Expansion Behavior of a Binary‐Solid Liquid Fluidized Bed with Large Particle Size Difference

The overall expansion of two dissimilar solid particle species with over a tenfold difference in their size and substantial density difference is investigated here for different compositions of the fluidized bed. Contrary to the widely held notion that the total bed height would be the sum of the heights of the two segregated mono‐component beds, the actual bed heights were, in fact, found to be lower. This volume contraction is found to strongly depend upon the mixing behavior prevailing in the binary‐solid fluidized bed. At the complete mixing of the two solid species, the bed‐contraction versus liquid velocity profile shows a global maximum. As a result, the overall bulk density profiles are similarly affected. Moreover, it is found here that correlations meant for predicting the porosity of the packing of binary particle mixtures can be satisfactorily extended to binary‐solid fluidized beds where solid species differ significantly in size.     

Study of Flow Characteristics of Ultrafine CaCO3 Powders in a Spouted Bed

The flow behavior of gas and ultrafine powder in a spouted bed was numerically investigated by using a two‐fluid model coupled with a population balance equation (PBE). The aggregation process is controlled by the PBE, which is solved by the direct quadrature method of moments. The agglomerate diameter is calculated according to the change in particle number. The solid pressure and viscosity were modified for agglomerates on the basis of the kinetic theory of granular flow. Distributions of diameter, solids volume fraction, and velocity are obtained by the new model. The influence of cohesive intensity and gas velocity on the diameter distribution were analyzed. The spout diameter, a vital parameter for the design of spouted beds, was calculated and a calculation formula is proposed.     

振动流化床内双组分颗粒的混合与分离特性

在300 mm′300 mm′20 mm的二维振动流化床中,装入平均粒径2和4 mm的分子筛颗粒,在低于流化速度(u相似文献   

Behaviour of Cohesive Powders in a Powder‐Particle Spouted Bed

Behaviour of cohesive powders in a powder‐particle spouted Bed (PPSB) has been investigated under several operating variables and solids properties. The elutriation rate constant based on the hold‐up of fine powders in the bed decreased with a decrease in the size of fine powders, and with an increase in the size of coarse particles under a constant superficial gas velocity. This finding is quite different from the elutriation phenomena of particles more than 100 µm in size. Moreover, the mean residence time of fine powders increased with a decrease in the superficial gas velocity and the size of fine powders, and decreased with a decrease in the size of coarse particles.     

Solid Recycle Characteristics of Loop‐seals in a Circulating Fluidized Bed

Solid recycle characteristics through a conventional and a newly developed loop‐seal (0.08 m i.d.) system are determined in a circulating fluidized bed of FCC or silica sand particles. In the loop‐seal developed here, gas was injected downward tangentially to the wall of the loop‐seal to increase solids mass flux with stable flow. For conventional loop‐seal, solids mass fluxes increase linearly with increasing aeration rate but it reaches a maximum value. At the same aeration rate with different aeration locations (0.1 – 0.6 m) in a conventional loop‐seal, a maximum solids mass flux is seen at a height to diameter ratio of 2.5. For the newly developed loop‐seal, mass fluxes of FCC and sand particles are higher and more stable than in conventional loop‐seal at the same aeration rate. The solid mass fluxes obtained have been correlated with the aeration rate and Archimedes number.     

三相流化床间歇操作中颗粒的混合与离析行为

在直径41 mm、高1500 mm的间歇操作三相流化床中对双组分固体颗粒的轴向浓度分布、混合和离析行为进行了实验研究. 实验所用固体混合物为密度相近、直径不同的大孔吸附树脂(H-103)与橡胶球. 采用多个百叶窗式金属网及床层膨胀法测量颗粒固含率及流化床气含率沿床层轴向的变化情况,借用描述液-固两相流化床的沉降-分散模型描述气-液-固三相流化床,并采用了Fan等的离析速度与床层高呈线性关系的假定. 实验结果证明,沉降-分散模型可以用来描述气-液-固三相流化床中的固体浓度分布,Fan等的假设是成立的.     

Bubbling and Bed Expansion Behavior Under Vibration in a Gas‐Solid Fluidized Bed

The effect of vibration on the flow patterns and fluidization characteristics including the minimum fluidization velocity (u_mf), the void fraction (ϵ_mf) at u_mf and the bed expansion ratio were examined. The powders used were spherical glass beads and their diameters were 6, 20, 30, 60 and 100μm. For group A powders, the manner in which the vibration affects the bubble formation was examined from the bed expansion ratio and the index of n/4.65. The area of the homogeneous fluidization region was also observed. The homogeneous fluidization region was broadened at a certain vibration strength, where the value of n/4.65 was a minimum. The bubble formation was observed even for 20μm powder (group C), at large vibration strengths and at high gas velocities. Under such conditions, the bed expansion ratio increased suddenly due to bubble formation. The bubbles broke the irregular bed structure, including various properties of agglomerates. Although the channel breakage was dominant flow pattern for group C powders, the bubbles also played an important role in the improvement of the fluidization.     

