A Novel Method to Fabricate Steel-Al Foam Sandwich Panel with Metallic Bonding

Al foam sandwich panel(AFS) with metallic bonding was fabricated by foaming a hotpressed three-layer composite with two steel facesheets and a melt route precursor as core. The melt route precursor was fabricated by dispersing undecomposed blowing agent into molten Al, followed by solidification. Microstructures of the joints during fabrication process were analyzed by scanning electron microscopy(SEM) and energy dispersive spectroscopy(EDS). Static three-point bending was conducted to evaluate joint quality of the AFS. It was found that a primary bonding was achieved by hot-pressing and significant diffusion layer of Fe-Al intermetallic compounds was sustained between steel and Al foam core by foaming. Damage modes of the AFS under three-point bending were dominated by indentation, plastic hinges, core shear and crack. Delamination between steel and foam was absent, implying that reliable metallic bonding was achieved. This method allows for producing large-scale AFS with steel facesheets.     

ZA27合金的铸态组织及晶界共晶体

研究分析了ＺＡ２７合金（锌－铝合金）的铸态组织及其分布特点。电子探针分析表明ＺＡ２７合金的初生α相和β相晶内偏析十分严重；在电镜下观察可见α相和β相已转变成层片相间的（α＋η）共析体，并从差热分析，微区分析等四个方面着重讨论了ＺＡ２７合金的晶界不平衡组织是共晶体（由α，β，η相组成），而不是共析体。退火处理可以消除晶界不平衡共晶体，并使成分均匀化，从而使ＺＡ２７合金的塑性得到明显提高。     

Novel MoS_2 Microspheres Formed by Solid-State Assembly of Ultratliin Nanoslieets

The MoS_2 microspheres with high specific surface area assembled by ultrathin nanosheets have been successfully synthesized by a facile and environmentally friendly reaction in a closed reactor at moderate temperatures.The solid-state assembly was realized by a simple calcination process,and the annealing temperature played a key role in the formation of the final microspheres.The influences of reaction temperature were carefully investigated.A possible formation mechanism about the solid-state assembly was proposed based on the experimental results.     

高锰钢晶界析出物的研究

本文对高锰钢的铸件及热处理后的金相组织进行了金相、X 光、电子探针及扫描电镜的分析。实验观察到,在钢中磷含量偏高或热处理过热时,沿晶界有磷化物、碳化物和奥氏体的三元共晶体沿原始奥氏体晶界析出,导致冲击韧性的明显下降及出现典型的沿晶脆性断口。     

铝合金微弧氧化陶瓷膜研究

在硅酸盐电解液中采用微弧氧化法在2024铝合金表面形成氧化物陶瓷膜．分别用扫描电镜、X射线衍射仪研究了陶瓷膜的组织形貌和相组成．相对致密均匀的膜层主要由α—Al2O3,γ-Al2O3和少量的非晶相物质组成．陶瓷层纳米硬度从内部到外部呈下降趋势．     

电压及成膜时间对Mg-Zn-Zr-Ca合金陶瓷膜微观组织影响

通过采用微弧氧化技术(MAO),研究微弧氧化处理电压及成膜时间对Mg-Zn-Zr-Ca生物镁合金陶瓷膜的微观结构的影响,从而探究出微弧氧化的成形机理,并获取最佳工艺参数.实验结果表明:与镁基体相比,Mg-Zn-Zr-Ca生物镁合金经微弧氧化处理后,其表面形成乳白色光滑的陶瓷膜,且在微弧氧化处理过程中,当处理电压为450 V和500 V,成膜时间为9 min和11 min时,所形成的陶瓷膜的微观表面微孔较分布均匀,微孔孔径以及表面孔隙率相对稳定.由此,为Mg-Zn-ZrCa生物镁合金选择合适的工艺参数进行微弧氧化表面处理提供理论依据.     

Cerium Chemical Conversion Coating on a Novel Mg-Li Alloy

A novel Mg-Li alloy was treated in a cerium nitrate solution and cerium chemical conversion coating was obtained on the alloy. Then the forming process, structure and corrosion resistance of the coating were investigated. The influential factors of cerium conversion coating were discussed through orthogonal experiments, and the optimum processing parameters were confirmed. XPS spectra displayed that the conversion coating consisted of cerium compounds, and the major component of the protective layer was a m...     

白酒中白色沉淀的分析及其产生原因

对某酒厂白酒在存放时酒瓶中出现的白色沉淀 ,通过各种方法进行了定性和定量分析 ,根据分析结果 ,探讨了沉淀产生的主要原因 ,并结合该酒厂的生产工艺 ,提出相应的解决和预防措施 .     

超硬铝合金LC9的超塑性效应

本文采用了简单的预处理工艺,开发超硬铝合金LC9的超塑性;并以等温拉伸试验和等温压缩试验相互对照、相互补充的试验方法,考察LC9的超塑性唯象学特性。结果表明,该合金的最高延伸率可达220％,m值为0.4,流动应力最低可达10MPa;最佳超塑性变形条件为:温度420℃,应变速率1.67×10~(-3)s~(-1)。     

Effect of Various Additives on Performance of Plasma Electrolytic Oxidation Coatings Formed on AZ31 Magnesium Alloy in the Phosphate Electrolytes

Plasma electrolytic oxidation(PEO) coatings were prepared on AZ31 magnesium alloy using alkaline phosphate as base electrolyte system, and with the addition of sodium silicate(Na_2SiO_3), sodium aluminate(NaAlO_2) and potassium fluorozirconate(K_2ZrF_6) as additives. The microstructure, phase composition and element composition as well as surface profile of the PEO coatings were analyzed by means of scanning electron microscopy(SEM), X-ray diffraction(XRD), energy dispersive X-ray spectroscopy(EDS), and threedimensional(3 D) optical profilometry. The corrosion and wear properties were evaluated by electrochemical potentiodynamic polarization in 3.5 wt% Na Cl solution and ball-on-disc wear tests, respectively. The results showed that the anions of the additives effectively participated in the coating formation influencing its microstructural features, chemical composition, corrosion resistance and tribological behaviour. It was observed that the sample treated by PEO in the electrolyte solution containing K_2ZrF_6 as an additive showed better corrosion and abrasive resistance.     

