Fracture toughness of M2 and H13 alloy tool steels

Abstract

The influence of microstructural variations on the fracture toughness of two tool steels having compositions (wt-%) lC–4Cr–5Mo–2V–6W (AISI M2 high-speed steel) and 0·35C–5Cr–1·5Mo;amp;#x2013;1V (AISI H13 hot-work steel) was investigated. In the as-hardened condition, the H13 steel has a higher fracture toughness than M2 steel, and the latter steel is harder. In the tempered condition, the H13 steel is again softer and has a higher fracture toughness than M2. There is a decrease in fracture toughness and an increase in hardness when the austenitizing temperature is above I050°C for M2 steel and above 1100°C for H13 steel, in both the as hardened and hardened and tempered conditions. The fracture toughness of both steels was enhanced by reducing the grain size and increasing the overall carbide volume in the matrix. The steel samples of average grain diameter ≥40μm exhibit 2–3 MN m ^?3/2 lower fracture toughness than samples of average grain diameter ≤15 μm. A high content of retained austenite appears to raise the fracture toughness of as-hardened M2 steel. Tempering improved the fracture toughness of M2 and H13 steels. The present results are explained using observations of changes in the microstructure and the modes of fracture.

MST/468     

Laser surface alloying of 1045 AISI steel using Ni–CrB2 powder

Abstract

Laser surface alloying is a process whose purpose is to improve the surface properties by incorporating alloying elements into the surface. The advantages of using laser for surface treatment are: formation of a non-equilibrium or amorphous phase as well as homogenisation and refinement of the microstructure, all without affecting the substrate properties. Powder (50 wt-%Ni–50 wt-%CrB₂) was injected into a melt pool created by a CW–CO₂ laser on AISI1045 steel plates. In order to alloy the entire surface, the sample was scanned at scan speeds in the range of 600–6000 mm min^–1 and the laser power was in the range of 1750–2500 W. The powder feed rate was 1·6 g min^–1, the laser beam was 2 mm in diameter, with 60% overlap between successive laser paths. Metallographic cross-sections were made of the samples. For each sample the following properties were characterised: layer depth, microhardness (HV), layer microstructure and composition. It has been found that the scan speed and the laser power affect the depth of the melt pool, the microstructure, the hardness and the treated layer composition. The laser boronised surface exhibits better wear resistance than D2 tool steel hardened to 59 ± 1 HRC. This will be discussed based on numerical analysis of the laser/material interaction.     

Electron beam surface treatment. Part I: surface hardening of AISI D3 tool steel

The effects of electron beam surface hardening treatment on the microstructure and hardness of AISI D3 tool steel have been investigated in this paper. The results showed that the microstructure of the hardened layer consisted of martensite, a dispersion of fine carbides and retained austensite while the transition area mainly consisted of tempered sorbite. Also, the microhardness of the hardened layer on the surface increased dramatically compared to that of base material. Finally, the hardening response of AISI D3 tool steel to electron beam surface treatment is closely related to the scanning speed of the electron beam.     

Effects of nanoparticle addition on hardening and tempering steel

Abstract

The effects of nanoparticle addition on the hardening and tempering 20MnCr steel have been investigated. Addition of oxide nanoparticles to the melt, through a new technology that ensures safe handling, was found to give as hardened steel hardness and tensile properties close to those of the conventional steel in the hardened and tempered condition. This has the potential to eliminate the tempering step in component production, with benefits for process efficiency. The effects on microstructure, hardness and tensile properties depend on the type and concentration of the nanoparticles added. The reduced tensile strength and hardness, and increased ductility, of the steels with nanoparticle additions are attributed to the presence of retained ferrite in these microstructures, in both the hardened and tempered condition. It is proposed that the application of this approach at an industrial scale has the potential to reduce energy consumption, cost and time in component production through the elimination of intermediate operations such as tempering.     

