Effect of tool rotational speed and pin profile on microstructure and tensile strength of dissimilar friction stir welded AA5083-H111 and AA6351-T6 aluminum alloys

The relatively new welding process friction stir welding (FSW) was applied in this research work to join 6 mm thick dissimilar aluminum alloys AA5083-H111 and AA6351-T6. The effect of tool rotational speed and pin profile on the microstructure and tensile strength of the joints were studied. Dissimilar joints were made using three different tool rotational speeds of 600 rpm, 950 rpm and 1300 rpm and five different tool pin profiles of straight square (SS), straight hexagon (SH), straight octagon (SO), tapered square (TS), and tapered octagon (TO). Three different regions namely unmixed region, mechanically mixed region and mixed flow region were observed in the weld zone. The tool rotational speed and pin profile considerably influenced the microstructure and tensile strength of the joints. The joint which was fabricated using tool rotational speed of 950 rpm and straight square pin profile yielded highest tensile strength of 273 MPa. The two process parameters affected the joint strength due to variations in material flow behavior, loss of cold work in the HAZ of AA5083 side, dissolution and over aging of precipitates of AA6351 side and formation of macroscopic defects in the weld zone.     

Effect of welding parameters on microstructure and mechanical properties of AA6061-T6 butt welded joints by stationary shoulder friction stir welding

Stationary shoulder friction stir welding (SSFSW) butt welded joints were fabricated successfully for AA6061-T6 sheets with 5.0 mm thickness. The welding experiments were performed using 750–1500 rpm tool rotation speeds and 100–300 mm/min welding speeds. The effects of welding parameters on microstructure and mechanical properties for the obtained welds were discussed and analyzed in detail. It is verified that the defect-free SSFSW welds with fine and smooth surface were obtained for all the selected welding parameters, and the weld transverse sections are obviously different from that of conventional FSW joint. The SSFSW nugget zone (NZ) has “bowl-like” shapes with fairly narrow thermal mechanically affected zone (TMAZ) and heat affected zone (HAZ) and the microstructures of weld region are rather symmetrical and homogeneous. The 750–1500 rpm rotation speeds apparently increase the widths of NZ, TMAZ and HAZ, while the influences of 100–300 mm/min welding speeds on their widths are weak. The softening regions with the average hardness equivalent 60% of the base metal are produced on both advancing side and retreating side. The tensile properties of AA6061-T6 SSFSW joints are almost unaffected by the 750–1500 rpm rotation speeds for given 100 mm/min, while the changing of welding speed from 100–300 mm/min for given 1500 rpm obviously increased the tensile strength of the joint and the maximum value for welding parameter 1500 rpm and 300 mm/min reached 77.3% of the base metal strength. The tensile fracture sites always locate in HAZ either on the advancing side or retreating side of the joints.     

Microstructure and tensile strength of friction stir welded joints between interstitial free steel and commercially pure aluminium

In the present study, the joining of interstitial free steel and commercial pure aluminium was carried out by friction stir welding (FSW) technique using tool rotational speeds of 600, 900, 1200 rpm and traverse speed of 100 mm/min. The microstructure and micro-hardness of the weld interface have been investigated. Optical microscopy was used to characterize the microstructures of different regions of friction stir welding joints. The scanning electron microscopy-back scattered electron (SEM-BSE) images show the existence of the different reaction layers in the welded zone. The Al₃Fe intermetallic compound has been observed in the weld interface and their thickness increase with the increase in tool rotational speed. Tensile strength was also evaluated and maximum tensile strength of ∼123.2 MPa along with ∼4.5% elongation at fracture of the joint have been obtained when processed at 600 rpm tool rotational speed.     

The optimisation of process parameters for friction stir spot-welded AA3003-H12 aluminium alloy using a Taguchi orthogonal array

The aim of the present work is to optimise the welding parameters for friction stir spot welded non-heat-treatable AA3003-H12 aluminium alloy sheets using a Taguchi orthogonal array. The welding parameters, such as the tool rotational speed, tool plunge depth and dwell time, were determined according to the Taguchi orthogonal table L9 using a randomised approach. The optimum welding parameters for the peak tensile shear load of the joints were predicted, and the individual importance of each parameter on the tensile shear load of the friction stir spot weld was evaluated by examining the signal-to-noise ratio and analysis of variance (ANOVA) results. The optimum levels of the plunge depth, dwell time and tool rotational speed were found to be 4.8 mm, 2 s and 1500 rpm, respectively. The ANOVA results indicated that the tool plunge depth has the higher statistical effect with 69.26% on the tensile shear load, followed by the dwell time and rotational speed. The tensile shear load of the friction stir spot welding (FSSW) joints increased with increasing plunge depth. Additionally, examination of the weld cross-sections, microhardness tests and fracture characterisation of the selected friction spot welded joints were conducted to understand the better performance of the joints. All the fractures of the joints during tensile testing occurred at stir zone (SZ), where the bonded section was minimum. The tensile shear load and tensile deformation of the FSSW joints increased linearly with increasing the bonded size. The finer grain size in the SZ led to the higher hardness, which resulted in higher fracture strength. When the tensile shear load of the joints increased approximately 3-fold, the failure energy absorption of the joints increased approximately 15-fold.     

