AISI316奥氏体不锈钢低温PC、PN和PC+PN表面硬化处理

对AISI 31 6奥氏体不锈钢进行了低温离子渗碳 (PC)、离子渗氮 (PN)和离子渗碳 +离子渗氮 (PC +PN)双重复合处理 ,处理后的奥氏体不锈钢可以在不降低耐蚀性能的基础上大幅度地提高不锈钢表面硬度和耐磨性。渗入奥氏体晶格中的碳或 (和 )氮可以形成一种碳或 (和 )氮的过饱和固溶体 (S相 ) ,但没有铬的碳化物或 (和 )氮化物析出。由于PC +PN双重复合处理后的奥氏体不锈钢渗层内的最大含氮量位于渗层的外表面 ,而最大的含碳量则位于渗层较深的部位 ,因而经离子双重复合处理后的奥氏体不锈钢的表面既有离子渗氮处理的高硬度 ,又有离子渗碳处理后的高的渗层厚度和较好的硬度梯度等特点。     

离子氮碳氧复合渗对45钢耐磨性能的影响

用离子氮碳氧复合渗处理的方法 ,在绝热式离子热处理炉上对 45钢试样进行处理。通过金相显微镜和X射线衍射仪观察了化合物层的显微组织和微观结构及在MPX 2 0 0型盘销式摩擦磨损试验机上进行纯滑动干磨损试验。结果表明 ,45钢经离子氮碳氧复合渗处理后 ,表层可获得化合物和氧化物的复合渗层 ,明显提高 45钢的耐磨性能。     

奥氏体不锈钢的低温离子软氮化处理

利用低压等离子体辉光放电技术对AISI 31 6奥氏体不锈钢进行低温离子软氮化硬化处理。处理后的奥氏体不锈钢属于一种无氮化铬或碳化铬析出的氮和碳的过饱和固溶体 (S相结构 )。这种渗入钢中的过饱和氮和碳元素引起奥氏体晶格发生畸变 ,使渗层的硬度和耐磨性都有较大幅度的提高。由于处理后的奥氏体不锈钢渗层内的最大含氮量和最大含碳量分别出现在不同的深度 ,既有离子渗氮处理的高硬度 ,又有离子渗碳处理的高渗层厚度和良好的硬度梯度等特点     

离子氮化－PECVD TiN膜复合处理提高切边模具寿命研究

对用于制作冷作模具的两种高速钢W18Cr4V和W6Mo5Cr4V2Al进行离子渗氮－PECVDTiN复合处理,研究了复合处理层的组织与性能特点。结果表明较之单一PECVDTiN,离子渗氮－PECVDTiN复合处理改善膜基界面结合,显著提高膜基结合强度与耐磨性;采用优化的复合处理可提高高速钢制不锈钢六角螺栓切边模使用寿命一倍以上。     

离子氮化—PECVDTiN膜复合处理提高切边模具寿命研究

对用于制作冷作模具的两种高速钢W18Cr4V和W6Mo5Cr4V2Al进行离子渗氮-PECVDTiN复合处理,研究了复合处理层的组织与性能特点,结果表明：较之单一PECVD TiN,离子渗氮-PECVDTiN复合处理改善膜基界面结合,显著提高膜基结合强度与耐磨性;采用优化的复合处理可提高高速钢制不锈钢六角螺栓切边模使用寿命一倍以上。     

离子辅助沉积对 ZnS/MgF2滤光片光谱漂移的影响

采用霍尔源离子辅助沉积(IAD)技术制备了ZnS/MgF2多层膜窄带干涉滤光片,并与常规沉积条件下制备的样品作比较.结果发现离子辅助沉积明显减小了滤光片的光谱漂移,实测漂移小于O.5 nm,光谱稳定性得到很大提高.计算了滤光片中MgF2膜层的聚集密度,离子辅助沉积使MgF2膜的聚集密度从常规条件下的0.70提高到O.97,增幅达38%.间隔层对光谱漂移的影响最大,越远离间隔层的膜层,其影响越小.     

