm. The sensor was also used to monitor continuously varying liquid levels in a tank and was able to detect the displacement of liquid level with less than /spl plusmn/0.1 cm error. The sensor successfully detected and located anti-personnel mines buried under sand with less than 1.8 and 0.2 cm of errors in horizontal and vertical directions, respectively.     

Temperature correction of radiometric and geometric models for an uncooled CCD camera in the near infrared

This paper presents radiometric and geometric models for both temperature and displacement noncontact measurements using an uncooled charge-coupled device (CCD) video camera. Such techniques ("one sensor-two measures") represent an interest in many industrial low cost applications and scientific domains. To benefit from both measurements, we have to use the camera's spectral response in the near infrared spectral band from 0.75 to 1.1 /spl mu/m. In this spectral band, the temperature variations of an uncooled CCD camera are taken into account in the radiometric and geometric models. By using physical models for CCD camera, we quantify detector's quantum efficiency, sensor noise and spatial resolution as a function of the wavelength and of the detector temperature. These models are confirmed by experimental results of calibration with a low cost uncooled camera based on a Sony detector and operating over the detector temperature range of -30 to -50/spl deg/.     

Fabrication and characterization of nano-sized SrTiO/sub 3/-based oxygen sensor for near room-temperature operation

Nano-sized SrTiO/sub 3/-based oxygen sensors were fabricated from synthesized SrTiO/sub 3/ and commercial SrTiO/sub 3/ using the high-energy ball milling and the thick-film screen-printing techniques. The particle sizes, microstructural properties, oxygen-sensing properties, and humidity effects of the synthesized nano-sized SrTiO/sub 3/-based oxygen sensors were characterized using X-ray diffraction (XRD), transmission electron microscope, scanning electron microscope (SEM), and gas sensing measurements. Experimental results showed that the particle size of the powders was milled down to be around 27 nm. The effect of different annealing temperatures (400/spl deg/C, 500/spl deg/C, 600/spl deg/C, 700/spl deg/C, and 800/spl deg/C) on the gas sensing properties of the synthesized SrTiO/sub 3/ sensor from nitrogen to 20% oxygen was characterized. The commercial SrTiO/sub 3/ devices annealed at 400/spl deg/C, both with 0-h and 120-h milling time, were used for comparison. The optimal relative resistance (R/sub nitrogen//R/sub 20%oxygen/) value of 6.35 is obtained for the synthesized SrTiO/sub 3/ sample annealed at 400/spl deg/C and operating at 40/spl deg/C. This operating temperature is much lower than that of conventional metal oxide semiconducting oxygen gas sensors (300/spl deg/C-500/spl deg/C) and SrTiO/sub 3/ oxygen gas sensors (>700/spl deg/C). The response and recovery times are 1.6 and 5 min, respectively. The detected range is 1-20% oxygen. The impedance of the synthesized SrTiO/sub 3/ sensor with annealing at 400/spl deg/C and operating at 40/spl deg/C (from 1 mHz to 10 MHz) in 20% oxygen ambient was found to be independent of the relative humidity (dry, 20% RH, 80% RH, near 100% RH).     

Chemical warfare agent detection using MEMS-compatible microsensor arrays

Microsensors have been fabricated consisting of TiO/sub 2/ and SnO/sub 2/ sensing films prepared by chemical vapor deposition (CVD) on microelectromechanical systems array platforms. Response measurements from these devices to the chemical warfare (CW) agents GA (tabun), GB (sarin), and HD (sulfur mustard) at concentrations between 5 nmol/mol (ppb) and 200 ppb in dry air, as well as to CW agent simulants CEES (chloroethyl ethyl sulfide) and DFP (diisopropyl fluorophosphate) between 250 and 3000 ppb, are reported. The microsensors exhibit excellent signal-to-noise and reproducibility. The temperature of each sensor element is independently controlled by embedded microheaters that drive both the CVD process (375/spl deg/C) and sensor operation at elevated temperatures (325/spl deg/C-475/spl deg/C). The concentration-dependent analyte response magnitude is sensitive to conditions under which the sensing films are grown. Sensor stability studies confirm little signal degradation during 14 h of operation. Use of pulsed (200 ms) temperature-programmed sensing over a broad temperature range (20/spl deg/C-480/spl deg/C) enhances analyte selectivity, since the resulting signal trace patterns contain primarily kinetic information that is unique for each agent tested.     

Extrinsic Fabry-Perot interferometry for noncontact temperature control of nanoliter-volume enzymatic reactions in glass microchips

Optical fiber extrinsic Fabry-Perot interferometry (EFPI) was investigated as a noncontact temperature sensor and utilized for regulating the temperature of small-volume solutions in microchips. Interference pattern analysis determined the optical path lengths (OPL) associated with reflections from various surfaces on or in the microchip, in particular, from gold sputtered on the bottom of a microchannel. Since OPL is directly proportional to refractive index, which is dependent on solution temperature, the EFPI sensor was capable of noncontact monitoring of solution temperature simply from alterations in the measured path length. Calibration of the sensor against a thermocouple was performed while heating the microchip in a noncontact manner with an IR lamp. The combination of EFPI temperature sensor, IR-mediated heating, and air cooling allowed a fully noncontact system for small-volume temperature control in microchip structures, and its utility was illustrated by optimal digestion of DNA by a temperature-dependent restriction endonuclease in 320 nL. The functionality and simplicity of the microchip EFPI temperature sensor was enhanced by replacing the prebonding sputtered gold with a tunable, chemically plated semireflective silver coating created in situ after chip fabrication. This provided an 8-fold improvement in the lowest detectable temperature change (deltaT = 0.1 degrees C), facilitated primarily by enhanced reflection from both the bottom and top surfaces of the microchannel. This approach for controlling micro- and nanoscale reactions--with heating, cooling, and temperature control being carried out in a completely noncontact fashion--provides an accurate and sensitive method for executing chemical and biochemical reactions in microchips.     

