Bending properties of hollow super-elastic Ti–Ni alloy wires and compound wires with other wires inserted

The purpose of this research was to investigate the possible orthodontic application of the hollow super-elastic Ti–Ni alloy wire, which was thought not only to deliver much lower and more continuous orthodontic force than conventional Ti–Ni wires, but also be able to be applied as a compound wire when combined with another wire. The examinations of bending properties were performed by the three-point bending test. The following results were obtained. 1. The hollow wire had lower load in the super-elastic range, smaller load-deflection rate and stress hysteresis in comparison with the conventional wire of the same diameter. 2. The load of the hollow wire was controllable by heat treatment. The stress hysteresis was further decreased by a two-step heat treatment. 3. The compound wire formed by inserting other types of wires into the hollow core exhibited changes in various bending properties such as increased load or load-deflection rate, according to the types and diameters of the inserted wire. The hollow wire delivers much lighter and more continuous orthodontic force, and, through heat treatment or deployment as a compound wire, it is possible to alter various bending properties. Therefore, this hollow wire was evaluated as a promising candidate for orthodontic application.     

Force‐deflection behaviour of NiTi archwires in a polytetrafluoroethylene (Teflon) bracket system

In orthodontic treatment, archwire forces for tooth movement is influenced by the magnitude of friction encountered during the sliding motion of archwire along the bracket slot. Friction will reduce the archwire force, and subsequently modify the constant force delivery trend into a slope. The aim of this work is to investigate the force‐deflection behaviour of nickel‐titanium (NiTi) shape memory alloy archwire on polytetrafluoroethylene (Teflon) as the bracket. Sliding tests was performed to determine the coefficient of friction of polytetrafluoroethylene‐NiTi material combinations. The force‐deflection behaviour was evaluated from a modified bending tests, at two different configurations; commercial stainless‐steel bracket and hand‐made polytetrafluoroethylene bracket. During test, wires were deflected into different deflections (2 mm, 3 mm and 4 mm) by using four commercial NiTi archwires at different sizes and geometry. From the test; coefficient of friction for polytetrafluoroethylene‐NiTi wire was recorded as small as 0.07. On force‐deflection graphs, bending load on 3 mm and 4 mm deflection were observed higher on stainless steel (SS) bracket compared with polytetrafluoroethylene bracket. Due to small coefficient of friction on polytetrafluoroethylene‐NiTi configuration, the NiTi archwire exhibited the activation and deactivation force within the plateau limit. Greater friction on stainless steel‐nickel‐titanium bracket configuration causes wire to release force in a slope trend. This finding highlights the potential of polytetrafluoroethylene as a material in the bracket slot to minimize friction during orthodontic treatment.     

Force-deflection behavior of NiTi archwire at different configurations of bracket system

NiTi shape memory alloy archwire is widely used in orthodontic treatment, replacing stainless steel for the flat and low deactivation force it can offer. However, the presence of friction at the contact region of wire and bracket may cause the low deactivation force to be ineffective to induce tooth movement. This work evaluated the bending deformation behavior of NiTi archwire in application using conventional orthodontic stainless steel bracket in levelling treatment. Experimental test rig was developed to perform three-brackets bending test at room temperatures (27 °C). The bracket used was 0.022-in stainless steel and the archwire was 0.016-in NiTi round wire. Fabricated polytetrafluoroethylene (Teflon) bracket was used as a control experiment to represent frictionless condition of deformation on three-bracket bending. Additionally, elastomeric ligature was also used to evaluate the effect of friction produced by the elastomer. Bending tests were done at 3 different deflection magnitudes of 2 mm, 3 mm and 4 mm. The results show that bending deformation behavior of the wire on frictionless Teflon bracket produced a flat force plateau on both activation and deactivation. On the other hand, when stainless steel brackets were used, the force plateau exhibited positive gradient on the activation and negative gradient on the deactivation.     

