软磁金属合金多层磁性薄膜研究进展

概括介绍了金属软磁合金多层薄膜巨磁电阻效应和巨磁阻抗效应的研究和应用，对多层薄膜的制备方法和表征手段作了介绍。磁性金属多层薄膜的层间耦合的理论和模型也进行了介绍。重点是三明治结构、白旋阀结构及隧道结结构等多层膜。最后介绍了磁电阻磁头和磁传感器等应用情况和对该领域研究的展望。     

SmCo/Co多层交换弹性纳米晶复合永磁薄膜的制备和磁耦合研究

利用磁控溅射的方法,在室温条件的Si基片上制备了[SmCo(25nm)/Co(x)]4/SmCo(25 nm)多层交换弹性纳米晶复合永磁薄膜(Co层厚度x=0～10 nm),经过550 ℃/20 min的真空退火处理使薄膜结晶后,进行磁性测试和磁耦合分析.结果表明:SmCo层厚度固定为25 nm时,调整Co层的厚度,从0至10 nm逐渐增加,矫顽力从2270.3 kA·m-1逐渐降低至1040.5 kA·m-1,同时,饱和磁化强度和剩磁随Co层厚度增加逐渐增加,上升了60％.当加入10 nm的Co层后,多层膜的最大磁能积比125 nm的单层SmCo薄膜增加了46％.另外,与SmCo/Co双层交换弹性薄膜在退磁过程中表现的零场附近的软硬磁双相行为相比,SmCo/Co多层交换弹性薄膜表现出单相反转行为,说明体系中的两种磁性层具有更好的磁耦合.经过磁耦合研究发现,当Co软磁层较薄时,薄膜中磁性颗粒以颗粒间交换耦合为主;当软磁层厚度增加时,颗粒间交换耦合减弱,静磁耦合增强,保证了软硬磁相之间的良好磁耦合作用.Co层的加入有效地提高了薄膜的磁性能.     

浅谈高精度磁测在粤北某多金属矿区勘查中的应用

高精度磁测在多金属矿区勘查中应用广泛,它对弱磁性目标物的勘查以及隐伏磁性体在地表产生的弱磁异常研究都有良好的效果。本文是通过对在粤北某多金属矿区开展高精度磁测扫面工作,探测矿区多金属矿化引起的磁异常,结合地质成矿规律进行综合解释,对多金属矿化体深部找矿进行预测,为下一步开展地质找矿或工程验证提供靶区。     

纳米室温磁制冷工质材料的研究

简述了室温磁制冷材料的发展历史和纳米技术，概述了磁制冷材料研究的重点。总结了室温磁制冷工质材料具有优良性能的标准，并且给出了从微观、唯象和纳米方面研究室温磁制冷材料的新思路。介绍了纳米技术在室温磁制冷材料研究中的应用，重点讲述了纳米化对室温磁制冷材料的影响，预测了磁制冷材料的发展趋势。     

钛合金表面硬质膜层研究进展

综述了近年来钛合金材料表面硬质膜层的研究进展,详述了钛合金表面扩渗层、多元素掺杂复合强化硬质膜层以及多层复合结构强化硬质膜层的研究现状及取得的成果,分析了现有钛合金表面硬质膜层研究存在的问题,指出:钛合金表面硬质膜层的强韧性匹配与界面强化仍需深入研究,同时需有效开展钛合金表面硬质膜层的工程应用研究,促进硬质膜层在钛合金材料表面的产业化应用。     

基于COM+和UML的多层分布式制造执行系统的开发研究

结合AriMES的研究设计开发 ,提出了一种采用COM 技术实现可扩展逻辑层的多层分布式制造执行系统技术方案 ,介绍了UML建模在系统设计中的实现方法 ,给出了COM 和UML技术在AriMES的应用实例。对比传统面向对象C/S结构的制造执行系统 ,基于COM 和UML的多层分布式制造执行系统具有良好的扩展性和鲁棒性 ,在实现上也能大大缩短开发周期     

