高铬白口铸铁复合孕育的作用及动力学条件

采用V渣+Ti+Zn对高铬白口铸铁进行复合孕育。在炉内、炉外实行“二步法”处理并按孕育合金异质形核的生核能大小设计分级处理的顺序,起到了控制碳化物的析出量和改善析出形态、净化铁液、净化晶界、细化晶粒等良好的孕育效果。     

高锰钢复合变质的作用及动力学条件

采用RE-Ca-Ti-Al对高锰钢进行复合变质.在炉内、炉外实行"二步法"处理并按变质合金异质形核的生核能大小设计分级处理的顺序,起到了控制碳化物的析出量和改善析出形态,净化钢液,净化晶界,细化晶粒等良好的变质效果.这些变化主要是复合变质所产生的动力学效应对其影响的结果.这种变质作用受制于复合变质在冶金处理过程中所应具备的相关的动力学条件.     

高铬白口铸铁复合变质的作用及动力学效应

采用Re-A l-B i-Mg对高铬白口铸铁进行复合变质。在炉内、炉外实行"二步法"处理并按变质合金异质形核的生核能大小设计分级处理的顺序,起到了控制碳化物的析出量和改善析出形态,净化铁液,净化晶界,细化晶粒等良好的变质效果。这些变化主要是复合变质所产生的动力学效应对其影响的结果。     

高铬白口铸铁复合变质的作用

采用RE-A1-Bi-Mg对高铬白口铸铁进行复合变质。在炉内、炉外实行“二步法”处理并按变质合金异质形核的生核能大小设计分级处理的顺序，起到了控制碳化物的析出量和改善析出形态，净化铁液，净化晶界，细化晶粒等良好的变质效果。这些变化主要是复合变质所产生的动力学效应对其影响的结果。这种变质作用受制于复合变质在冶金处理过程中所应具备的相关的动力学条件。     

复合变质对低铬白口铸铁的作用

采用Re-Al-Bi—Mg对低铬白口铸铁进行复合变质。在炉内、炉外实行“二步法”处理并按变质合金异质形核的生核能大小设计分级处理的顺序,起到了控制碳化物的析出量和改善析出形态、净化铁液、净化晶界、细化晶粒等良好的变质效果。这些变化主要是复合变质所产生的动力学效应对其影响的结果。这种变质作用受制于复合变质在冶金处理过程中所应具备的相关的动力学条件。     

用于小型薄壁灰铸铁铸件的复合孕育方法

介绍了在中频炉熔炼及废钢+增碳剂+回炉料配料条件下,生产小型薄壁灰铸铁件的复合孕育方法.该孕育方法将SiSr孕育剂与SiFe复合使用,能有效确保A型石墨析出、改善断面组织的均匀性、减少白口倾向,因而既能强化孕育效果,又能降低生产成本.     

耐蚀高磁导率合金Ni46MoCu的热处理

耐蚀高磁导率合金Ni46MoCu是一种新合金,生产厂家推荐使用氢气炉、真空炉两种热处理方法.氢气炉处理周期长、费用高;真空炉处理,用推荐的压力处理时粘结严重,提高压力处理时,合金磁性能不合格.试验证实,选用真空氢气保护炉对该合金进行复合净化退火处理后,磁性能合格并达到Ⅱ级合金磁性能标准.     

汽车车轮用低碳Nb微合金钢中的析出行为研究

通过热模拟试验,研究了Nb微合金钢中的碳氮化析出物在高温及低温等温过程中的析出行为.试验结果表明:在高温时,应变诱导NbC析出需要一定的孕育时间.随着高温等温温度的升高,析出物的数量增多.当高温等温时间达到300 s时,单一析出转变为复合析出,同时随着温度的升高,复合析出聚合长大,数量明显减少,形状变为不规则形状;在低温时,随着等温温度的升高,析出数量略有增多.随着等温时间的延长,析出物的数量略有增多,尺寸略有增大.     

高强灰铸铁孕育覆盖剂的研究

生产高强度灰铸铁一般要经孕育处理和加稻草灰覆盖操作.本文提出的孕育覆盖剂主要由孕育元素、助溶剂和覆盖材料三部分的碎粒混合组成.其处理工艺是一种把孕育处理和其他炉外处理技术——熔渣处理、过滤处理和铁水的覆盖保温工艺结合起来的综合炉外处理工艺.即在出铁槽上把一定量的孕育覆盖剂撒到流动的铁水上将孕育和覆盖两个处理工序一次完成.经孕育覆盖剂处理的机床铸铁件在生产中试用,证明具有如下效果;1.简化炉前操作,改善工作环境.2.孕育效果良好,并延长衰退时间.3.提高铁水流动性,并使铸造内应力显著降低.     