奥氏体不锈钢离子渗氮-PECVD-TiN复合处理层组织与性能特性研究

对１Ｃｒ１８Ｎｉ９Ｔｉ 奥氏体不锈钢进行离子渗氮－ ＰＥＣＶＤ ＴｉＮ 复合处理, 研究了复合处理层的组织与性能。结果表明： 复合处理层具有优良的膜基结合强度; 较之不锈钢基体, 耐磨性显著提高; 在０－５ ｍｏｌ／Ｌ Ｈ２ＳＯ４ 溶液中, 复合处理层不仅比单一渗氮层的耐蚀性高, 在过钝化区还表现出比不锈钢基体更优越的耐蚀性。     

奥氏体不锈钢离子氮化与离子软氮化的比较

文章对1Cr18Ni9Ti奥氏体不锈钢分别进行离子氮化与离子软氮化处理,工艺条件:处理温度480℃,处理时间8h,工作气压500Pa,工作电压800V,氨气流量1L/min;离子软氮化采用丙酮作为渗碳气氛,丙酬流量为0.01L/min.实验结果表明:离子氮化处理后渗层厚度为48μm,表面显微硬度为1310 HV0.1;离子软氮化处理后渗层厚度为70μm,表面显微硬度为1286HV0.1,且离子软氮化比离子氮化渗层厚度更厚、硬度梯度更缓和.     

离子辅助沉积对 Nb2O5薄膜特性的影响

为了提高Nb2O5薄膜的聚集密度,改善氧化铌薄膜的光学特性和机械特性,采用霍尔源离子辅助沉积(IDA)技术在K9玻璃基板上制备了Nb2O5单层薄膜,并与常规沉积条件下制备的Nb2O5薄膜作了比较.由于IAD技术使Nb2O5膜的聚集密度提高了14%,膜层折射率从常规工艺的2.03上升到2.18,膜层的附着力和牢固度从常规工艺的1.0×107N/m2提高到129.7×107N/m2.     

AISI 304奥氏体不锈钢活性屏离子渗碳

利用活性屏离子热处理技术对AISI 304奥氏体不锈钢进行低温离子渗碳(AS-PC)处理,可以在不锈钢表面形成一层无碳化铬析出的碳的过饱和固溶体(Sc相)。处理后的奥氏体不锈钢可以在不降低耐蚀性能的基础上大幅度提高不锈钢表面的硬度,并解决了不锈钢直流离子渗碳温度均匀性差,工件存在边缘效应等问题,ASPC渗碳试样表面基本可以保持原色。     

Surface wear resistance properties of Ta＋N implanted W18Cr4V high speed steel

High-speed steel W18Cr4V is commonly used in industries such as blade and mould manufacturers because of its high level of hardness and toughness, red-hardness and resistance. Ion implantation is an effective method to improve the wear resis-tance of W18Cr4V. In our investigation, Ta and Ta+N ion implantation was performed on W18Cr4V high-speed steel. The surface properties after implantation were evaluated by measuring friction coefficients while the carbonyl phase of the surface was ana-lyzed by X-ray diffraction analysis. It was found that the friction coefficients of the treated samples were much lower. Samples implanted with Ta+N had a lower friction coefficients than samples implanted only with Ta. This can be attributed to the formation of a new chemical compound, Fe7Ta3, on both surfaces. An even harder chemical compound, Fe2N, was formed on both sttrfaces of Ta+N implanted samples.     

Cooperative effect of surface alloying and laser texturing on tribological performance of lubricated surfaces

The cooperative effect of laser surface texturing (LST) and double glow plasma surface alloying on tribological performance of lubricated sliding contacts was investigated. A Nd:YAG laser was used to generate microdimples on steel surfaces. Dimples with the diameter of 150 μm and the depth of 30–35 μm distributed circumferentially on the disc surface. The alloying element Cr was sputtered to the laser texturing steel surface by double glow plasma technique. A deep diffusion layer with a thickness of 30 μm and a high hardness of HV900 was formed in this alloy. Tribological experiments of three types of samples (smooth, texturing and texturing + alloying) were conducted with a ring-on-disc tribometer to simulate the face seal. It is found that, in comparison with smooth steel surfaces, the laser texturing samples significantly reduce the friction coefficient. Moreover, the lower wear rate of the sample treated with the two surface techniques is observed.     

