Analysis of tribological feature of the oxide scale in hot strip rolling

In this paper, the effects of the flow stress of the scale and steel, and the friction coefficients at the scale-steel and the roll-scale interfaces on the final surface roughness have been studied. The surface roughness increases for both oxide scale and steel with an increasing friction coefficient at the roll-scale interface. However, the roughness increment is limited. The calculated roughness is close to the measured value. The temperature affects the scale roughness transfer, and the maximum difference is about 25% when the temperature is 850-1025 °C for rolling speeds 0.12-0.72 m/s. The developed model is applicable in hot strip mills.     

Modeling of anisotropic plastic behavior of ferritic stainless steel sheet

Modeling of anisotropic plastic behavior of ferritic stainless steel sheet (Type 409) was investigated using the three yield functions of Hill [A theory of the yielding and plastic flow of anisotropic metals. Proceedings of Royal Society of London, Series A 1948;193:281–97.], Barlat and Lian [Plastic behavior and stretchability of sheet metals. Part I: A yield function for orthotropic sheets under plane stress conditions. International Journal of Plasticity 1989;5:51–66] and Barlat et al. [Plane stress yield function for aluminum alloy sheet. Part I: Theory. International Journal of Plasticity 2003;19:1297–319.] (referred to as Yld2000-2d) criteria. Mechanical behaviors were characterized based on uniaxial tension, balanced biaxial bulge, and disk compression tests. Directionalities of yield stresses and r values were predicted from the three criteria and compared with experimental results. In order to verify the modeling accuracy of the three functions under complex loading conditions, cylindrical cup drawing and limiting dome height tests were carried out numerically and experimentally. It has been demonstrated that the result from Yld2000-2d criterion exhibits good agreement with experimental data. The effects of anisotropic hardening on earing and necking were also investigated based on the different levels of plastic work.     

Study on the oxidation of stainless steels 304 and 304L in humid air and the friction during hot rolling

In rolling process, the contact friction is of crucial importance for accurate modeling, optimum design and control of industrial rolling processes. It is important to characterize the features of the oxide scale of stainless steel in hot strip rolling because the scale on the strip surface affects friction coefficient and thermal conductivity coefficient. To some extent, the rolling force and friction condition depend on the thickness and the microstructure of the oxide scale. Oxidation tests of stainless steels 304 and 304L were carried out in a high temperature electric resistance furnace. The humid air in which the water vapour content can be controlled was generated and remained to flow into the chamber of the furnace in 2.5 × 10⁻⁴ m³/s to study the effect of humidity on the oxidation of stainless steels. The microstructure and thickness of oxide scale layer of stainless steels were obtained and two or three oxide layers can be found. The humid air has a significant effect on the growth of oxide scale. Hot rolling tests were carried out on Hille 100 rolling mill. The friction condition at the roll–strip interface during hot rolling of stainless steel was determined and the transfer of surface roughness was discussed.     

Analysis of the friction and wear behavior of hot work tool scale: application to the hot rolling process

In hot forming processes, the interface tool/product is important for the quality of the finished product. In hot rolling, the scale formed on the roll material plays an essential role. As soon as the contact oxide–oxide is established between the roll and the slab, friction allows the process to start. However, the oxide scale will continue to grow under the cyclic action of hot contacts and water cooling and will be subjected to thermo-mechanical stresses. Beyond a certain critical thickness, the oxidized surface layer of the cylinders has not sufficient mechanical strength to withstand the shear stresses.

The wear and friction behavior of the oxides appearing on the surface of the hot working rolls is not well known. The influence of these oxides on the friction and, consequently, the quality of the products of finishing mills, seems very significant. So, in this study, we investigate the evolution of the friction coefficient and the wear, according to the growth, the nature and the thickness of the formed scale. We use a high temperature pin on disc tribometer. The pin consists of material “rolls” while the disc consists of the slab. The pin is instrumented with thermocouples in order to couple the friction coefficient measurements with the thermal gradient in the pin and the surface temperature and the formed oxides. Then, the characterization of the surfaces is done by scanning electronic microscopy (SEM) and EDS analyses. We use the method of sin² Ψ to evaluate residual stresses of oxide and correlate these data with shear stress behavior.     