Microstructure and Properties of Semisolid A356 Alloy Strip Affected by Nozzle Temperature of a Novel Micro Fused-Casting

The semisolid A356 alloy strip was prepared by a novel continuous micro fused-casting process.The microstructure evolution and mechanical property of A356 aluminum alloy strip with different nozzle temperatures were investigated.The nozzle temperature had great influences on the microstructure and property primarily accompanied with the crystal change in the fused-casting area through the cooling conditions.The results showed that the semisolid A356 alloy strip samples fabricated by micro fused-casting demonstrated good performances and uniform structures with the nozzle temperature at 593 ℃ and the stirring velocity at 700 r/min.The fine grains of the primary a-Al phase with average grain size of 51 μm and shape factor up to 0.71 were obtained under the micro fused-casting process,and the ultimate average vickers hardness came up to 83.39±0.89 HV,and the tensile strength and elongation of the A356 alloy strip reached 245.32 MPa and 7.85%,respectively.     

服装工程专业“三明治”数学探索

本文就如何采用产学结合的方式培养服装企业需要的工程技术人才及对“三明治”教学改革中的“实践学期”的教学内容进行了探索。     

装饰合金的研究

本文通过正交试验设计了最佳的合金成分,并简要介绍了合金的生产工艺。试验结果明表,该合金具有优良的加工性能,良好的耐蚀性,其表面呈现与18开金相似的金黄色泽。合金初步应用于生产证明,它的综合性能是比较好的,并可以获得良好的经济效益。     

Effect of Pouring Temperature on Microstructure and Properties of A356 Alloy Strip by a Novel Semisolid Micro Fused-Casting for Metal

A novel semisolid micro fused-casting(MFC) for preparing A356 alloy strips is proposed, and the effects of process parameters of pouring temperature on the microstructure and properties of A356 alloy strips are investigated. MFC means that the semisolid metal slurry was pressed out from the outlet of bottom of crucible to the movable plate, and directly solidified and formed layer by layer. The microstructure and properties of A356 semisolid alloy slurry were influenced by the cooling conditions. Results show that the aluminu alloy A356 strip samples fabricated by micro fused-casting had good performances and uniform structures with the pouring temperature at 595 ℃ and the substrate movement speed at 18 mm/s. The fine grains of the primary a-Al phase with average grain size of 53 μm and shape factor up to 0.72 was obtained, the ultimate tensile strength of the aluminum alloy A356 strip reaches 243.79±3.91 MPa, while the average vickers hardness is 82.65±1.86 HV.     

一种新型SPWM逆变器

本文提出一种主电路采用ＩＧＢＴ，控制电路主要采用ＧＡＬ和ＥＰＲＯＭ设计的新型ＳＰＷＭ数字控制逆变器，论述了设计方法，给出了实验结果，该系统电路简捷、速度快，抗干扰能力强，可在很宽的载波频率范围内应用和深入研究。     

快速凝固 Al-Fe 合金中准晶相的研究

在快速凝固Ａｌ－Ｆｅ－Ｖ－Ｓｉ合金棒材中发现了１种圆形准晶相,尺寸为０２～０５μｍ,成分为Ａｌ－８０ａｔ％Ｆｅ－２．１ａｔ％Ｖ－３．２ａｔ％Ｓｉ。对此准晶进行了透射电镜、Ｘ－光衍射结构分析,并对准晶的形成机制进行了讨论。     

一种全新的Turbo-MIMO接收机方案

为有效克服MIMO中多发送天线引入的空间干扰,结合Turbo编码提出了一种全新和高效的接收机方案。该方案修正了Turbo软迭代译码算法,同步进行干扰检测和Turbo译码,从信息论的角度可以更充分地利用接收的信息。多接收天线可以对判决似然比和迭代译码的外部信息提供分集增益,从而进一步提高系统性能。该方案克服了传统的空时技术,比如STBC（空时分组码）和BLAST（空时层处理）的发送天线、发送时隙以及接收天线间的约束限制。仿真结果从系统性能和迭代参数证实了算法的有效性。     

多主元AlFeCuCoNiCrTi1.5合金的研究

多主元高熵合金是一种新型的合金,具有许多优越的性能。通过电弧熔炼法制备了AlFeCuCoNiCrTi1.5高熵合金,并在不同温度下进行退火处理,利用XRD、SEM以及洛氏硬度仪分析了它在不同的退火温度处理后的组织及硬度变化,结果表明随着退火温度的逐渐升高,该合金中的相除了长大其组织结构保持不变,但是其硬度值会越来越高,到了1000℃甚至达到了61.5HRC。另外,利用阳极极化法测试了铸态下AlFeCuCoNiCrTi1.5高熵合金在0.5MH2SO4溶液和1MNaCl溶液中的电化学性能,极化曲线表明,在0.5MH2SO4溶液中的,与304不锈钢相比,该合金具有较低的腐蚀速率;在1MNaCl溶液,该合金的腐蚀速率与304不锈钢相当,但是其耐点蚀的能力要优于304不锈钢。