Full‐Loop Simulation of Gas‐Solids Flow in a Pilot‐Scale Circulating Fluidized Bed

In order to study the system hydrodynamics in a circulating fluidized bed (CFB), a 3D full‐loop simulation was conducted for a pilot‐scale CFB. The Eulerian‐Eulerian two‐fluid model with the kinetic theory of granular theory helped to simulate the gas‐solids flow in the CFB. The system hydrodynamics including pressure balance, vectors of gas and solids, distribution of solids holdup, and instantaneous circulating rates were obtained to get a comprehensive understanding of the system. It was predicted that the main driving force was the pressure drop of the storage tank. The storage height and valve opening were critical operating factors to control the riser operation. The effects of operating conditions including solids circulating rates and superficial gas velocity on the hydrodynamics were investigated to provide guidance for the stable operation of the CFB system.     

南屯电厂220t／h循环流化床煤泥、煤矸石混烧锅炉的方案设计

介绍了南屯电厂220t/h循环流化床煤泥、煤矸石混烧锅炉的开发研究,锅炉设计特点及各项指标规范。     

Flow Characterization of a Three‐Phase Circulating Fluidized Bed Using an Ultrasonic Technique

The axial and radial distributions of solid and gas holdups were investigated in an air‐water‐glass bead circulating fluidized bed (GLSCFB) using a new ultrasonic technique, with a new method based on signal fluctuations. The cross‐sectional averaged gas and solid holdups measured at two axial positions appear to be similar at all studied operating conditions. The radial non‐uniformity decreases with increasing liquid velocity but does not change with an increasing solid circulating rate. The radial distribution of gas holdup was more uniform for 1.3 mm beads than for 433 µm glass beads.     

Effect of Volume Fraction of Material on Separation by Density Difference in a Liquid‐Fluidized Bed of Inert Particles

A liquid‐fluidized bed was used to separate a pure material from a mixture. A quantity of relatively large sized material was immersed in an inert‐particle fluidized bed and the behavior of materials was examined for different liquid velocities. In particular, the volume fraction of the material was varied and its effect on the separation characteristics was examined. The material floats on the inert‐particle fluidized bed when the density of the material is lower than the apparent density of the bed, regardless of the volume fraction of the material. The apparent density of the bed can be adjusted by changing the liquid velocity. The materials in the upper portion of the bed affect the properties of the bed below them, i.e., the void fraction decreases and the apparent density increases in the inert‐particle suspension when materials are present in the upper portion of the bed. Therefore, the materials float on the bed although the apparent density of the inert‐particle suspension obtained from the case without material is less than the density of the material at a relatively high volume fraction of material. This phenomenon occurs more easily for lighter and smaller materials. This means that small inert particles and low liquid velocities are the optimum operating conditions for the separation.     

Behavior of Pieces of Plastic Sheet in Solid‐Liquid Fluidized Bed with Stirring

A solid‐liquid fluidized bed of inert particles can be used to separate pure objects from a mixture. Pieces of plastic sheet were selected as the objects to be separated. To estimate the separation characteristics, the behavior of pieces of plastic sheet in the bed was examined experimentally. Slow stirring was used to improve the fluidization state of the bed. The object size and the volume ratio of objects to inert particles were varied. The use of stirring of the bed was effective in improving the fluidization state of the bed, and the objects, which sank in the bed without stirring, moved from the bottom to the upper portion of the bed at a certain liquid velocity. This liquid velocity increases with decreasing object size, and it also increases as the volume ratio of objects to inert particles in the bed increases. When the volume ratio of objects to inert particles is too high, the objects are distributed throughout the entire bed, regardless of the liquid velocity.     

Experimental Study on Flow Behavior in a Gas‐Solid Fluidized Bed for the Methanol‐to‐Olefins Process

A cold model experimental system is established to investigate the flow behavior in a gas‐solid fluidized bed for the methanol‐to‐olefins process catalyzed by SAPO‐34. The system comprises a gas distributor in a F 300 × 5000 mm acrylic column, double fiber optic probe system and a series of cyclones. The experiments are carried out under conditions of atmospheric pressure and room temperature with different superficial velocities (0.3930–0.7860 m s^–1) and different initial bed heights (600–1200 mm). The effects of radial distance, axial distance, superficial gas velocity, and initial bed height on the solid concentration and particle velocity in the bed are discussed. The time‐averaged solid concentration and rising particle velocity profiles under different conditions are obtained. The results show that an increase in the value of r/R or initial bed height results in an increase in the solid concentration but a decrease in the rising particle velocity in the dense phase area, while improvement of the superficial gas velocity has a negative influence on the solid concentration but results in an increase in the rising particle velocity.     