光子晶体光纤F-P干涉式高温传感器研究

本文提出一种用于高温测量的光子晶体光纤F-P干涉传感器,通过熔接机放电使无截止单模光子晶体光纤(ESM-PCF)一个端面完全塌陷,然后再将其与单模光纤(SMF-28e)熔接起来,最后按照设计长度切断ESM-PCF。由于在熔接点处ESM-PCF完全塌陷使其模场直径扩大,减小了与SMF-28e的模场失配损耗,并提高了熔接面的反射光强。这种方式制作简单,相对于以往的光子晶体光纤F-P干涉传感器具有更高的干涉光强度。实验结果表明,该传感器测量温度可达1100℃,温度灵敏度为29.4nm/℃,可以预见这种结构稳定、线性度好的全光纤传感器在机械、航空、冶金领域等具有一定的潜在应用价值。     

Fiber-optic temperature sensor based on interaction of temperature-dependent refractive index and absorption of germanium film

The interaction of a large temperature-dependent refractive index and a temperature-dependent absorption of semiconductor materials at 1550 nm can be used to build a very sensitive, film coated fiber-optic temperature probe. We developed a sensor model for the optical fiber-germanium film sensor. A temperature sensitivity of reflectivity change of 0.0012/°C, corresponding to 0.1°C considering a moderate signal processing system, over 100°C within the temperature regime of -20°C to 120°C, has been demonstrated by experimental tests of the novel sensor. The potential sensitivity and further applications of the sensor are discussed.     

Fiber-optic Sagnac interferometer for noncontact structural monitoring in power plant applications

The design of a noncontact fiber-optic sensor is described for the detection of acoustic emission for structural integrity monitoring in high-temperature power plant applications. The sensor is based on a Sagnac interferometer and produces an output proportional to target velocity, without the need for active phase stabilization. It is inherently insensitive to low-frequency perturbations of the instrument or the target and incorporates an environmentally insensitive downlead, which may be of arbitrary length. It is shown that the sensor is capable of meeting the specifications for structural integrity monitoring of high-temperature power plant components based on acoustic emission detection and has a velocity resolution of 50 nm s(-1) Hz(-1/2).     

Temperature correction to chemoresistive sensors in an e-NOSE-ANN system

The influence of the temperature coefficient of resistance in the chemoresistive response of inherently conductive polymer (ICP) sensors in the performance of an artificial neural network (ANN) e-natural olfactory sensor emulator (e-NOSE) system is evaluated. Temperature was found to strongly influence the response of the chemoresistors, even over modest ranges (ca. 2/spl deg/C). An e-NOSE array of eight ICP sensor elements, a relative humidity (RH/spl plusmn/0.1%) sensor, and a resistance temperature device (RTD/spl plusmn/0.1/spl deg/C) was tested at five different RH levels while the temperature was allowed to vary with the ambient. A temperature correction algorithm based on the temperature coefficient of resistance /spl beta/ for each material was independently and empirically determined then applied to the raw sensor data prior to input to the ANN. Conversely, uncorrected data was also passed to the ANN. The performance of the ANN was evaluated by determining the error found between the actual humidity versus the calculated humidity. The error obtained using raw input sensor data was found to be 10.5% and using temperature corrected data, 9.3%. This negligible difference demonstrates that the ANN was capable of adequately addressing the temperature dependence of the chemoresistive sensors once temperature was inclusively passed to the ANN.     

Analysis and design of a CMOS angular velocity- and direction-selective rotation sensor with a retinal Processing circuit

This paper implements and analyzes a CMOS angular velocity- and direction-selective rotation sensor with a retinal processing circuit. The proposed rotation sensor has a polar structure and is selective of the angular velocity and direction (clockwise and counterclockwise) of the rotation of images. The correlation-based algorithm is adopted and each pixel in the rotation sensor is correlated with the pixel that is 45/spl deg/ apart. The angular velocity selectivity is enhanced by placing more than one pixel between two correlated pixels. The angular velocity selectivity is related to both the number and the positions of the edges in an image. Detailed analysis characterizes angular velocity selectivity for different edges. An experimental chip consisting 104 pixels, which form five concentric circles, is fabricated. The single pixel has an area of 91/spl times/84/spl mu/m/sup 2/ and a fill factor of 20%, whereas the area of the chip is 1812/spl times/1825/spl mu/m/sup 2/. The experimental results concerning the fabricated chip successfully verified the analyzed characteristics of angular velocity and direction selectivity. They showed that the detectable angular velocity and range of illumination of this rotation sensor are from 2.5/spl times/10/sup -3/ /spl pi//s to 40 /spl pi//s and from 0.91 lux to 366 lux, respectively.