Effects of shot peening on bending fatigue strength of spring steel SS 2090

Abstract

The influence of prior surface condition and of a shot peening treatment on the bending fatigue strength of a standard Si–Cr spring steel (SS 2090) has been investigated. This steel was initially hardened and tempered to a hardness of 52–54 HRC. After shot peening, compressive residual stresses had been introduced into a surface layer of depth ~0·3 mm, with the maximum value of ~1000 MN m^?2 being found close to the surface. The effect of this treatment was to increase the fatigue limit by ~40% to 890 MN m^?2. Coincident with this increase was a change in the site of fatigue initiation from a surface to a subsurface location beneath the compressive residual stress layer. The initiating inclusions, which were 20–40 μm in size, were analysed and found to be Al₂O₃. At stress amplitudes greater than the fatigue limit, initiation was invariably found to occur at the surface and was not always due to inclusions. Inclusion initiated failure has been modelled using the size and spatial distribution of inclusions in the test bars in addition to the variation of applied and residual stresses through the section. A crack propagation criterion based on linear elastic fracture mechanics is used, assuming that propagation is controlled by stress intensity threshold value. It is assumed that small cracks exist at oxide inclusions from the beginning of the fatigue life and that failure is associated with the propagation of one of these cracks.

MST/1392     

Predictive modeling of multi-track laser hardening of AISI 4140 steel

Laser hardening provides benefits over the conventional hardening processes, including minimum distortion in the parts and the absence of a quenchant. This process is also faster than conventional hardening processes and can be used for selective hardening of specific areas of components. One known problem with laser hardening in steels, however, is back tempering when a large area is hardened by multiple, overlapping passes. This study focused on the development of a numerical model to predict the back tempering in multi-track laser hardening. A tempering model was combined with existing models of thermal behavior and phase change kinetics, which were developed earlier in the authors’ group, to predict three-dimensional hardness profiles after multiple track laser hardening. The combined model was first validated through multi-track laser hardening tests and then used to predict and optimize the laser hardened case depth in multi-track laser hardening of AISI 4140 steel. The predictions and parameters optimized to obtain maximum case depth with the least variation along width of the hardened zone were experimentally verified. Case depths up to 2 mm were obtained with 5 mm overlapping of laser tracks.     

Effect of grain size on austenite stability and room temperature low cycle fatigue behaviour of solution annealed AISI 316LN austenitic stainless steel

Abstract

The present paper investigates completely reversed room temperature low cycle fatigue (LCF) behaviour of solution annealed austenitic stainless steel AISI 316L with two different grain sizes of 90 and 139 μm developed by solution annealing treatment at 1050 and 1150°C respectively and at six strain amplitudes ranging between ± 0·375 and ± 1·00%. Complete cyclic hardening has been observed for both the grain sizes. While fine grained steel shows an improvement in cyclic life compared with that of coarse grained steel for strain amplitudes ± 0·375 and ± 0·50%, and perfectly follows the Coffin–Manson (C–M) behaviour within the experimental domain, higher cyclic life with bilinear C–M behaviour is observed in the case of coarse grained steel at ± 0·625% strain amplitude and above. Optical microscopy of fatigue fracture surfaces reveals the formation of martensite on cyclic straining predominantly at higher strain amplitudes.     

Precipitation,microstructure and mechanical properties of low nickel maraging steel

Abstract

A maraging steel with a composition of Fe–12·94Ni–1·61Al–1·01Mo–0·23Nb (wt-%) was investigated. Optical, scanning electron and transmission electron microscopy and X-ray diffraction analysis were employed to study the microstructure of the steel after different aging periods at temperatures of 450–600°C. Hardness and Charpy impact toughness of the steel were measured. The study of microstructure and mechanical properties showed that nanosized precipitates were formed homogeneously during the aging process, which resulted in high hardness. As the aging time is prolonged, precipitates grow and hardness increases. Fractography of the as forged steel has shown mixed ductile and brittle fracture and has indicated that the steel has good toughness. Relationships among heat treatment, microstructure and mechanical properties are discussed. Further experiments using tensile testing and impact testing for aged steel were carried out.     

Cutting mechanism during machining of hardened steel

Abstract

Chip segmentation and the tool forces involved during cutting of hardened steel are discussed. AISI 4340 steel was machined on an engine lathe to study chip morphology, tool forces, and the surface generated. It was found that chip segmentation occurs when the hardness of the steel exceeds a certain value, and that the tool forces associated with chip segmentation are very high. A transformed layer of untempered martensite and retained austenite was produced when the cutting conditions were severe.

MST/469     

Laser Surface Hardening of 9CrSi Steel

The effects of laser hardening parameters such as beam power,beam diameter and scanning rate on microstructure and mardness of 9CrSi steel were investigated.The microstructure of the surface layer of 9CiSi steel was changed from pearlite to martensite,retained austenite and carbide by laser hardening .The depth of the hardened layer increased with increasing laser energy density and the surface hardeness increased by 3-5times as high as the untreated steel.The laser hardened surface had good wear resistance due to martensite and carbide in the surface layer.The wear mode at low speed was abrasive,while the wear mode at high speed was adhesive.     