Microstructure and mechanical properties as a function of rotation speed in underwater friction stir welded aluminum alloy joints

A 2219-T6 aluminum alloy was underwater friction stir welded at a fixed welding speed and various rotation speeds in order to illuminate the influence of rotation speed on the performance of underwater joints. With increasing rotation speed, the hardness of the stir zone (SZ) gradually increases due to the increase in dislocation density. The tensile strength first increases from 600 to 800 rpm and then reaches a plateau in a wide rotation speed range. After that a remarkable decrease in tensile strength occurs owing to the formation of void defect. The joint welded at lower rotation speed tends to be fractured in the SZ. At higher rotation speeds, the hardness increase in the SZ makes the fracture locations of defect-free joints move to the thermal-mechanically affected zone (TMAZ) or heat affected zone (HAZ).     

Effect of welding parameters on microstructure and mechanical properties of friction stir spot welded 5052 aluminum alloy

Friction stir spot welding (FSSW) is a newly-developed solid state joining technology. In this study, two types of FSSW, normal FSSW and walking FSSW, are applied to join the 5052-H112 aluminum alloy sheets with 1 mm thickness and then the effect of the rotational speed and dwell time on microstructure and mechanical properties is discussed. The lower sheet material underneath the hook didn’t flow into the upper sheet due to the concave surface in the shoulder and groove in the anvil. The hardness profile of the welds exhibited a W-shaped appearance and the minimum hardness was measured in the HAZ. The results of tensile/shear tests and cross-tension tests indicate that the joint strength decreases with increasing rotational speed, while it’s not affected significantly by dwell time. At the rotational speed of 1541 rpm, the tensile/shear strength and cross-tension strength reached the maximum of 2847.7 N and 902.1 N corresponding to the dwell time of 5 s and 15 s. Two different fracture modes were observed under both tensile/shear and cross-tension loadings: shear fracture and tensile/shear mixed fracture under tensile/shear loadings, and nugget debonding and pull-out under cross-tension loadings. The performance of the welds plays a predominant role in determining the type of fracture modes. In addition, the adoption of walking FSSW brings unremarkable improvements in weld strength.     

Feasibility study of friction spot welding of dissimilar single-lap joint between poly(methyl methacrylate) and poly(methyl methacrylate)-SiO2 nanocomposite

In this work, the feasibility of friction spot welding (FSpW) of a commercial poly(methyl methacrylate) (PMMA) GS grade and a PMMA 6 N/2 wt% silica (SiO₂) nanocomposite was investigated. Single-lap joints welded at rotational speeds of 1000, 2000 and 3000 rpm were produced. The analysis of the joint microstructure and material flow pattern indicated that joints could be produced using all of the tested welding conditions. However, the joint produced at 1000 rpm displayed sharp weld lines (weak links), indicating insufficient heat input, while the welds produced at 3000 rpm displayed excessive plastic deformation (bulging of the bottom plate), volumetric defects and a lack of material mixing in the welded area, associated with higher heat input. The weld produced at a rotational speed of 2000 rpm resulted in improved material mixing, which was indicated by the absence of weld lines and volumetric defects due to the more correct heat input. This welding condition was selected for further mechanical testing. Lap shear testing of PMMA GS/PMMA 6 N/2 wt% SiO₂ nanocomposite single lap joints welded at 2000 rpm resulted in an average ultimate lap shear strength of 3.9 ± 0.05 MPa. These weld strength values are equal to or better than those obtained using state-of-the-art welding techniques for PMMA materials, thereby demonstrating the potential of friction spot welding for thermoplastic nanocomposites.     

