Spray Drying of Chicken Meat Protein Hydrolysate: Influence of Process Conditions on Powder Property and Dryer Performance

The influence of operational conditions of a spray dryer on powder properties and equipment performance during spray drying of chicken meat hydrolysate was evaluated by a central composite rotatable design. The independent variables were inlet air temperature (120 to 200°C) and feed flow (0.1 to 0.38 kg/h). Spray dryer performance was assessed through estimation of product recovery, outlet air temperature, thermal efficiency, and energy on the dryer, obtained by mass and heat balance in the dryer system. Powder property was characterized in respect to antioxidant activity. The stable free radical diphenylpicrylhydrazyl (DPPH) was used to estimate the antioxidant activity of protein hydrolysate powder. This response varied from 38.7 to 59.4% and was only affected by inlet air temperature. Moreover, the results demonstrate a significant effect of the processing conditions on dryer performance. The increase of feed flow results in higher thermal efficiency and lower energy on dryer. Higher product recovery values were obtained at lower inlet air temperature and feed flow.     

PERFORMANCE OF SPRAY DRYER WITH INTEGRATED FILTER AND FLUID BED

Spray dryers featuring a fluid bed integrated into the base of a spray drying chamber have proved one of the most significant developments introduced into industry during the last decade, producing dust-free particulates under low product temperature conditions. The latest design development involves all particulate collection and exhaust air cleaning within the drying chamber with the use of integrated metallic filter elements (with CIP capability). This eliminates handling of fines outside the drying chamber and simplifies the exhaust air system contributing to lower pressure drop losses and lower overall energy consumption. This paper describes the performance of a pilot plant sized spray dryer featuring a drying chamber with both integrated particulate filters and fluid bed. Various products were tested. The results showed that the placing of particulate filters inside the drying chamber does not adversely affect the agglomeration process and that the powder quality compared with that achieved in a standard Fluidized Spray Dryer can be reproduced in this new design concept, with every possibility for improved quality due to no powder handling outside the drying chamber. The work also showed that by containing the powder within the drying chamber, notable operational advantages are apparent and that scale-up of the design concept represents no apparent difficulties.     

CONVECTIVE DRYING OF AGRICULTURAL PRODUCTS. EFFECT OF CONTINUOUS AND STEPWISE CHANGE IN DRYING AIR TEMPERATURE

Samples of banana were dried in a two-stage heat pump dryer capable of producing stepwise control of the inlet drying air temperature while keeping absolute humidity constant. Two stepwise air temperature profiles were tested. The incremental temperature step change in temperature of the drying air about the mean air temperature of 30 °C was 5 °C. The total drying time for each temperature-time profile was about 300 minutes. The drying kinetics and color change of the products dried under these stepwise variation of the inlet air temperature were measured and compared with constant air temperature drying. The stepwise air temperature variation was found to yield better quality product in terms of color of the dried product. Further, it was found that by employing a step-down temperature profile, it was possible to reduce the drying time to reach the desired moisture content.     

Applying Spray Drying to Customized Powder Manufacture

Spray drying is an important continuous industrial process for drying pumpable liquid formulations irrespective of their heat sensitivity, rheology, solids content and processing rate. Furthermore spray drying has the capability through drying chamber design, plant layout and mode of operation to produce dried products of specific particulate size and morphology. These are important aspects when spray drying technology is applied to the needs of customized powder manufacture. There are many examples in industry where spray dried powders have to meet stringent specifications set by such factors as end-product powder quality standards dictated by global competition, dry raw material characteristics required for optimum downstream processing, and dry materials handling to comply with environmental, health and safety issues. Spray drying is no longer regarded just as a convective industrial drying concept, but also as an integral part of modern manufacturing practices applying powder technology. This paper r     

用喷雾干燥方法制造具有指定特性的颗粒

Spray drying is an important continuous industrial process for drying pumpable liquid formulations irrespective of their heat sensitivity, rheology, solids content and processing rate. Furthermore spray drying has the capability through drying chamber design, plant layout and mode of operation to produce dried products of specific particulate size and morphology. These are important aspects when spray drying technology is applied to the needs of customized powder manufacture. There are many examples in industry where spray dried powders have to meet stringent specifications set by such factors as end-product powder quality standards dictated by global competition,dry raw material characteristics required for optimum downstream processing, and dry materials handling to comply with environmental, health and safety issues. Spray drying is no longer regarded just as a convective industrial drying concept, but also as an integral part of modern manufacturing practices applying powder technology. This paper reviews the aspects of spray dryer design and operation for consideration when customized powder manufacture is involved.     