A semi-empirical method for predicting hardened case depths in laser heat treating

Some predictions on the hardness and hardening depths on laser heat treatment of steels can be obtained when specific characteristics of both laser processes (heating and cooling rates) and laser heat treated steels (microhardness profiles) are taken into account. Some controlled surface temperature laser heat treatments have been carried out with a medium power c.w. CO₂ laser on a medium carbon steel (AISI/SAE1045), allowing these predictions to be tested. In particular, knowing the surface temperature has enabled an analytical algorithm to be used to describe thermal processes and a simple exponential expression to be employed to carefully predict the hardened case depth.     

Dot Matrix Hardening of Steels Using a Fiber Optic Coupled Pulsed Nd:YAG Laser

This paper describes a novel process called “Dot Matrix Hardening” as applied to Ol, D2 and AISI 4340 steels. This process uses a pulsed laser (particularly an Nd:YAG laser) to create a uniform distribution of transformation-hardened spots to cover only a certain percentage of the desired surface. Due to significantly reduced energy input, wear resistance can be imparted to thin and intricate parts without distortion. In addition, with the use of a coupled fiber optic beam delivery system, this process provides greater flexibility compared to conventional CO₂ laser hardening for a number of applications. The use of an Nd:YAG laser also eliminates the need of absorptive coating required for hardening with a CO₂ laser. With optimized processing parameters, a relatively uniform hardened layer is obtained within the hardened spot, with a thickness of about 60 um and hardness values around 800 HV₁₀₀. The sliding wear test results show that the wear resistance of Ol samples with only 20-40% area coverage of laser-hardened spots is similar to the 100% covered laser dot hardened sample as well as the furnace hardened (Re 60) sample.     

Effect of multicomponent modifier on microstructure and mechanical properties of high Ni–Cr–Mo cast iron

Abstract

The microstructure and mechanical properties of high Ni–Cr–Mo indefinite chilled cast iron with the addition of a newly developed multicomponent modifier consisting of mixed rare earths, Si–Ca alloy and Bi–Sb alloy have been investigated through optical microscopy, X-ray diffraction and scanning electron microscopy, along with hardness, impact toughness and wear resistance measurements. After the addition of the modifier, the grain sizes of the primary austenite and eutectic carbides are found to be greatly refined, and the typically highly continuous net-like carbides become less interconnected but rather appear more blocky shaped. Such microstructure changes lead to mechanical property improvement in the cast specimen, with its hardness increased from 43 to 50 HRC, impact toughness from 6·3 to 7·8 J cm^?2 and ?20% increase in abrasive wear resistance.     

Integrated laser based pre-tempering at laser welding of AISI 1045 steel by using 3D-scanner optics

Laser-based pre-heating of laser beam welding with a 3D scanning optics, applied to AISI 1045 steel, is studied. Laser beam welding of heat-treatable steel is challenging due to martensitic hardening in combination with defects. Pre-tempering aims the reduction of the cooling rates and martensitic microstructure within the weld seam. An oscillating defocused laser beam was guided over the surface for pre-heating by means of a 3D scanner optics. During pre-heating, the laser power, the scanning speed and the number of cycles were varied. Welding with 4000 W and 2 m/min with a focused laser beam was executed. Thus the resulting temperature profile behind the ongoing laser beam and cooling time T_8|5 between 800 °C–500 °C was significantly extended. Two parameter combinations (15 cycles|600 W|50 mm/s(²) and 10 cycles|800 W|50 mm/s²) succeeded in a microstructure of bainite and martensite. By extending the cooling time T_8|5 to 3.11 s(²) and 4.17 s². Thus, average hardness for laser based pre-tempering of 487 HV 0.5(²) and 455 HV 0.5² was achieved. As a reference, global pre-heating at 400 °C using a heating plate can reduce the average hardness of the weld zone from 729 HV 0.5 at room temperature to 304 HV 0.5 at a cooling time T_8|5 of 5.63 s.     

