磁场频率对固溶时效处理AZ91合金焊接接头组织和性能的影响

对AZ91镁板进行钨极氩弧焊（TIG）过程中,外加不同频率纵向交流磁场,并在焊后进行固溶时效处理,本文对焊接接头固溶时效处理后的组织性能进行了分析。结果表明,经固溶时效处理后,大量弥散的β-Mg17Al12相从基体α-Mg中析出,其析出数量先随磁场频率增加而增多,之后又减少。从而导致焊接接头的显微硬度、抗拉强度和塑性先增大后减小,而焊接接头的耐电化学腐蚀性先减小后增大。磁场频率为15 Hz时,其接头耐蚀性最差,但接头显微硬度、抗拉强度和塑性最好。     

磁场频率对AZ91合金焊接接头直接时效的组织和性能的影响

对AZ91镁合金板进行钨极氩弧焊（TIG）,并在焊接过程中施加了不同频率纵向交流磁场,焊后对焊接接头直接进行了时效处理,并和焊后固溶时效处理方式进行了对比。结果表明：随着磁场频率的增加,AZ91镁合金焊接接头经直接时效处理后,焊缝中的β-Mg17Al12相由连续状析出形态变成非连续状析出,其组织形态与焊后固溶时效相比,β-Mg17Al12相较粗大且数量减少;并随着磁场频率增加,直接时效后的焊接接头析出β-Mg17Al12相先变得均匀细小后又变得粗大,其接头的力学性能先变好后变差,而焊接接头的抗电化学腐蚀性先减小后增大。与固溶时效相比,直接时效后接头的力学性能较差,但耐腐蚀性能更好。     

外加磁场对AZ31镁合金焊接接头组织性能的影响

在对5mm厚的AZ31镁合金板进行GTAW焊接的过程中，外加纵向交流磁场，研究了磁场对焊接接头的力学性能和显微组织的影响，并探讨了磁场的作用机理。结果表明：外加纵向磁场通过旋转电弧对熔池进行搅拌，不仅可以细化晶粒，使焊接接头的抗拉强度、硬度得到改善，还可以净化熔池中液态镁合金（使杂质球化并弥散分布），此外磁场的引入还可降低镁合金焊接热裂纹的敏感性，抑制热裂纹的产生。     

外加磁场对AZ31镁合金焊接接头组织性能的影响

在对5mm厚的AZ31镁合金板进行GTAW焊接的过程中,外加纵向交流磁场,研究了磁场对焊接接头的力学性能和显微组织的影响,并探讨了磁场的作用机理。结果表明:外加纵向磁场通过旋转电弧对熔池进行搅拌,不仅可以细化晶粒,使焊接接头的抗拉强度、硬度得到改善,还可以净化熔池中液态镁合金(使杂质球化并弥散分布),此外磁场的引入还可降低镁合金焊接热裂纹的敏感性,抑制热裂纹的产生。     

铸态AZ91D镁合金双面TIG焊焊接接头组织研究

对3mm厚铸态镁合金进行TIG焊研究,采用交流、双面焊接,其正面焊接电流为120A,背面焊接电流分别为80、90、100A,焊接速度和保护气体流量不变,焊接完成后按照标准程序对焊缝取样,用光学显微镜观察焊接接头的微观组织.分析表明:焊缝表面成形不好,焊缝表面存在明显缺陷;随着背面焊接电流的增加,焊缝中网状β-Mg17Al12相减少,而颗粒状的β-Mg17Al12相增多.     

热处理对磁场作用下AZ91镁合金焊接接头组织和性能的影响

对5 mm厚的AZ91镁板进行钨极氩弧焊的过程中,外加纵向交流磁场,并在焊后进行固溶、固溶时效和时效处理. 通过对接头显微组织和力学性能分析,研究磁场参数对热处理后AZ91焊接接头组织和性能的影响规律. 结果表明,磁场作用下的AZ91镁合金焊接接头比未施加磁场的焊接接头经固溶处理后晶粒更加细小;经固溶时效处理后更多细小弥散的β-Mg₁₇Al₁₂相大量在α-Mg上析出;经时效处理后析出的β-Mg₁₇Al₁₂相更加细小、断续、分散,且施加磁场的焊接接头比未加磁场的焊接接头热处理后硬度、强度和塑性都得到提高.     