Spray Drying of Tomato Pulp: Effect of Feed Concentration

The effect of feed concentration on spray drying of tomato pulp preconcentrated to 78, 82, and 86% wet basis is investigated in two spray drying systems: a pilot scale spray dryer (Buchi, B-191) with cocurrent regime and a two-fluid nozzle atomizer, and the same connected with an absorption air dryer (Ultrapac 2000). Data for the residue on the chamber and cyclone walls were gathered and two types of efficiencies were calculated as an indication of the spray dryer performance. Tomato powders were analyzed for moisture, particle size, and bulk density. In both spray drying systems, with increases in tomato pulp concentration overall thermal efficiency, evaporative efficiency, material loss in the cyclone, powder moisture content, and bulk density decreased, whereas powder particle size increased. On the contrary, the effect of feed solids content on residue formation and product recovery was dependent on the drying medium. In the standard dryer, the higher the feed concentration, the higher was the residue accumulation, and the lower the product recovery, whereas in the modified system increases in pulp concentration resulted in lower residue formations and higher product yields.     

Hygienic Design Requirements for Spray Drying Operations

Spray drying is used extensively in the food and food-related industries for the manufacture of a wide range of products in dry particulate form both as powders and agglomerates. Spray drying produces these products by atomizing a liquid formulation within a suspended particle drying system. Therefore, the spray-drying process features moist particles existing both in an airborne state and as a semi-dried product present at the walls of the drying chamber, ducts, and associated powder handling components. The presence of any partially dried product within the warm components of the drying system over an extended period of time can result in microbial growth. This presents a possible hygienic risk in such cases where products are sensitive to this form of contamination. With the increasing use of spray drying in the above-mentioned industries, there is greater focus on hygienic spray dryer design and the operating considerations that need to be taken into account, so that hygienic processing can be economically achieved. This is irrespective of whether a hygienic evaluation involves an existing spray dryer or the engineering phase of a new plant.

This article addresses industrial personnel associated with a hygienic manufacturing operation involving spray drying and offers guidelines for assessing whether an existing or planned new spray dryer meets hygienic engineering/design criteria for economic operation without risks of powder quality degradation through contamination.     

Hygienic Design Requirements for Spray Drying Operations

Spray drying is used extensively in the food and food-related industries for the manufacture of a wide range of products in dry particulate form both as powders and agglomerates. Spray drying produces these products by atomizing a liquid formulation within a suspended particle drying system. Therefore, the spray-drying process features moist particles existing both in an airborne state and as a semi-dried product present at the walls of the drying chamber, ducts, and associated powder handling components. The presence of any partially dried product within the warm components of the drying system over an extended period of time can result in microbial growth. This presents a possible hygienic risk in such cases where products are sensitive to this form of contamination. With the increasing use of spray drying in the above-mentioned industries, there is greater focus on hygienic spray dryer design and the operating considerations that need to be taken into account, so that hygienic processing can be economically achieved. This is irrespective of whether a hygienic evaluation involves an existing spray dryer or the engineering phase of a new plant.

This article addresses industrial personnel associated with a hygienic manufacturing operation involving spray drying and offers guidelines for assessing whether an existing or planned new spray dryer meets hygienic engineering/design criteria for economic operation without risks of powder quality degradation through contamination.     

Spray Drying Performance of a Laboratory Spray Dryer for Tomato Powder Preparation

This work investigates the performance of a spray dryer for tomato powder preparation by spray drying of tomato pulp. Samples of tomato pulp with a 14% constant total solids concentration were used, and a pilot scale spray dryer (Buchi, B-191) with cocurrent operation and a two-fluid nozzle atomizer was employed for the spray drying process. Twenty-four different experiments were conducted keeping constant the feed rate, the feed temperature, and the atomizer pressure, and varying the compressed air flow rate, the flow rate of drying rate, and the air inlet temperature. In each experiment the air outlet temperature was recorded. Data for the residue remaining in the chamber and cyclone walls was gathered and two types of efficiencies were calculated as an indication of the spray dryer performance. Analysis of experimental data yielded correlations between residue accumulation and the variable operating conditions. The same operating parameters had a great influence on the air outlet temperature whereas temperature deviations were observed comparing measured air outlet temperatures with corresponding outlet adiabatic saturation temperatures.     

Heat Pump Drying of Green Sweet Pepper

Thin-layer drying experiments under controlled conditions were conducted for green sweet pepper in heat pump dryer at 30, 35, and 40°C and hot air dryer at 45°C with relative humidities ranging from 19 to 55%. The moisture content of sweet pepper slices reduced exponentially with drying time. As the temperature increased, the drying curve exhibited a steeper slope, thus exhibiting an increase in drying rate. Drying of green sweet pepper took place mainly under the falling-rate period. The Page equation was found to be better than the Lewis equation to describe the thin-layer drying of green sweet pepper with higher coefficient of determination and lower root mean square error. Drying in heat pump dryer at 40°C took less time with higher drying rate and specific moisture extraction rate as compared to hot air drying at 45°C due to lower relative humidity of the drying air in a heat pump dryer though the drying air temperature was less. The retention of total chlorophyll content and ascorbic acid content was observed to be more in heat pump–dried samples with higher rehydration ratios and sensory scores. The quality parameters showed a declining trend with increase in drying air temperature from 30 to 45°C. Keeping in view the energy consumption and quality attributes of dehydrated products, it is proposed to dry green sweet pepper at 35°C in heat pump dryer.     