一种铸铁用复合过滤器的开发

所开发的用于铸铁的双层过滤器(复合过滤器)同时具有无衰退的孕育功能和净化功能.该复合过滤器由涂挂孕育剂的第一层过滤器和比第一层过滤器更细的第二层过滤器所组成.使用复合过滤器进行了灰铸铁和球墨铸铁的浇注试验,在灰铸铁中,得到了A型石墨,提高了抗拉强度.在球墨铸铁中,石墨大小、形状变得均匀,改善了伸长率.伴随在孕育过程产生的夹杂物可以被第二层过滤器所截获.结果表明这一复合过滤器具有良好的孕育和过滤效果.     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

Thermodynamics Study on the Decomposition of Chromite with KOH

Institute of Process Engineering, Chinese Academy of Sciences, China, has proposed a method for oxidative leaching of chromite with potassium hydroxide. Understanding the mechanism of chromite decomposition, especially in the potassium hydroxide fusion, is important for the optimization of the operating parameters of the oxidative leaching process. A traditional thermodynamic method is proposed and the thermal decomposition and the reaction decomposition during the oxidative leaching of chromite with KOH and oxygen is discussed, which suggests that chromite is mainly destroyed by reactions with KOH and oxygen. Meanwhile, equilibrium of the main reactions of the above process was calculated at different temperatures and oxygen partial pressures. The stable zones of productions, namely, K2CrO4 and Fe2O3, increase with the decrease of temperature, which indicates that higher temperature is not beneficial to thermodynamic reactions. In addition, a comparison of the general alkali methods is carried out, and it is concluded that the KOH leaching process is thermodynamically superior to the conventional chromate production process.     

Influence of Heat Treatment on Damping Behaviour of the Magnesium Wrought Alloy AZ61

The effect of isochronal heat treatments for 1h on variation of damping, hardness and microstructural change of the magnesium wrought alloy AZ61 was investigated. Damping and hardness behaviour could be attributed to the evolution of precipitation process. The influence of precipitation on damping behaviour was explained in the framework of the dislocation string model of Granato and Lücke.     

Effect of Rare Earth Doping on Impedance,Modulus and Conductivity Properties of Multiferroic Composites:0.5(BiLa_xFe_(1-x)O_3)–0.5(PbTiO_3)

The Lanthanum-doped bismuth ferrite–lead titanate compositions of 0.5(Bi LaxFe1-xO3)–0.5(Pb Ti O3)(x = 0.05,0.10,0.15,0.20)(BLxF1-x-PT) were prepared by mixed oxide method.Structural characterization was performed by X-ray diffraction and shows a tetragonal structure at room temperature.The lattice parameter c/a ratio decreases with increasing of La(x = 0.05–0.20) concentration of the composites.The effect of charge carrier/ion hopping mechanism,conductivity,relaxation process and impedance parameters was studied using an impedance analyzer in a wide frequency range(102–106Hz) at different temperatures.The nature of Nyquist plot confirms the presence of bulk effects only,and non-Debye type of relaxation processes occurs in the composites.The electrical modulus exhibits an important role of the hopping mechanism in the electrical transport process of the materials.The ac conductivity and dc conductivity of the materials were studied,and the activation energy found to be 0.81,0.77,0.76 and 0.74 e V for all compositions of x = 0.05–0.20 at different temperatures(200–300 °C).     

Using Finite Element and Contour Method to Evaluate Residual Stress in Thick Ti-6Al-4V Alloy Welded by Electron Beam Welding

This work was to reveal the residual stress profile in electron beam welded Ti-6Al-4V alloy plates(50 mm thick) by using finite element and contour measurement methods.A three-dimensional finite element model of 50-mmthick titanium component was proposed,in which a column–cone combined heat source model was used to simulate the temperature field and a thermo-elastic–plastic model to analyze residual stress in a weld joint based on ABAQUS software.Considering the uncertainty of welding simulation,the computation was calibrated by experimental data of contour measurement method.Both test and simulated results show that residual stresses on the surface and inside the weld zone are significantly different and present a narrow and large gradient feature in the weld joint.The peak tensile stress exceeds the yield strength of base materials inside weld,which are distinctly different from residual stress of the thin Ti-6Al-4V alloy plates presented in references before.     

