共查询到20条相似文献,搜索用时 62 毫秒
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以海上某深井区块为研究对象,使用(w)50%甲酸钾盐水为基液,通过优选及研制抗高温增黏剂、复合降滤失剂以及流型调节剂等主要处理剂,并采用改性铁矿粉进行加重的方式,开发出一种新型抗高温高密度有机盐钻井液体系.室内评价了其基本性能、沉降稳定性、抑制性能、润滑性能和抗污染性能,评价结果表明:该钻井液体系具有稳定的流变性、较低... 相似文献
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通过对钙基膨润土钠化和有机改性,制备出了可抗240℃的白油基钻井液用有机土。测试表征及评价结果表明,改性后季铵盐类有机覆盖剂进入蒙脱石层间,在蒙脱石表面发生化学键连,晶层间距增大到18.78,有机土层片变得疏松;与国内外有机土相比,该有机土在白油中胶体率高,抗温性强,能起到很好的增粘提切和较好的流变性能,具有较好的推广前景。 相似文献
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选用对苯乙烯磺酸钠(SSS)、2-丙烯酰胺基-2-甲基丙磺酸(AMPS)、丙烯酰胺(AM)单体为原料,利用自由基聚合的方式,得到一种抗高温耐盐聚合物降滤失剂.通过傅里叶红外光谱分析(FT-IR)表明合成产物结构与设计结构相符.当降滤失剂加量为1.8%时,室温下和210℃下淡水基浆的滤失量分别为7.9mL和13.5mL;在25%NaCl和3%CaCl2的盐水泥浆中,钻井液的滤失量分别为14.8mL和11.0mL.通过扫描电镜(SEM)可以分析钻井液形成的滤饼的微观结构,由此得到降滤失剂作用的机理是:当降滤失剂吸附在黏土表面时,降滤失剂可以使黏土颗粒在钻井液中分散,从而形成致密的滤饼来减少滤失量. 相似文献
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The effect of etching temperature on the photoluminescence emitted from, and the morphology of, p-type porous silicon 总被引:1,自引:0,他引:1
The temperature at which silicon is electrochemically etched has been found to influence the structure and photoluminescence properties of porous silicon. Decreasing the temperature increased both the current efficiency of the dissolution process and the porosity of the resulting porous layer. Furthermore, a blue-shift was observed in the photoluminescence indicating that the decreased temperature allowed smaller nanocrystals to be formed. An analysis of temperature dependence of the pore initiation and propagation models currently available in the literature failed to yield a satisfactory explanation for the decrease in the average size of the nanocrystals indicated by the results presented in the present paper. Therefore it was proposed that at lower temperature smaller nanocrystals are stabilized due to a combination of their reduced solubility and the increased viscosity of the diffusion layer that leads to a higher localized concentration of silicon ions, thereby allowing smaller nanocrystals to be in equilibrium with their surroundings. The fact that previous authors did not observe blue-shifting highlights the importance of the composition of the etching solution in controlling the quality of the porous silicon produced. 相似文献
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3-溴噻吩的合成及其在有机合成中的应用 总被引:2,自引:0,他引:2
3 -溴噻吩是一种重要的有机化工中间体 ,它的合成主要通过还原和异构化这两个方面的作用来实现。它的用途主要用于噻吩聚合物的合成。以 3 -溴噻吩为原料可合成 3 -( 6-溴己基 )噻吩 ,也可合成 3 -己基噻吩 ,再以后者为原料 ,合成不同的噻吩聚合物。它的用途将更加广阔。 相似文献
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《Ceramics International》2023,49(20):33057-33072
The temperature stability and temperature stability range of barium titanate-based pulse energy-storage ceramics were modified by Bi2O3 tailoring in (Ba0.98-xLi0.02Bix) (Mg0·04Ti0.96)O3 (x = 0, 0.025, 0.05, 0.075, 0.1) and (Ba1.03-1.5xLi0.02Bix) (Mg0·04Ti0.96)O3 (x = 0.125, 0.15, 0.2, 0.25) ceramics. Excellent pulse energy-storage performances of ceramic films are achieved via the new dual priority strategy of establishing cationic vacancies and forming a liquid phase. The dielectric constant plateau appears due to the cubic phase and space charges. Outstanding temperature stability, frequency stability and antifatigue performance are obtained in the ceramics, and their variations are all less than 15%. The comprehensive energy-storage properties with dual priority parameters of energy-storage density and efficiency of 3.13 J/cm3 and 91.71%, accompanied by an excellent pulse discharge energy density of 2.48 J/cm3, current density of 1313.23 A/cm2 and power density of 195.26 MW/cm3 are gained at x = 0.1. The perfect pulse energy-storage performances as well as ultrahigh stability are correlated with synergistic effects of multiphase coexistence, cubic phase, liquid-phase sintering, grain size, ceramic resistance, space charges and polar nanoregions. The comprehensive parameters indicate that the (Ba0·88Li0·02Bi0.1) (Mg0·04Ti0.96)O3 ceramics have potential application in high precision fields. 相似文献