SOME CRITERIA OF SPRAY DRYER DESIGN FOR FOOD LIQUID

Spray drying has many applications for a wide variety of dried food powders. The quality of spray dried food is quite dependent on the atomization characteristics and the heat and mass transfer on drops inside the spray dryer. This paper deals with some design criteria of the spray dryer such as the atomizer, the drop trajectory and the heat/mass transfer between the drop and the drying air.     

FULL CONTAINMENT SPRAY DRYING

ABSTRACT

Aspects of safety, environmental protection, and powder quality will continue to influence advances within spray dryer design and operation, and the concept of full containment spray drying offers a means to meet future industrial requirements. Process air recycle and powder containment within the drying chamber leads to no process air discharge to atmosphere, provides a more favorable operator environment around the spray dryer installation, reduces regions within the dryer layout where potential explosive powder/air mixtures can exist, improves yields, reduces powder losses, and provides easier cleaning operations with reduced wash water requirements.     

A Method for Determination of Porosity Change from Shrinkage Curves of Deformable Materials

The novel low-cost band thermodynamic dryer equipped with a solar collector, a parabolic focusing collector, a heat exchanger, screw fan, and a drying cabinet with a band was designed and tested. The maximum temperature in the solar collector reached 85°C, which was 55°C above the ambient temperature. The required drying time was 4.5 h, much reduced from the traditional solar drying time of 48 h. The final moisture content of the Roselle calyx was 12% w.b., which is the recommended storage moisture content. Measurements of ambient temperature and humidity, air temperature, and relative humidity inside the dryer as well as solids moisture loss-in-weight data are employed as a means to study the performance of the dryer. Solar drying was compared with conventional sun drying and heated air drying, using the following evaluation criteria: drying time, dried Roselle color, texture, taste, and production cost. For evaluation, a model-based Technique for Order Preference by Similarity to Ideal Solution (TOPSIS) methodology was used. After the evaluation, the proposed continuous solar dryer was found to be better than conventional drying and heated air drying due to slower drying rate and better quality of the dried Roselle.     

Drying Kinetics and Quality of Shrimp Undergoing Different Two-Stage Drying Processes

Abstract

An innovative two-stage drying concept is presented in this article. The work considered drying of shrimp using a superheated steam dryer followed by a heat pump (SSD/HPD) or a hot air dryer (SSD/AD) both from drying kinetics and dried product quality points of view. The experiments were performed using the first-stage superheated steam drying temperature of 140°C while the second-stage heat pump drying (or hot air drying) was performed at 50°C. The moisture content of shrimp at the end of the superheated steam drying stage was varied between 30 and 40% (w.b.). The effect of tempering between SSD/HPD was also investigated. Shrinkage, color, rehydration behavior, texture (toughness and hardness), and microstructure of dried shrimp were measured. The results showed that SSD/HPD dried shrimp had much lower degree of shrinkage, higher degree of rehydration, better color, less tough and softer, and more porous than single-stage SSD dried shrimp. It was also found that SSD/AD gave redder shrimp compared to shrimp dried in a single-stage superheated steam dryer. No improvement in terms of shrinkage and rehydration behavior was observed, however.     

Spray Drying Performance of a Laboratory Spray Dryer for Tomato Powder Preparation

Abstract

This work investigates the performance of a spray dryer for tomato powder preparation by spray drying of tomato pulp. Samples of tomato pulp with a 14% constant total solids concentration were used, and a pilot scale spray dryer (Buchi, B-191) with cocurrent operation and a two-fluid nozzle atomizer was employed for the spray drying process. Twenty-four different experiments were conducted keeping constant the feed rate, the feed temperature, and the atomizer pressure, and varying the compressed air flow rate, the flow rate of drying rate, and the air inlet temperature. In each experiment the air outlet temperature was recorded. Data for the residue remaining in the chamber and cyclone walls was gathered and two types of efficiencies were calculated as an indication of the spray dryer performance. Analysis of experimental data yielded correlations between residue accumulation and the variable operating conditions. The same operating parameters had a great influence on the air outlet temperature whereas temperature deviations were observed comparing measured air outlet temperatures with corresponding outlet adiabatic saturation temperatures.     