Effect of welding parameters on microstructure and mechanical properties of friction stir welded joints of a super high strength Al–Zn–Mg–Cu aluminum alloy

Samples made of a super high strength aluminum alloy with high Zn content were friction stir welded with rotation rates of 350–950 rpm and welding speeds of 50–150 mm/min. The effect of welding parameters on the microstructure and mechanical properties was investigated. It was observed that the grain size of the nugget zones decreased with the increasing welding speed or the decreasing tool rotation rate. Most of the strengthening precipitates in the nugget zone were dissolved back and the intragranular and grain boundary precipitates in the heat affected zone coarsened significantly. The greatest ultimate tensile strength of 484 MPa and largest elongation of 9.4 were obtained at 350 rpm−100 mm/min and 350 rpm−50 mm/min, respectively. The ultimate tensile strength and elongation deteriorated drastically when rotation rate increased from 350 to 950 rpm at a constant welding speed of 100 mm/min.     

Microstructure,mechanical and corrosion properties of friction stir welded high nitrogen nickel-free austenitic stainless steel

Friction stir welding (FSW) was applied to a 2.4 mm thick high nitrogen nickel-free austenitic stainless steel plate using tungsten–rhenium (W–Re) tool. The high-quality weld was successfully produced at a tool rotational speed of 400 rpm and a traveling speed of 100 mm/min. The microstructure, mechanical and corrosion properties of the weld were studied. The nitrogen content of the weld was almost identical to that of base metal (BM). FSW refined grains in the stir zone (SZ) through dynamic recrystallization and led to increase in hardness and tensile strength within the SZ, while the ductility was slightly decreased. The failure of tensile specimens occurred in the BM. TEM results revealed precipitates of Cr₂₃C₆ of size ~ 1 μm in the SZ, although their content was small. The precipitation of Cr₂₃C₆ and increase in δ-ferrite in the SZ led to small decrease in both pitting and intergranular corrosion resistance.     

Microstructural characteristics and mechanical properties of non-combustive Mg–9Al–Zn–Ca magnesium alloy friction stir welded joints

Non-combustive Mg–9Al–Zn–Ca magnesium alloy was friction stir welded with rotation speeds ranging from 500 to 1250 rpm at a constant welding speed of 200 mm/min. Defect-free joints were successfully produced at rotation speeds of 750 and 1000 rpm. The as-received hot extruded material consisted of equiaxed α-Mg grains with β-Mg₁₇Al₁₂ and Al₂Ca compounds distributed along the grain boundaries. Friction stir welding produced much refined α-Mg grains accompanied by the dissolution of the eutectic β-Mg₁₇Al₁₂ phase, while Al₂Ca phase was dispersed homogeneously into the Mg matrix. An increase in rotation speed increased the α-Mg grain size but not significantly, while microstructure in the heat affected zone was almost not changed compared with the base material. The hardness tests showed uniform distributed and slightly increased harness in the stir zone. Results of transverse tensile tests indicated that the defect-free joints fractured at the base material, while longitudinal tensile tests showed that the strength of the defect-free welds was improved due to microstructural refinement and uniform distribution of intermetallic compounds.     

Comparative study on local and global mechanical properties of bobbin tool and conventional friction stir welded 7085-T7452 aluminum thick plate

7085-T7452 plates with a thickness of 12 mm were welded by conventional single side and bobbin tool friction stir welding (SS-FSW and BB-FSW, respectively) at different welding parameters. The temperature distribution, microstructure evolution and mechanical properties of joints along the thickness direction were investigated, and digital image correlation (DIC) was utilized to evaluate quantitatively the deformation of different zones during tensile tests. The results indicated that heat-affected zone (HAZ), the local softening region, was responsible for the early plastic deformation and also the fracture location for SS-FSW samples, while a rapid fracture was observed in weld nugget zone (WNZ) before yield behavior for all BB-FSW specimens. The ultimate tensile strength (UTS) of SS-FSW joints presented the highest value of 410 MPa, 82% of the base material, at a rotational speed of 300 rpm and welding speed of 60 mm/min, much higher than that of BB-FSW joints, with a joint efficiency of only 47%. This should be attributed to the Lazy S defect produced by a larger extent of heat input during the BB-FSW process. The whole joint exhibited a much higher elongation than the slices. Scanning electron microscopic (SEM) analysis of the fracture morphologies showed that joints failed through ductile fracture for SS-FSW and brittle fracture for BB-FSW.     

Impact of friction stir welding on recrystallization of oxide dispersion strengthened ferritic steel

Oxide dispersion strengthened (ODS) steels can be used as the structural materials in the future fusion reactors and the fuel cladding materials in the advanced fission reactors. However, the weldability of ODS steels is a severe problem. In the present study, defect-free joints of the 15Cr-ODS ferritic steel were achieved by friction stir welding at different rotation speeds. The recrystallization, hardness and tensile properties are highly related with the rotation speed of the stir tool. The higher rotation speed results in coarser grains in the top SZ, while the grain size exhibits more complicated relation with the rotation speed in the SZ center. The joint welded at 250 rpm exhibits a maximum tensile strength of 974 MPa that reaches about 84% of that of the base metal.     