Preparation and characterization of plasma Cu surface modified stainless steel

Cu modified layer was prepared on the surface of AISI304 stainless steel by plasma surface alloying technique.The effects of processing parameters on the thickness,surface topography,microstructure and chemical composition of Cu modified layer were characterized using glow discharge optical emission spectroscopy(GDOES),scanning electron microscopy(SEM)and X-ray diffraction(XRD).The experimental results show that the surface modified layer is a duplex layer(deposited + diffused layer)with thickness of about 26 μm under the optimum process parameters.The modified layer is mainly composed of a mixture of Cu and expanded austenite phase.The ball-on-disk results show that the modified layer possesses low friction coefficients(0.25)and excellent wear resistance(wear volume 0.005×109 μm3).The Cu modified layer is very effective in killing the bacteria S.aureus.Meanwhile,no viable S.aureus is found after 3 h(100% killed)by contact with the Cu alloyed surface.     

Electrochemical corrosion behavior of steel wires in a coalmine with a corrosive medium

A 6 × 19 point-contact hoisting cable was used as our research object to examine the progress of corrosion of steel wires in a laboratory, simulating the actual working conditions in a coalmine. An electrochemical method was used to investigate the corrosion behavior of steel wires with different surface treatments of a corrosive acid solution. The results show that anode activation of steel wire mainly occurs during pre-corrosion, where the anode activation process of bare steel wires is the fastest as is their corresponding corrosion speed, while the anode activation process of oil coated steel wires and their corresponding corrosion speed are the lowest. During the intermediate and late immersion periods,a passive film is generated on the surface of steel wires, which are gradually damaged with the passage of time. Local pitting corrosion occurs easily on the surface of steel wires with a high-polarization potential.Suitable equivalent circuits were chosen to fit the electrochemical impedance spectroscopy (EIS) of steel wires over various corrosive times and different surface treatments, which indicate good fitting results.The double electrical layer charge-transfer resistance increases in the sequence: bare steel wire,untreated steel wire and oil coated steel wire and their corrosion resistance decreases in turn, which is consistent with their polarization curves. The oil layer provides a certain protective effect on untreated steel wires, but its effect is not entirely clear.     

离子渗碳不锈钢表面电化学亮化工艺的优化

采用电化学方法对低温离子渗碳后的奥氏体不锈钢表面进行了亮化处理。由于不锈钢离子渗碳后的硬化层厚度仅为50μm左右,所以在亮化处理过程中应尽可能减少硬化层的减薄量。实验采用正交试验法对亮化处理的工艺参数进行了优化,并对优化后的工艺参数进行了验证。结果表明,采用优化后的工艺参数对渗碳不锈钢进行亮化处理,不但可以恢复不锈钢原有的颜色,改善其表面质量,而且硬化层的损失很小,不锈钢表面仍具有很高的硬度。     

等离子喷焊ZrC增强铁基喷焊层Q345复合板的制备

对Q345钢板进行等离子喷焊表面处理,通过正交实验优化了Q345表面处理的最佳工艺参数,优化的喷焊工艺为电流60 A、焊枪行走速度20 mm/min、送粉量为35％、离子气流量为1.2～1.4 L/min、保护气流量为10～12 L/min.结果表明,Q345基板的组织正常,为珠光体+铁素体组织,热影响区处金相组织仍为...     

The hydro-abrasive erosion wear behavior of duplex-treated surfaces of AISI H13 tool steel

The influence of duplex surface treatments consisting of a DC-pulsed plasma nitriding process and subsequent coatings of CrN and TiAlN deposited by physical vapor deposition(PVD)on AISI H13 tool steel was studied in this article.The treated samples were characterized using metallographic techniques,SEM,EDS,and microhardness methods.Hydro-abrasive erosion wear tests were performed in a specifically designed wear tester in which the samples were rotated in a wear tank containing a mixture of distilled water and ceramic abrasive chips with a fixed rotational speed.The wear rates caused by the abrasive particle impacts were assessed based on accumulated weight loss measurements.The worn surfaces were also characterized using optical microscopy,SEM,and EDS.Microhardness measurements indicated a significant increase in the surface hardness of the duplex-treated samples.The surfaces of the samples with the TiAlN coating were approximately 15 times harder than that of the untreated samples and 3 times that of the plasma nitrided samples.Hydro-abrasive erosion wear results showed that the duplex surface treatments,especially the CrN coating,displayed the highest erosion wear resistance.