AZ91镁合金激光焊接研究综述

阐述了AZ91镁合金激光焊接的国内外研究成果,介绍了AZ91镁合金激光焊接工艺和接头组织与性能的研究现状.总结发现,当前针对超细晶的AZ91系镁合金的激光焊接研究较少,同时AZ91镁合金激光焊对焊接工业要求极高,若焊接工艺参数选择不当,会出现焊接裂纹、咬边、气孔、凹坑和焊不透等现象.其焊接工艺参数的确定与焊接头组织性能...     

脉冲磁场对AZ91D镁合金凝固组织的影响

研究了脉冲磁场作用下AZ91D镁合金凝固组织的变化,考察了冷却速度、磁场强度和放电频率对AZ91D镁合金晶粒大小的影响,并对磁场影响凝固组织的机理进行了探讨。试验结果表明:在脉冲磁场的作用下,AZ91D镁合金的凝固组织显著细化,其初生相由发达的树枝晶转变为均匀细小的蔷薇状晶体,共晶网络变得细小且不连续,聚集在晶界上的共晶组织减少;合金的晶粒尺寸随着冷却速度的降低,磁场强度或放电频率的增加而逐渐减小。     

热处理工艺对AZ91镁合金组织与性能的影响

通过对AZ91镁合金进行不同工艺的固溶处理和时效处理,研究了热处理工艺对AZ91镁合金显微组织、力学性能和耐腐蚀性能的影响。结果表明,固溶和时效处理可以明显提高AZ91镁合金的力学性能和耐腐蚀性能。分级固溶处理可使AZ91镁合金的抗拉强度提高27 MPa,-20℃冲击吸收功增加10 J,腐蚀电位正移196 mV。     

钇添加量和固溶处理对AZ91D镁合金组织的影响

添加适量稀土元素钇的AZ91D镁合金采用真空熔炼、金属型铸造的方法获得,并对之进行了固溶处理;研究了钇的添加量及固溶处理时间对AZ91D合金组织的影响.结果表明,经350℃固溶处理16h、钇含量约为0.6％的AZ91D镁合金具有均匀、细小的组织和最佳的力学性能和.     

Microstructure refinement of AZ91D alloy solidified with pulsed magnetic field

The effects of pulsed magnetic field on the solidified microstructure of an AZ91D magnesium alloy were investigated. The experimental results show that the remarkable microstructural refinement is achieved when the pulsed magnetic field is applied in the solidification of AZ91D alloy. The average grain size of the as-cast microstructure of AZ91D alloy is refined to 104 μm. Besides the grain refinement, the morphology of the primary α-Mg is changed from dendritic to rosette, then to globular shape with changing the parameters of the pulsed magnetic field. The pulsed magnetic field causes melt convection during solidification, which makes the temperature of the whole melt homogenized, and produces an undercooling zone in front of the liquid/solid interface by the magnetic pressure, which makes the nucleation rate increased and big dendrites prohibited. In addition, primary α-Mg dendrites break into fine crystals, resulting in a refined solidification structure of the AZ91D alloy. The Joule heat effect induced in the melt also strengthens the grain refinement effect and spheroidization of dendrite arms.     

深冷处理对AZ31镁合金焊接接头组织与性能的影响

针对镁合金焊接接头的软化问题,采用不同深冷时间对AZ31镁合金MIG焊接接头进行了深冷处理,并测试与分析了不同深冷时间下焊接接头的力学性能和显微组织。结果表明,深冷处理可显著强化AZ31镁合金焊接接头,其中经过(-196℃,12 h)深冷处理后的焊接接头,硬度提高了8.3%,抗拉强度与伸长率分别提高了15.43%和10.16%;随着深冷时间的延长,焊接接头的组织进一步细化,并有第二相在基体上不断析出,且呈弥散分布。     