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本文用Brabender塑化仪,双锟开炼机研究了刚性有机粒子对PVC/CPE共混体熔融塑化为及力学性能的影响,探讨了不同加工温度对PVC/CPE共混体力学性能的影响,实验表明:添加少量刚性有机粒子后,体系的塑化时间缩短,塑化行为改善,韧性有较大幅度提高,拉伸强度有所改善,加工温度为160-180℃体系性能最好。 相似文献
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Yazhu Dong Zhiyong Zhou Ruihong Liang Xianlin Dong 《Journal of the American Ceramic Society》2022,105(2):1558-1567
Phase structure has a strong influence on the temperature stability of ceramics; however, their influence on BiScO3-xPbTiO3 has been neglected. To meet the requirements for practical applications, (0.98-x)BiScO3-xPbTiO3-0.02Bi(Sn1/3Nb2/3)O3 (BS-xPT-BSN, 0.59 ≤ x ≤ 0.65) polycrystalline ferroelectrics with rhombohedral phase, morphotropic phase boundary (Cm and P4mm coexisting), and tetragonal phase has been prepared and studied. The relationship between the phase structures and temperature stability is established from the macro properties as well as the underlying domain behaviors. The results show that the tetragonal phase is not sensitive to temperature because of its stable domains, which is a positive motivator for improving the temperature stability of ceramics. This work provides a new strategy for the design of high-temperature piezoelectric ceramics in the future. 相似文献
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分散剂对纳米四氧化三铁磁流体稳定性的影响 总被引:3,自引:0,他引:3
通过球磨手段,经表面活性剂表面处理颗粒,制备稳定分散纳米四氧化三铁磁性液体。选择表面活性剂GD-01、GD-02和GD-03,研究了溶液pH、球磨时间和表面活性剂用量对磁性液体分散性的影响,采用红外光谱分析仪(FT-IR)和高分辨透射电子显微镜(HRTEM)表征磁性液体中的颗粒。结果表明: GD-02的最佳pH为4.5,GD-01和GD-03的最佳pH为2.5,最佳球磨时间皆为5 h,最佳表面活性剂为GD-02,其最佳用量为0.5 g左右,此时颗粒表面形成稳定的吸附双电层结构,通过静电位阻和空间位阻作用,阻止颗粒团聚,制得分散性能很好的纳米磁性液体。 相似文献
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《Ceramics International》2023,49(16):26834-26846
Transparent glass ceramic with Ba2NaNb5O15 as the main crystal phase was prepared, and the appropriate heat treatment condition was selected as 710 °C/150 min through various characterizations. The luminous intensity and thermal stability were enhanced significantly when the glass ceramic was used as the luminous matrix. After introducing Ti4+ ions as charge compensators, the luminescence performance and thermal stability were further improved, and the reasons for this were analyzed. At 458 K, the luminous intensity of 0.5%Eu3+ doped glass ceramic containing 0.5%Ti4+ can maintain about 65% of room temperature with a chromaticity shift of 5.16 × 10−2. The relative and absolute sensitivities of 0.7%Er3+ doped glass ceramic were 4.04 × 10−3 K−1 and 1.31% K−1. Introducing Ti4+ ions would weaken the population redistribution ability of 2H11/2 and 4S3/2 levels and reduce the temperature sensitivity. However, the sample containing Ti4+ shows good thermal stability, its green emission at 458 K has a small chromaticity shift of 6.45 × 10−3. The research shows that the glass ceramic can be used as a good luminescent host material, and Eu3+/Er3+ doped glass ceramic can be used in the fields of LEDs or temperature sensing. 相似文献