Phase transformation behavior and wire drawing properties of Ti-Ni-Mo shape memory alloys

Transformation behavior and wire drawing properties of Ti-Ni-Mo shape memory alloys have been investigated by means of differential scanning calorimetry (DSC) measurements, X-ray diffraction, electron microscopy, tensile tests and wire drawing tests. Mo addition to a Ti-Ni binary alloy induced the R phase transformation, and consequently Ti-Ni-Mo alloys showed two stage transformation, i.e., from the B2(cubic) parent phase to the R(rhombohedral) phase, and then from the R phase to B19(monoclinic) phase. In the thermo-mechanically treated 51Ti-48.3Ni-0.7Mo alloy, reverse transformation temperature, Af, kept constant, irrespective of thermo-mechanical treatment conditions, while it changed in the thermo-mechanically treated 51Ti-49Ni and 51Ti-48.5Ni-0.5Mo alloys. Mo addition to Ti-Ni binary alloy decreased wire drawing stress. Wire drawing stress decreased with raising intermediate annealing temperature monotonously when the annealing treatment was made in vacuum. When the annealing treatment was made in air, however, it decreased with raising annealing temperature up to 923 K, and then increased. Optimum intermediate annealing temperature of Ti-Ni-Mo alloys for wire drawing was 823 K, above which a thick oxide film which reduced the drawability of the alloys was formed on the surface of alloy wires.     

Experimental investigation on the debonding strength in shape memory alloy wire reinforced polymers

The interfacial shear strength between the shape memory alloy (SMA) wire and epoxy matrix was evaluated experimentally using a single wire pull-out test. Moreover, the effect of pre-strain in SMA wires on the interfacial behavior was studied by pre-straining the SMA wires to 2% and 4% pre-strains. Experiments were conducted in both martensite and austenite phases of SMA. Results showed that pre-straining SMA wire in the martensite phase caused enhancement in interfacial shear strength due to recovery force generation. Further, 9.7% and 33% improvements in the interfacial shear strength were achieved at 2% and 4% of SMA pre-strain, respectively. However, the enhancement of interface behavior did not occur, when the SMA wires were subjected to pre-strain in the austenite phase.     

Pass schedule of wire drawing process to prevent delamination for high strength steel cord wire

The high-speed drawing of high carbon content steel wires is usually conducted at room temperature employing a number of passes or reductions through several dies. In the multipass drawing process, the temperature rise at each pass affects the mechanical properties of the final product (such as its bending and torsion properties, and its tensile strength). This temperature rise during deformation encourages delamination in the wire, which has a deleterious influence on the torsional properties and durability of the wire. In this study, we investigated the delamination of wires using torsion tests and evaluated the wire temperature during drawing. Our data shows that one of the main reasons for delamination was an excessive rise in wire temperature. Based on our experimental results, in order to prevent delamination due to an excessive rise in wire temperature, a new isothermal pass schedule that could control the wire temperature was designed. The pass redesign for the conventional high carbon (0.75 wt%C) steel cord wire drawing process with delamination was carried out by using the isothermal pass schedule to control the wire temperature. In order to verify the effectiveness of the proposed method, wire drawing and torsion test were conducted. From the results of experiments, it was possible to produce high carbon steel cord wire without delamination.     

A practical in situ wire: a composite wire with many in situ processed Nb3Sn cores of an internal diffusion type

As a superconducting in situ wire for practical use, we propose a new type of composite wire with fine cores consisting of in situ processed wires of an internal diffusion type. These Nb₃Sn wires have merit in a simple fabrication process and a high stability compared with ordinary multifilamentary Nb₃Sn wires. Expected properties of the new type of Nb₃Sn wires were estimated based on a series of experimental results for a single in situ Nb₃Sn wire used as a fine core. A quantitative reliability of the new design estimation was examined by comparing the theoretical values with observed data on the electromagnetic properties of a test wire.     

绳锯线弓角静态测量方法的研究

金刚石绳锯在切割圆弧板材时,受到进给方向的阻力,形成"线弓角",使板材中部产生"过切",严重时导致材料报废.为解决这一问题,提出了线弓角的概念,从理论上提出了一种基于悬臂式力传感器的绳锯线弓角的静态测量方法,通过轴力传感器输出的电压值计算出线弓角度.试验在自行设计和搭建的绳锯线弓角测量平台上进行,用钢丝绳模拟串珠绳产生线弓角,并进行导轮受力与线弓角关系的静态测量试验分析,以验证该方法测量线弓角的可行性.试验结果表明:在一定范围内,串珠绳初始张紧力越大,线弓角的计算值越接近理论值.因此,采用所提出的测量方法,当装有轴力传感器的导轮处在刚好与钢丝绳接触的状态下,选择合适的初始张紧力,可以测得较准确的角度值.     