DYNAMIC SIMULATION AND CONTROL OF CONVEYOR-BELT DRYERS

Abstract

The dynamic behavior of conveyor-belt dryers involving externally controlled heat and mass transfer phenomena has been studied via digital simulation. The investigation concerned an industrial dryer used for the moisture removal from wet raisins. The dryer consisted of three drying chambers and a cooling section, all involving the same conveyor belt. For each chamber, perfect temperature control was assumed for the drying air temperature, while its humidity was left uncontrolled. The effect of material temperature and moisture content at the entrance of the dryer and the drying air temperature on material temperature and moisture content at the exit of the dryer and the corresponding drying air humidity, have been explored by step forcing the disturbance and manipulated variables in the non-linear dryer model simulator. Results showed that material moisture content at the exit of the dryer is greatly affected by material moisture content at the entrance as well as by the drying air temperature. Reliable transfer functions for each process module were obtained by fitting several transfer function models on the simulated data using a least-squares approach. It was found that when input material moisture content could be instantly measured, the system responded slowly enough so that excellent control could be achieved for material moisture content at the exit of each chamber. In this case a Pi-feedback cascade temperature controller was used. When a 15 sec delay measuring sensor was introduced, poor performance was observed. A simplified lead-lag feedforward controller, added to the system, in conjunction with the primary Pi-feedback cascade controller, resulted in good control performance of the delay sensor system.     

ON THE STUDY OF TIME-VARYING TEMPERATURE DRYING—EFFECT ON DRYING KINETICS AND PRODUCT QUALITY

ABSTRACT

The ability of heat pump dryer to produce controlled transient drying conditions, in terms of temperature, humidity and air velocity, has given it an edge over other drying systems. Exploiting this characteristic, we studied and compared the effect of different temperature-time profiles on the quality of agricultural products in a tunnel heat pump dryer capable of providing up to 14.6 kW of cooling capacity. The product quality refers to the color change of the products. Samples of banana and guava were dried in batches in a two-stage heat pump dryer. The effects of the starting temperature of a selected profile and the cycle time on both drying kinetics and product quality were studied. It was observed that by employing a step change in drying air temperature with the appropriate starting temperature and cycle time, it was possible to reduce significantly the drying time to reach the desired moisture content with improved product color.     

DYNAMIC SIMULATION AND CONTROL OF CONVEYOR-BELT DRYERS

The dynamic behavior of conveyor-belt dryers involving externally controlled heat and mass transfer phenomena has been studied via digital simulation. The investigation concerned an industrial dryer used for the moisture removal from wet raisins. The dryer consisted of three drying chambers and a cooling section, all involving the same conveyor belt. For each chamber, perfect temperature control was assumed for the drying air temperature, while its humidity was left uncontrolled. The effect of material temperature and moisture content at the entrance of the dryer and the drying air temperature on material temperature and moisture content at the exit of the dryer and the corresponding drying air humidity, have been explored by step forcing the disturbance and manipulated variables in the non-linear dryer model simulator. Results showed that material moisture content at the exit of the dryer is greatly affected by material moisture content at the entrance as well as by the drying air temperature. Reliable transfer functions for each process module were obtained by fitting several transfer function models on the simulated data using a least-squares approach. It was found that when input material moisture content could be instantly measured, the system responded slowly enough so that excellent control could be achieved for material moisture content at the exit of each chamber. In this case a Pi-feedback cascade temperature controller was used. When a 15 sec delay measuring sensor was introduced, poor performance was observed. A simplified lead-lag feedforward controller, added to the system, in conjunction with the primary Pi-feedback cascade controller, resulted in good control performance of the delay sensor system.     

SOME CRITERIA OF SPRAY DRYER DESIGN FOR FOOD LIQUID

Abstract

Spray drying has many applications for a wide variety of dried food powders. The quality of spray dried food is quite dependent on the atomization characteristics and the heat and mass transfer on drops inside the spray dryer. This paper deals with some design criteria of the spray dryer such as the atomizer, the drop trajectory and the heat/mass transfer between the drop and the drying air.     

ON THE STUDY OF TIME-VARYING TEMPERATURE DRYING—EFFECT ON DRYING KINETICS AND PRODUCT QUALITY

The ability of heat pump dryer to produce controlled transient drying conditions, in terms of temperature, humidity and air velocity, has given it an edge over other drying systems. Exploiting this characteristic, we studied and compared the effect of different temperature-time profiles on the quality of agricultural products in a tunnel heat pump dryer capable of providing up to 14.6 kW of cooling capacity. The product quality refers to the color change of the products. Samples of banana and guava were dried in batches in a two-stage heat pump dryer. The effects of the starting temperature of a selected profile and the cycle time on both drying kinetics and product quality were studied. It was observed that by employing a step change in drying air temperature with the appropriate starting temperature and cycle time, it was possible to reduce significantly the drying time to reach the desired moisture content with improved product color.