铝合金表面磁屏蔽层的制备及性能

研究了在ZL102合金表面用等离子喷涂和有机树脂粘结法制备低频磁屏蔽防护层，对有机防护层与基体的结合力及各自的防护能力进行了测试。     

稀土系磁制冷材料的研究与发展

较详细地总结了国内外不同温区的稀土系磁致冷材料的研究成果，重点介绍了稀土系室温磁致冷材料的研究现状、存在的问题以及在磁制冷机中的应用情况。结合磁致冷材料及其在样机中应用的最新进展，预测了磁致冷材料的发展趋势。     

NiO和(Pt/Co)多层膜的交换耦合作用及对其矫顽力的影响

研究了用磁控溅射法制备的(Pt/Co)多层膜和绝缘体反铁磁材料NiO之间的磁学和晶体学相互作用。室温下,当NiO覆盖在(Pt/Co)多层膜上面且NiO厚度大于25 nm时观察到了交换偏置,偏置场随NiO厚度的增加而增大。但总体上偏置场(HE)很小,对应NiO厚度为120nm时偏置场不到4000 A·m-1。NiO在(Pt/Co)多层膜下面时没有观察到交换偏置,但是对多层膜的矫顽力和垂直磁各向异性产生了很大影响。(Pt/Co)多层膜的矫顽力随NiO厚度的增加呈现非单调衰减趋势,当NiO厚度为1和3 nm时,矫顽力分别出现极小值和极大值,厚度超过3 nm的NiO使矫顽力单调下降,直至减小到接近零。(Pt/Co)多层膜的垂直磁各向异性随底层NiO厚度的增加逐渐变弱,最后垂直方向变为难轴。矫顽力和垂直磁各向异性的这种变化是由超薄NiO和(Pt/Co)多层膜之间可能存在的邻近效应,弱晶化NiO对(Pt/Co)多层膜(111)织构的影响以及NiO与(Pt/Co)多层膜之间的交换耦合共同作用造成的。     

电子束蒸发法制备Co/Ru多层膜的微观结构与磁电阻

采用电子束蒸发法制备具有不同Co层厚度的Co/Ru多层膜。采用X射线衍射(XRD)、高分辨透射电镜(HRTEM)、扫描电镜(TEM)等对多层膜的微观结构进行观察与分析,研究多层膜微观结构对多层膜磁阻性能的影响,并探讨多层膜磁阻的产生机理。结果表明:Co层的厚度tCo对于薄膜的微观结构和磁阻性能有很大影响,当tCo≥0.8 nm时Co/Ru多层膜以层状方式连续生长,且tCo越大,薄膜结晶越完整,薄膜呈现负磁阻效应;当tCo=0.5 nm时,Co/Ru多层膜为岛状生长,Co/Ru界面的不对称性使得薄膜出现正磁阻效应。     

Fex-C1-x/Si颗粒膜的巨磁电阻效应

利用激光脉冲沉积（PLD）方法制备了沉积于硅基片上的掺杂过渡金属的非晶碳膜结构Fex-C1-x/Si。Fex-C1-x/Si的磁电阻（MR）可正可负，随温度而变化。当温度T〈258K时，Fe0．011-C0.989／Si的MR为负值；当258K〈T〈340K时，该材料的MR为正值，在室温磁场为1T时，该材料的正MR可以大于20％。且在不同的温度范围中，该材料的MR和外加磁场的依存关系呈现出不同的特点：在T=280和300K时，当磁场小于1T时，MR随磁场的增加而快速增加，之后随磁场的继续增加MR增加开始变得缓慢；在T=350K时，MR近似以磁场的B^1.5。的规律变化；而在T=30K时，MR为负值且其大小随磁场的增加而减小。利用双通道模型对该MR效应进行了初步解释。     