Microstructures and Tensile Properties of Ultrafine-Grained Ni–(1–3.5) wt% SiC_(NP) Composites Prepared by a Powder Metallurgy Route

Silicon carbide nanoparticle-reinforced nickel-based composites(Ni–Si CNP),with a Si CNPcontent ranged from1 to 3.5 wt%,were prepared using mechanical alloying and spark plasma sintering.In addition,unreinforced pure nickel samples were also prepared for comparative purposes.To characterize the microstructural properties of both the unreinforced pure nickel and the Ni–Si CNPcomposites transmission electron microscopy(TEM) was used,while their mechanical behavior was investigated using the Vickers pyramid method for hardness measurements and a universal tensile testing machine for tensile tests.TEM results showed an array of dislocation lines decorated in the sintered pure nickel sample,whereas,for the Ni–Si CNPcomposites,the presence of nano-dispersed Si CNPand twinning crystals was observed.These homogeneously distributed Si CNPwere found located either within the matrix,between twins or on grain boundaries.For the Ni–Si CNPcomposites,coerced coarsening of the Si CNPassembly occurred with increasing Si CNPcontent.Furthermore,the grain sizes of the Ni–Si CNPcomposites were much finer than that of the unreinforced pure nickel,which was considered to be due to the composite ball milling process.In all cases,the Ni–Si CNPcomposites showed higher strengths and hardness values than the unreinforced pure nickel,likely due to a combination of dispersion strengthening(Orowan effects) and particle strengthening(Hall–Petch effects).For the Ni–Si CNPcomposites,the strength increased initially and then decreased as a function of Si CNPcontent,whereas their elongation percentages decreased linearly.Compared to all materials tested,the Ni–Si CNPcomposite containing 1.5% Si C was found more superior considering both their strength and plastic properties.     

Directional Growth of Tin Crystals Controlled by Combined Solute Concentration Gradient Field and Static Magnetic Field

A new method was introduced to achieve directional growth of Sn crystals. Microstructures in liquid(Pb)/liquid(Sn) diffusion couples were investigated under various static magnetic fields. Results show that the β-Sn crystals mainly reveal an irregular dendritic morphology without or with a relatively low static magnetic field(B0.3 T). When the magnetic field is increased to 0.5 T, the β-Sn dendrites close to the final stage of growth begin to show some directional character. With a further increase in the magnetic field to a higher level(0.8–5 T), the β-Sn dendrites have an enhanced directional growth character, but the dendrites show a certain deflection. As the magnetic field is increased to 12 T, the directional growth of the β-Sn dendrites in the center of the couple is severely destroyed. The mechanism of the directional growth of the β-Sn crystals and the deflection of the β-Sn crystals with the application of static magnetic field was tentatively discussed.     

Quantitative Analysis of the Crystallographic Orientation Relationship Between the Martensite and Austenite in Quenching–Partitioning–Tempering Steels

The orientation relationships(ORs)between the martensite and the retained austenite in low-and medium-carbon steels after quenching–partitioning–tempering process were studied in this work.The ORs in the studied steels are identified by selected-area electron diffraction(SAED)as either K–S or N–W ORs.Meanwhile,the ORs were also studied based on numerical fitting of electron backscatter diffraction data method suggested by Miyamoto.The simulated K–S and N–W ORs in the low-index directions generally do not well coincide with the experimental pole figure,which may be attributed to both the orientation spread from the ideal variant orientations and high symmetry of the low-index directions.However,the simulated results coincide well with experimental pole figures in the high-index directions{123}_(bcc).A modified method with simplicity based on Miyamoto’s work was proposed.The results indicate that the ORs determined by modified method are similar to those determined by Miyamoto’method,that is,the OR is near K–S OR for the low-carbon Q–P–T steel,and with the increase of carbon content,the OR is closer to N–W OR in medium-carbon Q–P–T steel.     

电化学噪声数据处理方法概述

综述了常见的电化学噪声数据处理方法,介绍了直流趋势剔除、统计分析、快速傅立叶变换(FFT)法计算功率谱密度(PSD)以及小波变换处理电化学噪声信号的基本过程,并阐释了各种数学处理及所得参数的物理意义。