Microstructure and mechanical properties of friction spot welded 6061-T4 aluminum alloy

Friction spot welding (FSpW) is a relatively new solid state joining technology developed by GKSS. In the present study, FSpW was applied to join the 6061-T4 aluminum alloy sheet with 2 mm thickness. The microstructure of the weld can be classified into four regions, which are stir zone (SZ), thermo-mechanically affected zone (TMAZ), heat affected zone (HAZ) and the base material (BM), respectively. Meanwhile, defects such as bonding ligament, hook and voids are found in the weld, which are associated to the material flow. The hardness profile of the weld exhibits a W-shaped appearance and the minimum hardness is measured at the boundary of TMAZ and SZ. Both the tensile/shear strength and cross-tension strength reach the maximum of 7117.0 N and 4555.4 N at the welding condition of the rotational speed of 1500 rpm and duration time of 4 s. Compared to cross-tension strength, the tensile/shear strength were stable with the variation of processing parameters. Three different fracture modes are observed under tensile/shear loading, which are plug type fracture, shear fracture and plug-shear fracture. There are also there different fracture modes under cross-tension loading, which are plug type fracture (on the upper sheet), nugget debonding and plug type fracture (on the lower sheet).     

Mechanical,fatigue and microstructural properties of friction stir welded 5083-H111 and 6082-T651 aluminum alloys

In this study, 5083-H111 and 6082-T651 aluminum alloy plates in 6 mm thickness that are used particularly for shipbuilding industry were welded using Friction Stir Welding (FSW) method as similar and dissimilar joints with one side pass at PA position with the parameters of 1250 rpm tool rotation, 64 mm/min welding speed and 2° tool tilt angle. Tensile tests results showed sufficient joint efficiencies and surprisingly high yield stress values. Bending fatigue test results of all joint types showed fatigue strength close to each other. Fatigue strength order of the joints were respectively FSWed 5083-5083, and 6082-6082 similar joints and 5083-6082 dissimilar joint. Cross sections of the weld zones have been analyzed with light optical microscopy (LOM) and fracture surface of fatigue test specimens were examined by scanning electron microscopy (SEM). Although there were no voids in radiographic and microscopic analyzes, 5083-6082 joint showed rarely encountered voiding effect under fatigue load. Microhardness measurements revealed rare result for FSWed AW5083 and novel result for FSWed 6082 aluminum alloy.     

Research on fatigue behavior of electron beam welding joint of 06Cr19Ni10 austenitic stainless steel sheet

06Cr19Ni10 austenitic stainless steel sheet square butt joints without filler metal addition were fabricated using EBW (electron beam welding) processes. Fatigue properties, tensile properties and microstructure of the welded joints were studied. It was found that the yield strength, tensile strength, elongation and Vickers hardness of EBW joint can reach the level of base material performance. Fusion zones consist of coarse columnar dendritic grains, which are perpendicular to the weld pool boundary. The hardness of heat affected zone is lower than weld centreline. The reason is that the grain of heat affected zone under the action of electron beam heat source happened recovery and recrystallization. The present work suggests that S–N curve slope of welding joint should be revised to m = 10 under the condition of high stress levels, and S–N curve slope is still m = 3.0 under the condition of low stress levels. Fatigue cracks did not extend along the minimum thickness of the section. On the contrary, fatigue cracks extended along the maximum height of the section.     

Characteristics of the reverse dual-rotation friction stir welding conducted on 2219-T6 aluminum alloy

Reverse dual-rotation friction stir welding (RDR-FSW) has great potential to obtain appropriate welding conditions through adjusting the independently rotating tool pin and surrounding shoulder. The welding torque exerted on the workpiece by the reversely rotating shoulder also cancels off a part of the welding torque exerted by the rotating tool pin, thus the clamping requirement for the workpiece is also reduced. In the present paper, a tool system for the RDR-FSW was designed and successfully applied to weld high strength aluminum alloy 2219-T6, and then microstructures and mechanical properties of the optimized joint were investigated to demonstrate the RDR-FSW characteristics. The weld nugget zone was characterized by the homogeneity of refined grain structures, but there was a three-phase confluction on the advancing side formed by different grain structures from three different zones. The tensile strength of the optimized joint was 328 MPa (73.7% of the base material), showing an obvious improvement when compared with the optimized joint welded by the FSW without the reversely rotating assisted shoulder. The tensile fracture occurred in the ductile fracture mode and the fracture path propagated in the weakest region where the Vickers hardness is the minimum.     