超磁致伸缩材料的研究新进展

近年来,稀土超磁致伸缩TbDyFe材料的研究进展迅速,既有新的研究方向如材料力学性能、合金的凝固过程、磁畴取向的分布、组分处于准同型相界的合金的性能等,也有传统的如热处理时施加高磁场及应力处理、新热处理方法等方面。此外,科研人员不断开发出新的稀土超磁致伸缩材料合金体系,即不同元素对TbDyFe体系的部分取代与添加,主要有Pr、Nd、Sm、Gd、Ho和Er等稀土元素及第八族的Co元素。     

Influence of Frequency and Bias Current on Asymmetrical GMI Effect in Co71.8 Fe4.9 Nb0.8 Si7.5 B15 Amorphous Glass-Covered Wires

The Co71.8Fe4.9Nb0.8Si7.5B15 amorphous glass-covered wires（AGCW）are prepared by the Taylor-Ulitovsky technique.The frequency dependence of asymmetrical giant magneto-impedance（AGMI）effect in amorphous glass-covered wires annealed by 70 mA DC current is here presented.The resistance R and the reactance X have been measured,respectively.The real part R and the imaginary part X of impedance play an important role at high frequency and low frequency,respectively.The influence of DC bias current from Ib=0 mA to Ib=5 mA at 30 MHz on the GMI effect in the glass-covered wires annealed by 70 mA DC current is investigated.The asymmetry becomes the largest around Ib=1 mA,and finally decreases for the larger bias current Ib=5 mA.The maximum ΔZ/Z ratio of 310% is observed at 58 MHz under 1 mA bias current.     

TbDyFe超磁致伸缩材料机电耦合特性实验研究

主要讨论TbDyFe超磁致伸缩材料电磁与机械耦合特性实验的若干问题,建立了电磁与机械耦合系统的物理模型并应用阻抗分析方法得到了相应的等效电路．设计制作了实验装置,测定了在电磁场与应力场共同作用下TbxDy1-xFe2-s三元稀土合金超磁致伸缩棒的机电耦合系数与电磁与机械耦合系统振动频率等．所得结果为进一步研制稀土超磁致伸缩换能器提供了重要的实验依据．     

Fe-Cu-Nb-Si-B薄带的淬态纳米化与巨磁阻抗效应

使用较低的快淬速度(V =2 2m·s- 1 ) ,可以使Fe Cu Nb Si B薄带实现淬态纳米晶化。Fe Cu Nb Si B薄带析出αFe(Si)纳米相,其晶粒尺寸在淬态薄带Fe73Cu1 .5Nb3Si1 3.5B9中约为15nm ,在Fe71 .5Cu3Nb3Si1 3.5B9中约为10nm。添加Cu元素可以细化淬态薄带的晶粒。实验发现磁阻抗ΔZ/Z0 ,磁电阻ΔR/R0 ,磁电抗ΔX/X0 三条曲线交叉于一点,通过推导发现此现象具有必然性。淬态薄带Fe74 .5-xCuxNb3Si1 3.5B9的磁阻抗显示了较强的Cu含量依赖性。在快淬速度v =2 2m·s- 1 下,在x =1.5和x =3左右观察到磁阻抗峰值现象。     

Lightweight Design and Verification of Gantry Machining Center Crossbeam Based on Structural Bionics

The lightweight and high efficiency of natural structures are the inexhaustible sources for engineering improvements. The goal of the study is to find innovative solutions for mechanical lightweight design through the application of structural bionic approaches. Giant waterlily leaf ribs and cactus stem are investigated for their optimal framework and superior performance.Their structural characteristics are extracted and used in the bio-inspired design of Lin MC6000 gantry machining center crossbeam. By mimicking analogous network structure, the bionic model is established, which has better load-carrying capacity than conventional distribution. Finite Element Method (FEM) is used for numerical simulation. Results show better specific stiffness of the bionic model, which is increased by 17.36%. Finally the scaled models are fabricated by precision casting for static and dynamic tests. The physical experiments are compared to numerical simulation. The results show that the maximum static deformation of the bionic model is reduced by about 16.22%, with 3.31% weight reduction. In addition, the first four natural frequencies are improved obviously. The structural bionic design is a valuable reference for updating conventional mechanical structures with better performance and less material consumption.     