The microstructure and wear behaviour of friction stir processed AISI 430 ferritic stainless steel

ABSTRACT

The microstructure and wear behavior of Friction Stir Processed (FSPed) AISI 430 ferritic stainless steel were analyzed in the present study. FSP was performed with a tool rotation and advancing speeds of 1400?rpm 16?mm/min respectively by employing a tungsten carbide tool. The FSPed microstructure consisted of a mixture of ferrite and martensite. After FSP, microhardness increased with respect to that of the as-received material. The wear resistance of the FS processed material was significantly enhanced if compared to that of the as-received substrate. According to the SEM analyses of the worn surfaces and wear debris, a combination of adhesive wear and delamination was observed in the case of the base metal. The wear mechanism shifted to mild adhesive wear after FSP. The superior wear resistance of the FS processed AISI 430 steel was attributed to the pronounced grain refinement and to martensite formation in the stir zone.     

Mechanical and metallurgical properties of friction welded AISI 304 austenitic stainless steel

Owing to the superior properties, of stainless steel it is pertinent to make use of it in various automotive, aerospace, nuclear, chemical and cryogenic applications. It is observed that a wide range of dissimilar materials can be easily integrated by solid phase bonding techniques, such as friction welding and explosive bonding. This study mainly focuses on friction welding of AISI 304 austenitic stainless steel. The friction processed joints are evaluated for their integrity and quality aspects. Friction welding of austenitic stainless steel was carried out using a KUKA friction welding machine (Germany). As the friction time increased, the fully plastically deformed zone (region I) in the vicinity of the bond line becomes increased. In contrast, an increase in friction time will decrease the region (region II) where the grains are partly deformed and grown. Tensile test results indicated that, the joint strength is decreased with an increase of the friction time. The detailed fractographic observation confirmed that the rupture occurred mostly at the joint zone and partly through the base material.     

Integration of batching and scheduling for hot rolling production in the steel industry

This paper investigates the hot rolling production scheduling problem in the steel industry and proposes a new mixed integer programming model for this problem based on the monolithic modeling strategy that integrates batching and scheduling. Using this strategy, the new model can simultaneously schedule multiple turns and simultaneously determine the production timetable of these turns in a global optimal view. A long-term tabu search heuristic using frequency-based memory is developed to obtain near-optimal solutions for this problem. Three kinds of speed-up strategies are developed to accelerate the search procedure of the proposed tabu search. A practical scheduling system combining the proposed mathematical model and the tabu search heuristic has been developed and tested on instances collected from practical production data. The experimental results show that the proposed mathematical model and the tabu search heuristic outperform both the current manual scheduling method and the traditional serial method.     

Effects of entraining velocity of lubricant and sliding velocity on friction behavior in stainless steel sheet rolling

A series of experiments was carried out using a rolling-type tribometer to investigate the effects on friction behavior of the entraining velocity of the lubricant at the inlet to the contact zone (V) and sliding velocity during deformation (ΔV). Experiments with stainless steel sheets of two different surface roughnesses showed that the variations in the friction coefficient with entraining velocity V and sliding velocity ΔV are largely dependent on the initial surface texture of the workpiece. For a smooth workpiece, the friction coefficient decreases with increasing sliding velocity ΔV but keeps almost constant with increasing entraining velocity V. However, for a rough workpiece, the friction coefficient initially decreases slowly and increases largely with increasing sliding velocity ΔV or decreasing entraining velocity V. Observation of the rolled surface for a smooth workpiece shows that, with increasing entraining velocity V, the slip band becomes more marked, and with increasing sliding velocity ΔV, the rubbed portions become more conspicuous. For a rough workpiece, galling occurs at high sliding velocity ΔV. The critical condition for galling outbreak is shown on the V-ΔV graph. The galling outbreak process is observed by interrupting the rolling process.     

