共查询到20条相似文献,搜索用时 62 毫秒
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导电聚苯胺及其复合物乳液聚合研究进展 总被引:1,自引:0,他引:1
众多导电聚合物中,聚苯胺(PANI)优越的环境稳定性、优异的电化学性能、光学性能使其从导电聚合物中脱颖而出,备受人们关注。但由于PANI的加工性差、力学性能低等缺陷,使其应用受到严重地制约。大量研究表明:乳液聚合可以简化工艺,降低成本,保护环境,还可以有效地改善PANI的可加工性和溶解性。并且,乳液聚合制备PANI的复合材料,可以较好地改善相客性差的缺点。因此,乳液聚合法成为现今PANI领域研究的一大热点。详细介绍了乳液聚合和微乳液聚合两种聚合方法,并综述了近年来乳液聚合制备PANI及其复合物的研究进展。 相似文献
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乳液聚合法合成聚苯乙烯高分子微球及表征 总被引:1,自引:0,他引:1
采用乳液聚合法合成高分子微球具有方法简单条件易控等特点,采用乳液聚合法合成了纳米级的聚苯乙烯高分子微球,研究了不同聚合条件下聚苯乙烯高分子微球的表征,结果表明,聚合温度、乳化剂用量、搅拌速度对聚苯乙烯高分子微球的平均分子量、粒径有显著影响。 相似文献
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超声辐照引发MMA微乳液聚合产物结构表征 总被引:6,自引:0,他引:6
表征了超声辐照引发MMA微乳液聚合产物的结构,透射电镜观察结果表明,超声辐照引发MMA微乳液聚合得到的PMMA乳胶粒平均粒径为36.5nm。粒径分布窄;粘度法测试表明得到的PMMA分子量约为5百万;红外光谱法和核磁共振氢谱法测试结果表明,超声辐照引发微乳液聚合得到的PMMA以间同立构为主。 相似文献
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聚醚、氨基改性有机硅乳液的研制 总被引:9,自引:1,他引:9
采用乳液聚合合成聚醚、氨基改性有机硅乳液,讨论了乳化剂、催化剂、改性剂用量及反应温度、反应时间对乳液聚合的影响;采用水相和逆相乳化法制得有机硅微乳液,并讨论了乳液的性能。 相似文献
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A method is proposed for estimating the parameters of a mixture of exponential and Weibull distributions for which the accuracy of preliminary estimates obtained by graphical analysis is refined in accordance with the criterion of maximum likelihood. The efficiency of the proposed method is supported by the results of statistical modeling. 相似文献
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An approximate analytical expression is derived for the velocity of the front of the wave of change of boiling modes on a
rod and on a plate. The impact of the Thomson effect and of the heater orientation in the gravity field is included. Adequate
agreement is demonstrated between the derived relations and experimental data. 相似文献
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Liebert A Wabnitz H Grosenick D Möller M Macdonald R Rinneberg H 《Applied optics》2003,42(28):5785-5792
A novel method for the determination of the optical properties of tissue from time-domain measurements is presented. The data analysis is based on the evaluation of the first moment and the second centralized moment, i.e., the mean time of flight and the variance of the measured distribution of times of flight (DTOF) of photons injected by short (picosecond) laser pulses. Analytical expressions are derived for calculation of absorption and of reduced scattering coefficients from these moments by application of diffusion theory for infinite and semi-infinite homogeneous media. The proposed method was tested on experimental data obtained with phantoms, and results for absorption and reduced scattering coefficients obtained by the proposed method are compared with those obtained by fitting of the same data with analytical solutions of the diffusion equation. Furthermore, the accuracy of the moment analysis was investigated for a range of integration limits of the DTOF. The moment analysis may serve as a comparatively fast method for evaluating optical properties with sufficient accuracy and can be used, e.g., for on-line monitoring of optical properties of biological tissue. 相似文献
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水三相点是开尔文热力学温度的唯一基准点,也是ITS-90国际温标重要的定义固定点。因此,水三相点不确定度分析对整个温标的建立、温度量值传递起着至关重要的作用。近3年来,中国计量科学研究院研制出一系列高质量的水三相点容器,加强了水三相点的研究,为不确定度的分析提供了更为可靠的实验依据。同时,不确定度的分析也是客观评价新研制容器性能的一个重要指标。因此,根据实验结果对新研制容器所复现的水三相点进行了不确定度评定。评定结果表明,其扩展不确定度为0.16mK(k=2.69,P=0.99)。 相似文献
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Conventional methods for summation of direct measurement errors are considered. Conditions under which these methods provide consistent results are stated. It is proposed to utilize for characteristic of the total error, its interval estimator or the half-sum of the value obtained by adding up its arithmetic and geometric random errors.Translated from Izmeritel'naya Tekhnika, No. 4, pp. 10–12, April, 1995. 相似文献