Studies on Regime Transition,Operating Range and System Stability in a Liquid‐Solid Circulating Fluidized Bed

In the present work, the variations in the solids circulation rate and solids holdup were analyzed to study the behavior of a liquid‐solid circulating fluidized‐bed (LSCFB) regime. The results confirm the existence of two regions in the regime of LSCFB. A new concept of critical liquid velocity, j_lc, is proposed in the present work for demarcation between region 1 and region 2, which is found to be a constant value of about 1.3 u_t for all particles considered. The operating range of the LSCFB regime is obtained for the various particles and a correlation is developed from the data to estimate the maximum total liquid velocity. The predicted maximum liquid velocity was compared with the experimental values and found to be in good agreement within ±9 %. The effects of total liquid velocity, particle size and density on the stable operating range are discussed. Analysis of the experimental results shows that stable operation prevails both in region 1 and region 2.     

Decolorization of RR‐120 Dye Using Ozone and Ozone/UV in a Semi‐Batch Reactor

Treatability of RR‐120 aqueous dye solutions using O₃ and O₃/UV was studied in a bench scale set‐up. Reduction in colour and chemical oxygen demand (COD) under various pH and initial dye concentrations were investigated. Pseudo first order reaction rate was satisfactorily used for kinetic interpretations in destruction of the dye. The results showed that decolorization with O₃ was faster at neutral pH values. While use of UV had a small effect on ozonation at low pH values, UV radiation had a considerable effect at pH values of 7 and above. It was found that ozone utilization efficiency of higher than 95% could be attained in the experimental set up.     

Prediction of the Behavior of a Liquid‐Fluidized Bed of Inert Particles Used for Separation by Density

A liquid‐fluidized bed of inert particles was used to separate a pure object from a mixture. One (binary solid‐liquid‐fluidized bed) or two (tertiary solid‐liquid‐fluidized bed) types of objects with relatively large‐sized particles were immersed in an inert‐particle bed, and the bed behavior was observed for different liquid velocities. The void fraction and apparent density of the inert‐particle suspension were predicted by considering the effect of the change in object position for different liquid velocities. The prediction method, which considers the change in the minimum fluidization velocity, accurately expressed the changes in the void fraction and the apparent density of the bed with the position of the objects in the bed. Using this method, the liquid velocity required to separate a certain kind of object from a mixture can be predicted.     

Agglomerate Sizes of Binary Nanoparticle Mixtures in a Vibro‐Fluidized Bed

Agglomerate size is one of the key factors influencing the fluidization behavior of nanoparticles. The effect of fluidization time, superficial gas velocity, and vibration frequency on agglomerate sizes for different binary mixtures of nanoparticles at the top of the bed was investigated in a vibrated fluidized bed (VFB). The agglomerate sizes decreased and fluidization quality was significantly enhanced owing to introduction of vibration energy. The Richardson‐Zaki equation combined with Stokes' law permitted the prediction of mean agglomerate sizes. Experimental and estimated results indicated that vibration led to a smaller agglomerate size. The mean predicted agglomerate sizes were in agreement with those determined experimentally in the VFB.     

Numerical Simulation of the Hydrodynamics of Gas/Solid Two‐Phase Flow in a Circulating Fluidized Bed with Different Inlet Configurations

The gas/solid flow characteristics in a circulating fluidized bed with two different inlet configurations were investigated by numerical simulation based on an Eulerian approach. In order to describe the interaction between the gas phase and the solid phase and the influence of the solid phase on the gas turbulence, a source term formulation with a more reasonable physical meaning was introduced. The simulation results were validated by the experimental data; then, the model was employed to examine the effect of the inlet configuration on the gas and solid feeding. The simulation results showed that, using the side feeding system, the distributions of solid flow and concentration were highly variable both over the column cross‐section and along the column height. However, such variations can be improved by using the elbow inlet system where the gas and solid are fed from the bottom.     

Enriched‐Air Gasification of Refuse‐Derived Fuel in a Fluidized Bed: Effect of Gasifying Conditions and Bed Materials

Enriched‐air gasification of refuse‐derived fuel (RDF) was carried out in a fluidized bed, investigating the effects of temperature, equivalence ratio (ER), oxygen percentage of enriched air (OP), and bed materials. For the bed material effect, calcined dolomite proved to be more effective for tar decomposition and resulted in higher CO and H₂ contents. In a bed of high‐alumina bauxite, an increased ER tended to cause a greater decrease in syngas quality. For both bed materials, a higher temperature and OP favored the production of combustible gas and led to higher cold gas efficiency. Increasing the ER resulted in higher gas yields and carbon conversion but lowered the concentration of the combustible component. The ash content of the char increased with temperature and OP, while the volatile and fixed carbon contents were decreased. The optimum conditions suggested in this study were an ER of 0.22 and an OP of 44.7 % at 750–800 °C in a bed of calcined dolomite.