固相合成AZ91D镁合金的组织和性能

利用固相合成方法在挤压比为11∶1的条件下,将AZ91D镁合金屑分别在573、623、673和723 K时制备成试样,对试样进行微观组织观察和力学性能测试。结果表明:在573~673 K时,AZ91D镁合金的抗拉强度和延伸率随合成温度的升高而增大,高于673 K时其抗拉强度和延伸率随合成温度的升高而降低,在合成温度为673 K时,其抗拉强度最高,达到384.4 MPa;在热挤出过程中氧化层被均匀弥散在组织中且发生动态再结晶,使固相合成AZ91D镁合金的力学性能与铸态和用铸锭热挤出制备的镁合金相比明显提高,在合成温度为673 K时,其延伸率为5.8%,比铸态增加152%;AZ91D镁合金屑在挤出过程中不能完全结合且出现较多的微裂纹,使其延伸率与铸锭热挤出制备的AZ91D镁合金相比低44%。     

电磁场对AZ91镁合金凝固态组织的影响

利用XRD和OM分析等手段研究了高频电磁场对AZ91合金凝固态组织的影响。结果表明：无磁场作用时,晶粒尺寸约为180μm,其组织的固相颗粒为树枝状。在磁场作用下AZ91的晶粒有所细化,晶粒尺寸约为120μm,晶粒变得圆整。用石英管作为加热容器会使石英管中的硅与镁反应生成Mg2Si。离石英管壁越近,合金中的Mg2Si越多。     

Microstructure and texture evolution of the cold-rolled AZ91 magnesium alloy strip under electropulsing treatment

The effect of electropulsing treatment (EPT) on the microstructure and texture evolution of the cold-rolled AZ91 magnesium alloy strip was investigated using X-ray diffraction (XRD) and electron backscattered diffraction patterns (EBSD). The results indicated that EPT accelerated tremendously the recrystallization behaviour of the cold-rolled AZ91 magnesium alloy strip at a relatively low temperature within a short time of 7 s. It also suppressed precipitation of β-Mg₁₇Al₁₂ phase, compared with conventional heat treatment. The recrystallized grains favourably weakened the intensity of the basal texture. A mechanism for rapid recrystallization process during EPT was proposed based on the enhancement of nucleation rate and atomic diffusion resulting from the coupling of the themal and athermal effects.     

Effect of heat input on microstructure and properties of welded joint in magnesium alloy AZ31B

Using the optical microscope, tensile test machine and micro-hardness meter, the effect of heat input on the microstructure and mechanical properties in fusion welding joints of AZ31B wrought alloys was investigated systematically, the mechanism on joint properties losing was analyzed, and a valid method to improve joint properties of the magnesium alloy fusion welding was explored. The results show that the heat input has an obvious effect on the microstructure and properties. Under the condition of penetration, with the heat input decreasing, the crystal grain in the weld and heat-affected zone (HAZ) becomes fine, the width of HAZ becomes obviously narrow, and the molding of the weld is improved, so the tensile strength and elongation are increased and the hardness of joints is improved. When the heat input reaches 60 J/mm, the high quality joints can he gained.     

钕对AZ91镁合金铸态组织的影响

利用光学显微镜、电子探针和X射线衍射仪研究Nd对AZ91镁合金铸态显微组织的影响，并利用Imagetool软件测量晶粒尺寸和面积。结果表明：少量Nd对α-Mg晶粒有显著的细化作用，平均晶粒尺寸由108μm降至约31μm，晶粒面积也明显减小，Nd的最佳加入量为0．5％。此外，Nd的加入致使β-Mg17Al12相弥散细小，组织中出现了粒状或针状Al3Nd化合物。     

Microstructure refinement of AZ31 alloy solidified with pulsed magnetic field

The effects of a pulsed magnetic field on the solidified microstructure of an AZ31 magnesium alloy were investigated. The experimental results show that the remarkable microstructural refinement is achieved when the pulsed magnetic field is applied to the solidification of the AZ31 alloy. The average grain size of the as-cast microstructure of the AZ31 alloy is refined to 107 μm. By quenching the AZ31 alloy, the different primary α-Mg microstructures are preserved during the course of solidification. The microstructure evolution reveals that the primary α-Mg generates and grows in globular shape with pulsed magnetic field, contrast with the dendritic shape without pulsed magnetic field. The pulsed magnetic field causes melt convection during solidification, which makes the temperature of the whole melt homogenized, and produces an undercooling zone in front of the liquid/solid interface, which makes the nucleation rate increased and big dendrites prohibited. In addition, the Joule heat effect induced in the melt also strengthens the grain refinement effect and spheroidization of dendrite arms.