Development of rapid heating and cooling (flash processing) process to produce advanced high strength steel microstructures

Abstract

Flash processing of an AISI8620 steel sheet, which involves rapid heating and cooling with an overall process duration of <10 s, produced a steel microstructure with a high tensile strength and good ductility similar to that of advanced high strength steels. Flash processed steel [ultimate tensile strength (UTS): 1694 MPa, elongation: 7·1%], showed at least 7% higher UTS and 30% greater elongation than published results on martensitic advanced high strength steel (UTS: 1585 MPa, elongation: 5·1%). The underlying microstructure was characterised with optical, scanning electron, transmission electron microscopy as well as hardness mapping. A complex distribution of bainitic and martensite microstructures with carbides was observed. A mechanism for the above microstructure evolution is proposed.     

Beitrag zum Verfestigungsverhalten der Stähle durch Kaltverformung

Hardening Behaviour of Steels by Cold Working Contrary to common opinion work hardening increases with higher initial hardness (strength) of steel. This is proved by analysing stressstrain curves of tensile tests at overeleastic load carried out with normalized, hardened and tempered steel. Test results taken from literature are supported by own experiments. Practical application of this fact is discussed very shortly.     

Microstructure and properties of sintered Cu–25Cr alloy

Abstract

Sintered and precipitation hardened Cu–25Cr (wt-%) contact alloys were prepared and their properties related to those of a precipitation and strain hardened reference alloy. The evolution of microstructure during sintering, solution heat treatment, and precipitation hardening was studied, in particular with respect to precipitate morphology and growth. The influence of microstructure on the hardness, strength, and electrical conductivity of Cu–25Cr alloys was evaluated. The relative importance of precipitation and strain hardening has been clarified, and it is shown that the contribution of the precipitation effect is dominant. The importance of monitoring the evolution of microstructure with respect to long term stability of Cu–Cr contact alloys is emphasised.

MST/999     

Microstructure,hardness and residual stress distribution of dissimilar metal electron beam welds: maraging steel and high strength low alloy steel

Abstract

The present investigation reports on a study that has been taken up to develop an understanding of the electron beam welding characteristics of similar and dissimilar combination of maraging steel and high strength low alloy steel, which are in the hardened condition, i.e. maraging steel, in a solution that was in treated and aged condition, whereas high strength low alloy steel in a quenched and tempered condition before welding. The joint characterisation studies include microstructural examination, microhardness survey across the weldment and measurement of residual stresses. Maraging steel weld metal is under compressive stress rather than tensile stress as observed in low alloy steel welds because the martensite transformation occurs at a relatively low temperature. It has been observed that, in dissimilar metal welds, tensile stress is observed at the fusion boundary of low alloy steel and weld metal, whereas compressive stress is obtained at the location between weld and maraging steel fusion boundary. Dissimilar weldment contains a soft region beside the interface on maraging steel side because of the diffusion of manganese from low alloy steel towards maraging steel. The observed residual stresses, hardness distribution across the similar and dissimilar metal welds are correlated with the observed microstructures.     

Numerical simulation of finish hard turning for AISI H13 die steel

A coupled thermo-mechanical model of plane-strain orthogonal turning of hardened steel was presented. In general, the flow stress models used in computer simulation of machining processes are a function of effective strain, effective strain rate and temperature developed during the cutting process. However, these models do not adequately describe the material behavior in hard machining, where the workpiece material is machined in its hardened condition. This hardness modifies the strength and work hardening characteristics of the material being cut. So, the flow stress of the work-material was taken with literature [H. Yan, J. Hua, R. Shivpuri, Development of flow stress model for hard machining of AISI H13 work tool steel. The Fourth International Conference on Physical and Numerical Simulation of Materials Processing, Shanghui in China, 2004, p. 5] in order to take into account the effect of the large strain, strain-rate, temperature and initial workpiece hardness. Then a series of numerical simulations had been done to investigate the effect of machining parameters on the machinability of hardened steel AISI H13 in finish turning process. The results obtained are helpful for optimizing process parameters and improving the design of cutting inserts in finish turning of hardened steel AISI H13.     

Electrochemical methods for studying hydrogen diffusivity,permeability, and solubility in AISI 420 and AISI 430 stainless steels

Abstract

Hydrogen permeation and diffusivity were studied electrochemically at temperatures between 283 and 343 K at constant current for annealed and hardened AISI 420 and annealed AISI 430 stainless steel. Permeation rate, effective diffusivity, and solubility were calculated from these data. Annealed AISI 420 shows higher permeation rate and lower diffusivity than annealed AISI 430 stainless steel. Hardened AISI 420 has the highest permeation rate and lowest effective diffusivity. The calculation of solubility values from permeation data is in good agreement with the values obtained using a newly developed electrochemical hydrogen solubility measurement technique.

MST/1026