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Utilization of beef fat might be improved via production of fractions with specific functional properties. Beef fat was fractionated using supercritical carbon dioxide at 40°C and pressures from 10.3–27.6 MPa. Extractions followed by one or two stage separation were collected into glass vials at atmospheric pressure and temperature. Resultant extracts were analyzed for fatty acid content by gas chromatography (GC). A significant difference in concentration due to extraction pressure for 16 straight chain fatty acids, 6 branched chain fatty acids, and 7 unknowns was found. Total fatty acids (mg/g extract) increased as pressure increased. Monounsaturated and polyunsaturated fatty acids increased with increasing pressure and solvent density as shown by the saturate/ unsaturate, saturate/monounsaturate, and saturate/polyunsaturate ratios. 相似文献
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Beef fat was fractionated using supercritical carbon dioxide at 40°C and pressures from 10.3–27.6 MPa. Fractions were analyzed for volatile content using purge and trap gas chromatography. One hundred six volatiles were identified. The concentrations of straight or branched-chain hydrocarbons, aldehydes, ketones, olefins, enals, lactones, and total volatiles were significantly influenced by extraction conditons. The control contained the least volatiles in each class analyzed. Total volatiles were concentrated over controls by 10–100 fold depending on treatment, with lowest pressure extraction conditions yielding highest concentrations of volatiles. 相似文献
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J.W. KING J.H. JOHNSON W.L. ORTON F.K. MCKEITH P.L O'CONNOR J. NOVAKOFSKI T.R. CARR 《Journal of food science》1993,58(5):950-952
Beef patties (raw, raw freeze-dried, cooked, and cooked freeze-dried) were prepared for treatment with supercritical carbon dioxide extraction (SC-CO). Each type of patty was then assigned to one of four treatments: control, static extraction at 170 atm/50°C, dynamic extraction at 170 atm/50°C and dynamic extraction at 544 atm/40°C. Freeze drying of the patties prior to SC-CO2 extraction improved removal of fat and cholesterol. Freeze drying enhanced (P<0.01) cholesterol extraction; however, precooking had limited effects (P>0.05) on cholesterol extraction. Supercritical fluid extraction could be effective to reduce the fat and cholesterol content of preformed meat products, without requiring communication of the sample. 相似文献
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For propane, conditions were 298K and 308K at the liquid vapor pressure. For supercritical mixtures, conditions were 308K at pressures from 8.9 to 15.7 MPa. The solubility of fat in CO2-propane increased with increasing pressure, up to 0.66wt% at 15.7 MPa. The average solubility of the fat in propane at 298K was 16.7wt% and at 308K it was 21.4wt%. The extracted fat was solid with a melting range of 295–314K. There was no apparent degradation of collagen during extractions. Beef shank fat extraction with propane is feasible and advantageous over use of supercritical CO2-propane. 相似文献
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Volatile Content and Sensory Attributes of Supercritical Carbon Dioxide Extracts of Cooked Chicken Fat 总被引:2,自引:0,他引:2
Volatile and sensory profiles were generated for extracts of cooked chicken fat obtained with supercritical carbon dioxide at 10.3 MPa, 20.7 MPa, and 31.O MPa at 40°C. Volatiles (318 total) were quantitated and 77 were identified. Concentrations of total volatiles, 7 compound classes, and 63 individual compounds were affected by treatments, generally increasing with decreasing extraction pressure. All extracts had higher concentrations than unextracted control. Total volatiles were concentrated 12-fold. Six sensory notes differed by treatment. Chicken fat aroma and flavor intensities were greater for all extracts than control and increased as pressure decreased. Total volatiles, 5 classes, and 42 individual compounds correlated with chicken fat aroma and/or flavor. 相似文献
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该文介绍超临界CO_2萃取在多不饱和脂肪酸纯化中应用,对超临界CO_2萃取多不饱和脂肪酸的相平衡基础研究和工艺研究现状进行详细介绍,并分析目前应用领域中存在问题,提出一些解决方法。 相似文献
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采用四因素三水平正交试验方案对超临界CO2 流体萃取蚕蛹油脂的工艺参数进行研究,考察温度、压力、CO2 流量和分离Ⅰ压力等参数对油脂萃取量的影响效果。结果表明:萃取压力30MPa、萃取温度40℃、CO2 流量25kg/h、分离Ⅰ压力9MPa 为最佳参数组合,此条件下油脂萃取率可达30.53%,影响油脂萃取量的主要因素是压力。并对其脂肪酸组成及理化性质指标进行分析和测定,结果表明所得油样中游离脂肪酸较少,有害的过氧化值低、不饱和脂肪酸含量高、无臭味。 相似文献
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超临界CO2萃取大蒜提取物 总被引:4,自引:0,他引:4
研究了超临界二氧化碳萃取大蒜精油的可行性 ,得出最佳的提取工艺条件为 15MPa,40℃。若只需得到蒜素可采用发酵醇提法预处理 ,这样所得蒜素的得率最高 ,可达 44 .5 7% ,若要得到大蒜精油必须进一步利用有机溶剂进行萃取 ,每千克大蒜可得大蒜精油 1.8g。同时对制得的大蒜精油进行了红外吸收光谱定性分析。 相似文献
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对CO2超临界流体代替水作介质下的制革酶脱毛进行了研究,并与常规条件下以水作介质进行的有温有浴酶脱毛和堆置酶脱毛作了对比。结果表明:在CO2超临界流体介质中进行制革酶脱毛是可行的,其脱毛分析液的总蛋白含量和羟脯氨酸含量分别约为常规酶脱毛的2倍和1~2倍,其脱毛分析液的酶活力损失低于常规酶脱毛。CO2超临界流体介质中酶脱毛后铬鞣的革,在本实验条件下其收缩温度达到95℃左右,高于常规酶脱毛后铬鞣的革。本实验中较为理想的在CO2超临界流体介质中进行制革酶脱毛的超临界反应条件为:反应压力8.5MPa、反应温度37℃、反应时间2h、AS1.398蛋白酶用量200单位/g皮。 相似文献
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超临界CO2萃取辣椒红色素的研究 总被引:5,自引:1,他引:5
本文着重研究了以传统溶剂萃取法得到的辣椒油树脂为原料,以无毒、易得、价廉的CO2为萃取剂,采用超临界萃取的方法提取辣椒红色素。通过对萃取压力、萃取温度、萃取时间、CO_2流量等条件的试验,获得了最佳的工艺参数。试验结果表明,超临界萃取法具有工艺简单、操作安全、产品质量好、萃取效率高等优点。 相似文献