Rolling and sliding: Separation of adhesion and deformation friction and their relative contribution to total friction

This study is concerned with determining the relative contribution of adhesion and deformation friction using rolling and sliding method. The challenges associated with in-vivo friction testing were overcome by utilising a novel substrate that mimics the viscoelastic behaviour and surface texture of human skin combined with a repeatable and reproducible test setup. The results show that in the dry state, deformation friction contributes 20% of the total friction while the remaining proportion is due to adhesion. These proportions are affected by probe material where for PTFE, deformation friction contributes 30% of the total friction. For the lubricated state, the contribution of deformation friction to total friction increases approaching 50–50% at the higher sliding speeds and normal loads investigated.     

不锈钢管接头精密成形的工艺分析与实验研究

不锈钢管接头截面积变化大，成形和脱模困难。本文对其塑性加工工艺方案进行分析比较，并通过工艺实验，验证工艺分析结果。该零件采用温挤压成形可以获得较好的技术经济效益；一次正挤压效率高，工艺力大；正挤-镦粗复合工艺则工艺力小，但效率较低。     

316LN不锈钢低速率应变下的热变形行为

目前, 对316LN不锈钢在低速率应变下的热变形行为研究很少. 本文选用工业316LN不锈钢, 通过Gleeble-3800热模拟试验机进行了600-1 100 ℃温度下, 应变速率为3×10-3 s-1的热压缩试验, 得到了真应力-应变曲线. 通过分析真应力-应变曲线和试样的微观组织, 得到了如下结论: 1 000 ℃和稍高温度是适于低速率应变下316LN不锈钢加工的温度.     

Energy conservation in stainless steel cold rolling applications

In order to predict the performance of rolling oils in actual production mills, from tests in laboratory mills, the influence of various factors, such as shape factors work roll diameter (D), strip thickness (h₁), operating conditions (reduction rate (r), peripheral velocity of roll (U₀), strip velocity (U₁)) and kinematic viscosity of the rolling oil (υ₀) was investigated. A parameter RLI (Rolling Lubrication Index = u₀(U₀+U₁)(1−r)(D/2h₁.r)^½) was found to be useful in predicting lubricating conditions in actual production mill applications. The coefficients of friction of mineral oils, some synthetic hydrocarbons including polybutene, and several kinds of additives were obtained from laboratory mills under the same condition of RLI value as that for finish rolling in actual production mills. With hydrocarbons, paraffins showed the lowest coefficient offriction, while aromatics exhibited a higher coefficient of friction, with naphthenes showing the highest. A high-quality rolling oil was formulated using a combination of ester and paraffinic mineral oil. It is observed that this new oil can save 14% of energy consumed by a laboratory mill compared with conventional rolling oils. In production mills, nearly the same energy conservation level can be achieved.     

不锈钢垫片的磨削加工

介绍了组合砂轮磨削不锈钢垫片时砂轮对加工表面质量和磨削力的影响。     

The representative topography of worn hot rolling mill cylinders

In this paper, a method is proposed to extract the most representative surface topography from n surfaces. A criterion is proposed that allows rejecting irrelevant topographical maps. Then, this methodology is applied on the hot rolling process, on replicas of industrial surfaces. These analyses have shown the major difference between ICDP and HSS roll behavior in terms of topography. Carbides oxidation observations correlates lab studies from bibliography. We confirm that this methodology is relevant to industrial investigations, especially on phenomena requiring non-destructive protocol.     

