共查询到18条相似文献,搜索用时 62 毫秒
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根据中草药浸提机制和扩散理论对飞天蜈蚣七多糖浸提的动力学进行初步研究。以Fick第二定律为基础,采用球形模型讨论液料比、提取时间、提取温度与飞天蜈蚣七中多糖浸出量之间的关系,从而建立提取过程中动力学模型,并由此推算出浸提多糖过程中的速率常数、活化能、相对萃余率、有效扩散系数等动力学参数。飞天蜈蚣七中多糖的浸出量随着温度的升高而增加、随着液料比的变化而变化、随着提取时间的增长而逐渐增加并最终趋于平衡;浸提多糖的相对萃余率符合指数模型;有效扩散系数也随着温度升高而增加并受到液料比的影响。研究得到的动力学模型可为飞天蜈蚣七多糖提取的工艺条件优化和深层次研究奠定理论基础。 相似文献
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人参皂苷的提取和精制工艺研究 总被引:2,自引:0,他引:2
以西洋参茎叶为原料,索氏提取法提取西洋参茎叶原料中人参皂苷,并采用高氯酸比色法,以人参皂苷标准品Re为对照品,分析西洋参茎和叶中人参皂苷的含量。结果表明,叶中人参皂苷的含量明显高于茎。故以叶为原料,研究不同的提取和精制工艺。结果表明:超声波提取人参皂苷提取率较水煎煮提取大。比较大孔树脂吸附和溶剂萃取两种不同精制工艺,正丁醇溶剂萃取精制得到的人参皂苷含量较大孔树脂吸附大,其人参皂苷提取率较大孔树脂吸附高,再经Al2O3脱色,得到西洋参叶人参皂苷含量均在90%以上。 相似文献
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酶法提取无患子皂苷的工艺研究 总被引:3,自引:0,他引:3
采用酶法提取无患子皂苷,研究了酶的类型对无患子皂苷提取的影响,并通过正交实验优化酶法提取工艺。结果表明,纤维素酶有助于无患子皂苷的提取,酶提法的较优工艺条件为:纤维素酶用量为无患子粉末质量的0.1%,酶提时间2.5 h,酶提温度50℃,pH值4.7。此时,无患子皂苷的提取率达到86.59%,比未加酶处理时提高了19.63%。 相似文献
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以西洋参茎叶为原料,索氏提取法提取西洋参茎叶原料中人参皂苷,并采用高氯酸比色法,以人参皂苷标准品Re为对照品,分析西洋参茎和叶中人参皂苷的含量。结果表明,叶中人参皂苷的含量明显高于茎。故以叶为原料,研究不同的提取和精制工艺。结果表明:超声波提取人参皂苷提取率较水煎煮提取大。比较大孔树脂吸附和溶剂萃取两种不同精制工艺,正丁醇溶剂萃取精制得到的人参皂苷含量较大孔树脂吸附大,其人参皂苷提取率较大孔树脂吸附高,再经A l2O3脱色,得到西洋参叶人参皂苷含量均在90%以上。 相似文献
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以剑麻膏为原料,考察了表面活性剂的种类及浓度、料液比、超声功率、萃取时间、萃取次数和浸泡时间对剑麻皂苷萃取的影响。确定较佳萃取条件为:十二烷基硫酸钠浓度0.025 8 mol/L,料液比1∶10(g∶mL),超声功率120 W,萃取时间40 min,萃取次数3次,浸泡时间4 h。同时考察了絮凝剂的种类及添加量、絮凝温度和复合絮凝剂对剑麻皂苷富集的影响。确定较佳絮凝条件为:100 mL剑麻皂苷萃取液中先加20 mL 1%聚合氯化铝,再加2 mL 0.1%阳离子聚丙烯酰胺的复合絮凝剂,絮凝温度50℃。对在较佳的萃取和絮凝条件下所得絮凝物进行水解,结果显示,该工艺得到的剑麻皂素的质量比传统工艺提高了15.5%,每生产1 g剑麻皂素酸用量减少了81.2%,COD排放量减少了96.5%。 相似文献
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对国产红豆越橘中花色苷的提取工艺进行了研究,得到了最佳提取工艺,即pH值为2的酸性水液提取,超滤法纯化。 相似文献
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Djerdj Karlovic Milan Sovilj Jovan Turkulov 《Journal of the American Oil Chemists' Society》1992,69(5):471-476
This paper describes the effect of temperature and moisture content on the kinetics of oil extraction from corn germ flakes
prepared by a dry degermination process. The experiments were carried out according to the factorial design 32. The moisture content in the extracted material was varied in the range 8%–12%, whereas the extraction temperature varied
in the range 52.5°C–57.5°C. From the method of response surfaces, a functional dependence was established between the extraction
rate, the moisture content in the material and the temperature of extraction. On the basis of this dependence, it was concluded
that moisture content had a crucial effect on the rate of oil extraction. A decrease in moisture from 12% to 8% yielded a
doubling of the extraction rate. On the other hand, temperature variations in the given range had no practical effect on the
course of the extraction. Kinetics of oil extraction was determined according to the method developed in the Leningrad Institute
of Oils and Fats (VNIIZh-method), modified to the extent described in the paper. 相似文献
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Ljiljana P. Stanojević Mihajlo Z. Stanković Dragan J. Cvetković Milorad D. Cakić Dušica P. Ilić Vesna D. Nikolić 《分离科学与技术》2016,51(11):1817-1829
Five extraction techniques, maceration, reflux, Soxhlet, Tillepape, and ultrasonic extraction, were used to obtain the extractive matter from nettle leaves. The antioxidant activity of extracts was assessed by DPPH, FRAP, and H2O2 test, while the total phenolic and total flavonoid content was determined according to the Folin–Ciocalteu and aluminium chloride methods, respectively. Model Ponomarev and a non-stationary diffusion model through the plant material were used for modelling extraction process. The extract obtained by Soxhlet extraction, containing higher amounts of extractive matter as well as phenolic and flavonoid compounds, showed better antioxidant activity than those obtained by other extraction techniques. 相似文献
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《分离科学与技术》2012,47(16):2501-2509
Supercritical fluid extraction (SFE) was used to extract three isoflavonoids including irigenin, irisfloretin and dichtomitin from Belamcanda chinensis (L.) DC. The parameters including pressure, temperature, sample particle size, and flow rate of CO2 were optimized with an orthogonal test. Under the optimized conditions of 15 MPa, 55°C, a sample particle size of 20–40 mesh and CO2 flow rate of 40 L h?1. The process was then scaled up by 10 times using a preparative SFE system. The yield of the crude extract from SFE was 4.1%, which contained irigenin, irisfloretin, and dichtomitin 0.71%, 0.49%, and 0.05%, respectively. To compare the extraction methods, Soxhlet Extraction (SE) was performed. The results indicated that SFE was better than SE. Irigenin, irisfloretin, and dichtomitin in the SFE extract were then separated and purified by high-speed counter-current chromatography (HSCCC) with a two-phase solvent system composed of petroleum ether–ethyl acetate–methanol–water (2:4:3:3, v/v). From 5.0 g of dry crude extract, 27.8 mg irigenin, 16.4 mg irisfloretin, and 2.1 mg dichtomitin were obtained at purities of 97.1%, 96.4%, and 98.0%, respectively, as determined by HPLC-PDA. These results well indicate that SFE and HSCCC are very powerful techniques for the extraction and purification of irigenin, irisfloretin, and dichtomitin from B. chinensis. 相似文献