Experiment on Nonlinear Properties Coupling Electromagnetism with Mechanics of Giant Rare Earth Magnetostrictive Materials

The electromagnetic and mechanical coupling properties of giant rare earth giant magnetostriction material TbxDy1 -xFe2 -z (0. 27 ≤x ≤ 0.3, 0 ≤ z ≤ 0.1 ) alloys were investigated by means of self-fabricated test apparatus. The effect of coupling mechanical with electromagnetic on magnetostrictive strain coefficient was discussed. The physical model of the coupling system was established. Based on the equivalent circuit of the coupling system, the magnetomechanical coupling coefficient was derived by means of impedance resistance analysis method.     

多中心骨巨细胞瘤9例报道与文献分析

Objective: The aim of this study was to investigate the clinical, radiographic and histiopathologic features of multicentric giant cell tumor of bone. Methods: All the clinical data of twenty tumors in nine patients of multicentric giant cell tumor that underwent surgical treatment in our department from 1990 to 2010 were retrospectively reviewed, which included three males and six females. The patients ranged from 15 to 45 years at diagnosis, with an average age of 22.3 years. Three of the patients were younger than twenty years of age. Most tumors arose in long bones, especially around the knee. Radiographically, the tumors in long bones usually manifested as expansive lytic lesions involving the metaphysis and extending into the epiphysis. Three tumors in three patients were confined to the metaphysis, and one tumor exhibited bone-forming lesions. All tumors were treated with curettage or resection. Results: The typical "giant cell" could be found in the oncologic examination in all cases. In some areas, such as the fibrohistiocytic regions, reactive bone forming and aneurysmal bone cyst-like changes could be found. Follow-up averaged 3.5 years, ranging from 6 months to 12 years. There was a recurrence of three tumors, and one patient died of pulmonary metastasis. Conclusion: Multicentric giant cell tumor occur often in younger patients than do solitary giant cell tumor. They are frequently present around the knee, and confined to the metaphysis. Each tumor arose independently, rather than being in multiple sites of metastatic lesion that develop from a single tumor. The risk of recurrence depends on the type of surgery that is performed.     

Giant Magnetoimpedance Effect in Fe89Zr7-xHfxB4 Ribbon

The giant magnetoimpedance (GMI) effect in Fe89Zr7-xHfxB4 (x=0.5 or 1.0) ribbon annealed at different temperatures was investigated. The results show that some addition of hafnium to Fe-Zr-B raises the GMI effect. There is an optimum annealing temperature about 570℃ for obtaining large GMI behavior in Fe89 Zr7-xHfxB4 (x=0.5 or 1.0) nanocrystalline ribbons. At 900 kHz, the magnetoimpedance for Fe89 Zr6Hf1B4 nanocrystalline ribbon monotonically changes with applied DC field, and reaches-33.4 % at 7 162 A/m. Meanwhile, the results show that the transverse anisotropy field of Fe89 Zr6 Hf1 B4 ribbons decreases with increasing annealing temperature from 520℃ to 620℃.     

以低纯度钆研究Gd5Si2Ge2的磁热效应及制备工艺

以99%级的低纯度金属Gd为原料, 采用真空感应炉制备工艺, 辅以1470 K热处理工艺, 获得了与99.99%级高纯度Gd为原料制备的Gd5Si2Ge2合金相近的磁热效应, 5 T外场下最大磁熵变达17.5 J·kg^-1·K^-1, 对比电弧熔炼与感应熔炼两种制备方法, 感应熔炼条件下C, N, O杂质含量明显降低, 发现了Gd5Si2Ge2合金巨磁熵变与相结构的本质联系.