Influence of tool geometry and rotational speed on mechanical properties and defect formation in friction stir lap welded 5456 aluminum alloy sheets

Friction stir welding of AA5456 aluminum alloy in lap joint configuration is with two different tempers, T321 and O, and different thicknesses, 5 mm and 2.5 mm was investigated. The influences of tool geometry and various rotational speeds on macrostructure, microstructure and joint strength are presented. Specifically, four different tool pin profiles (a conical thread pin, a cylindrical–conical thread pin, a stepped conical thread pin and Flared Triflute pin tool) and two rotational speeds, 600 and 800 rpm, were used. The results indicated that, tool geometry influences significantly material flow in the nugget zone and accordingly control the weld mechanical properties. Of particular interest is the stepped conical threaded pin, which is introduced for the first time in the present investigation. Scanning electron microscopy investigation of the fracture location of samples was carried out and the findings correlated with tool geometry features and their influences on material flow and tension test results. The optimum microstructure and mechanical properties were obtained for the joints produced with the stepped conical thread pin profile and rotational speed of 600 rpm. The characteristics of the nugget zone microstructure, hooking height, and fracture location of the weld joints were used as criteria to quantify the influence of processing conditions on joint performance and integrity. The results are interpreted in the framework of physical metallurgy properties and compared with published literature.     

Influence of probe offset distance on interfacial microstructure and mechanical properties of friction stir butt welded joint of Ti6Al4V and A6061 dissimilar alloys

Friction stir butt welding of titanium alloy Ti6Al4V and aluminum alloy A6061-T6 with 2 mm thickness was conducted by offsetting probe edge into the titanium alloy at rotation speed of 750 rpm and 1000 rpm and welding speed of 120 mm/min. The effect of probe offset distance on the interfacial microstructure and mechanical properties of the butt joint was investigated. When the probe offset distance is not sufficient, the two alloys cannot be completely joined together, i.e. there exists no bonding or kissing bonding at the root part of joint interface. However, when the probe offset distance is too large, a great amount of intermetallic compounds are formed at the joint interface and its adjacency, leading to fracturing roughly along the joint interface during a tensile test. In a proper range of probe offset distance, sound dissimilar butt joints are produced, which have comparatively high tensile strength and fracture in heat affected zone of the aluminum alloy during a tensile test.     

Microstructural evolution and mechanical properties of dissimilar Al–Cu joints produced by friction stir welding

5A02 aluminum alloy and pure copper were joined by friction stir welding (FSW). A defect-free joint was obtained when one of process parameters, i.e. the traverse speed was lowered from 40 mm/min to 20 mm/min. A good mixing of Al and Cu was observed in the weld nugget zone (WNZ). A large amount of fine Cu particles were dispersed in the upper part of the WNZ producing a composite-like structure. In the lower part, nano-scaled intercalations were observed and identified by transmission electron microscopy (TEM). These layered structures were subsequently confirmed as Al₄Cu₉ (γ), Al₂Cu₃ (ε), Al₂Cu (θ), respectively. Formation of these microstructures caused an inhomogeneous hardness profile. Particularly, a distinct rise in hardness was noticed at the Al/Cu interface. Excellent metallurgical bonding between Al and Cu gave rise to good behaviors in the tensile and bending strength.     

Evaluation of microstructures and mechanical properties of friction stir welded lap joints of Inconel 600/SS 400

The microstructures and mechanical properties of friction stir welded Inconel 600 and SS 400 lap joints were evaluated in this study. Friction stir welding was carried out at a tool rotation speed of 200 rpm and a welding speed of 100 mm/min. Application of friction stir welding was notably effective in reducing the grain size of the stir zone, as a result, the average grain size of Inconel 600 was reduced from 20 μm in the base material to 8.5 μm in the stir zone. The joint interface between Inconel 600 and SS 400 was soundly welded without voids and cracks, and MC carbides with a size of 50 nm were partially formed in the region of the lap joint interface in Inconel 600. In addition, a hook from SS 400 was formed on the advancing side of the Inconel 600 alloy, which directly affected an increase in the peel strength of the weld. In this study, we systematically discussed the effect of friction stir welding on the evolution of the microstructures and mechanical properties of friction stir lap jointed Inconel 600 and SS 400.