共查询到20条相似文献,搜索用时 265 毫秒
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“分离及复杂物质分析”课,是为了解决分析工作中物质的分离与富集的有关理论与实践的一门课程,它是在“分析化学”课程基础上进行的,是分析化学专业学生的一门必修课,也是化学专业学生的一门选修课。考虑到分析化学专业目前只设置大专班,学生的理论基础较薄弱,实验训练少,动手能力不强,为保证教学质量,使学生真正学到手,我在三年多的教学实践中,进行了如下三个方面的探索实践,取得了一定的效果。 相似文献
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Tengfei Fan Jianguo Feng Chao Ma Chi Yu Jing Li Xuemin Wu 《Journal of Porous Materials》2014,21(1):113-119
Porous microspheres with different sizes were prepared through solvent evaporation method with ethylcellulose as a matrix material and abamectin as a core material. The abamectin-loaded microspheres were characterized through scanning electron microscopy (SEM), dynamic light scattering (DLS), Fourier transform infrared spectroscopy (FTIR), and thermogravimetric analysis (TGA). The chemical structure of the microspheres was determined through FTIR. DLS analysis showed that the diameter of the microspheres range from 10 to 100 μm. SEM analysis revealed that the inner structure of the microspheres is characterized by a porous network. TGA revealed that the microspheres are thermally stable below 125 °C. The controlled release of abamectin from the microspheres into water and soil was also investigated. Abamectin was released from microspheres into water through diffusion. The release of abamectin into soil was mainly caused by erosion, a result that was verified through SEM. 相似文献
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新型干法水泥是目前水泥行业的发展趋势,中央控制室是新型干法水泥生产线的控制指挥中心。预分解窑系统需要控制的参数较多,综合考虑各参数的变化将有利于窑系统的稳定运行。窑头和窑尾参数是准确判断窑系统运行状况的重要参数,包括窑尾的温度、压力,窑头的温度、压力,窑尾的气体分析等,在操作中应引起操作员的重视。 相似文献
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西玛津在甘蔗及土壤中的残留消解动态 总被引:1,自引:0,他引:1
为了探明西玛津使用后在甘蔗及其土壤中的残留降解规律,采用气相色谱法研究了西玛津90%水分散粒剂在甘蔗及其土壤中的残留消解降解动态和最终残留实验。结果表明:西玛津在甘蔗和土壤中的降解动态方程分别为Ct=19.157e-0.0587t和Ct=1.689 8e-0.036t,半衰期分别为11.8 d和19.3 d;以1 647 g a.i./hm2和2 470.5 g a.i./hm2的剂量在甘蔗田进行喷雾处理,收获期甘蔗和土壤中的最终残留量分别小于0.01 mg/kg和0.02 mg/kg。 相似文献
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Development of microstructure in four hydrothermal reactions has been undertaken using scanning electron microscopy. These are clinker, clinker-sand, slag-lime and slag-lime-sand hydrothermal reactions. The microstructure of clinker hydration products displayed crumpled foils and tabular masses of calcium silicate hydrates; few cubic crystals of hydrogarnet appeared only during the initial stage of the reaction. In clinker-sand mixture the C-S-H phase was the only product identified. In slag-lime hydration the microstructure displayed both of the hydrogarnet crystals and the C-S-H phase. The hydration of slag-lime-sand mixture (an optimum composition) was associated with the formation of ill-crystallized tobermorite and crystalline 11A tobermorite as the main products. 相似文献
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介绍了近年来受阻胺类光稳定剂(HALS)新产品的研究开发情况,高分子量化受阻胺、多功能化受阻胺、低碱性化受阻胺和反应型受阻胺等不断出现;应用研究取得新进展,对PVC体系中有较好稳定的作用。 相似文献
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An organic functional silane was found to be the most efficient among several vector fluids in reactive blend compatibilization of the polyethylene (PE) / polystyrene (PS) / peroxide / vector fluid system. This paper involves further analysis of this reactive blending system. Surface tension data was used to calculate spreading coefficients which were compared to the amount of PE-PS copolymer formed during blending. A good correlation between a computed spreading coefficient and the degree of grafting of PS onto PE was found. The results suggest that the pattern of distribution of the vector fluid in PE / PS blends is the key factor leading to effective results. Furthermore, different peroxides were evaluated in PE / PS blends, in order to determine the dependence of PE / PS interfacial grafting reaction on the structure of the peroxide. 相似文献
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The metabolism of malonaldehyde (MA) was investigated in vivo using male Wistar rats and in vitro using rat liver mitochondria.
Twelve hr after intubation with [1,3-14C] MA, 60–70%, 5–15% and 9–17% of administered radioactivity was recovered in expired CO2, feces and urine, respectively. In rats intubated with [1,2-14C] acetate, the corresponding values were 68–82%, 1–2% and 2–3%.14CO2 evolution was initially slower after14C-MA administration than after14C-acetate administration and more radioactivity was excreted in the feces and urine. In vitro experiments using [1,3-14C] MA showed that MA is metabolized primarily in the mitochondria via reactions involving O2 utilization and14CO2 production. The apparent Km and Vmax were 0.5 mM and 9.3 nmol/min/mg protein for O2 uptake, respectively, and 2.0 mM and 2.4 nmol/min/mg protein for14CO2 production. Addition of malonic acid to mitochondrial incubates at concentrations inhibitory to succinate dehydrogenase did
not affect MA-induced O2 uptake but enhanced14CO2 production from14C-MA.14C-Acetate appeared to be the major accumulating metabolite in rat liver mitochondrial preparations following a 120-min incubation
with14C-MA. A probable biochemical route for MA metabolism involves oxidation of MA by mitochondrial aldehyde dehydrogenase followed
by decarboxylation to produce CO2 and acetate. 相似文献