Near-net-shape forming of 316L stainless steel powder under hot isostatic pressing

Near-net-shape forming of 316L stainless steel powder is investigated under hot isostatic pressing (HIPing). A stainless steel powder compact and an insert were encapsulated by a stainless steel container and hot isostatically pressed to produce an axisymmetric near-net-shape part. To simulate densification and deformation of a powder compact in the container during HIPing, the constitutive model of Abouaf et al., and that of McMeeking and co-workers were implemented into a finite element analysis. The thickness effect of the container on densification was also studied for the axisymmetric part during HIPing. Densification of a three-dimensional asymmetric part during HIPing was also investigated by comparing finite element calculations with experimental data by Eisen et al.     

EBSD investigation of the microstructure and texture characteristics of hot deformed duplex stainless steel

The microstructure and crystallographic texture characteristics were studied in a 22Cr‐6Ni‐3Mo duplex stainless steel subjected to plastic deformation in torsion at a temperature of 1000 °C using a strain rate of 1 s^?1. High‐resolution EBSD was successfully used for precise phase and substructural characterization of this steel. The austenite/ferrite ratio and phase morphology as well as the crystallographic texture, subgrain size, misorientation angles and misorientation gradients corresponding to each phase were determined over large sample areas. The deformation mechanisms in each phase and the interrelationship between the two are discussed.     

Tribological performances of Zn-based coating in direct hot stamping

In hot stamping of High Strength Steels, the severe tribological conditions make the metal sheet coating one of the most critical choices for the technical and economical success of the process. This paper presents the approach and the results in evaluating a Zinc-based coating applied to boron steel sheets in hot stamping operations. Thermal and physical-simulation experiments were carried out to evaluate the chemical interactions between the coating and the metal sheet and the tribological performances during the process. The coating proved to overcome most of the drawbacks of the currently utilized Al–Si coating.     

Mechanical behaviour of iron oxide scale: Experimental and numerical study

The paper addresses the identification of constitutive parameters of thick, brittle layers on metal substrates. Application is to the iron oxide behaviour during hot rolling processes of steel, where oxide scale breaking and embedding is one of the major causes of surface defects. Contact management of a FEM software has been adapted in order to address the transitions corresponding to transverse oxide fracture, along with two other mechanisms, namely delamination and interfacial stick/slip. It is applied to the hot strip rolling process to show pre-bite cracking and its consequences (“micro-extrusion” of the metal). To approximate the stress state prevailing at roll bite entry, the Four-Point Hot Bending Test (4PHBT) has been selected for the measurement of oxide properties. Oxidation is made in situ in the test rig under conditions similar to a hot strip mill (HSM) environment. Comparison of load-deflection curves for oxidized and non-oxidized samples allows the mechanical properties of the oxide to be determined. Above a critical temperature T_c - around 700 °C, but depending on strain rate - the oxide is ductile (with a very narrow plastic strain range, ?_p < 10⁻²) and elastic-viscoplastic (EVP) constitutive parameters are identified numerically. Below T_c, brittleness is manifested by an array of transverse, through-thickness cracks. Acoustic emission (AE) has been used to help detect the onset of fracture, while numerical simulation gives the critical fracture stress at the corresponding point of the load-deflection curve. Results for four low carbon steel grades are compared.     

有机硅涂层对316不锈钢的防护

研究了316不锈钢在高温（400℃）盐和水蒸气综合作用下的腐蚀行为及添加Al粉和Ti粉的有机硅涂层对不锈钢的防护作用。结果表明，316不锈钢裸样发生了较为严重的腐蚀。刷涂了有机硅涂层的316不锈钢在相同的条件下没有发生腐蚀，涂层对316不锈钢具有优异的防护作用．讨论了有机硅涂层的防护机理。     

Evaluation of intragranular misorientation parameters measured by EBSD in a hot worked austenitic stainless steel

An extensive characterization of hot deformed austenitic stainless steel was carried out using the electron backscatter diffraction technique. Special emphasis was given to the misorientation parameters related to different length scales. These parameters show a behaviour that is sensitive to the amount of applied strain and also lead to increasing values for both the strain and the scale length.
At the same time, the use of different thresholds and scan steps in the evaluation of the parameters were analyzed in order to assess the validity of the results.