Comparison between solid and hollow reinforced concrete beams

Comparison between test results of seven hollow and seven solid reinforced concrete beams is presented. All of the fourteen beams were designed as hollow sections to resist combined load of bending, torsion and shear. Every pair (one hollow and one solid) was designed for the same load combinations and received similar reinforcement. The beams were 300 × 300 mm cross-section and 3,800 mm length. The internal hollow core for the hollow beams was 200 × 200 mm creating a peripheral wall thickness of 50 mm. The main variables studied were the ratio of bending to torsion which was varied between 0.19 and 2.62 and the ratio in the web of shear stress due to torsion to shear stress due to shear force which was varied between 0.59 and 6.84. It was found that the concrete core participates in the beams’ behaviour and strength and cannot be ignored when combined load of bending, shear and torsion are present. Its participation depends partly on the ratio of the torsion to bending moment and the ratio of shear stress due to torsion to the shear stress due to shear force. All solid beams cracked and failed at higher loads than their counterpart hollow beams. The smaller the ratio of torsion to bending the larger the differences in failure loads between the hollow and solid beams. The longitudinal steel yielded while the transverse steel experienced lower strain values.     

Metallurgical Investigation of Failed Locked Coil Track Ropes Used in a Mining Conveyor

A locked coil track rope (LCTR) is essentially composed of wires (round and rail-shaped) laid helically in different layers. These wire ropes are sometimes used in conveyors carrying empty and loaded buckets in mining areas. During service, such wire ropes may fail prematurely due to disintegration/failure of individual groups of wires. To understand the genesis of LCTR wire failures, a detailed metallurgical investigation of failed rope wires was made and included visual examination, optical microscopy, scanning electron microscopy (SEM), and electron probe microanalysis (EPMA). Two types of failed wires were investigated; one is from a 40 mm diameter locked coil track rope and the other from a 53 mm locked coil track rope. Optical microscopy of failed round wires in the 53 mm diameter rope clearly revealed fully decarburized layers at the surface and a few grain-boundary cracks. From the location of the failure, it was clear that apart from static tensile loads, the wire ropes had been subjected to bending and unbending loads near the saddle, as fully loaded or empty buckets traveled access the conveyor. The SEM studies confirmed that the fracture had been caused by initiation of fatigue cracks in the decarburized zone under conditions of repeated bending and unbending stresses superimposed on the static tensile load.     

Phase transitions in coated nickel titanium arch wires: A differential scanning calorimetric and X-ray diffraction analysis

Shape memory and super-elastic properties of orthodontic nickel titanium wires, which are crucial for its clinical performance are dependent on the austenitic–martensitic phase transitions in its metallic microstructure that happen as a result of temperature or stress. The objective of this study was to compare the austenitic–martensitic phase transitions in new, black oxide coated nickel titanium (0·016 inch, Black Diamond, NiTi) arch wires in the ‘as-received’ form, from the manufacturer and ‘retrieved form’ after two months of intraoral use. This was done to analyse whether the new oxide coated nickel titanium wires suffered any significant loss in shape memory and super elasticity properties at the end of two months of intra oral use, findings of which could give valuable inferences prior to its widespread application in clinical practice. Five arch wire samples in both groups were investigated for their austenitic–martensitic phase transitions in an in vitro set up, using differential scanning calorimetry (DSC), (?90° to 100°C at a rate of 10°C/min) and X-ray diffraction (XRD) analysis (10° to 90°), as a function of temperature. Martensitic–austenitic thermograms showed an intermediate rhombohedral phase in the heating cycle of both groups, but cooling cycles showed direct reversal from austenitic to martensitic phase. Lower austenitic start ( $A_{\rm \textbf{s}}$ = 10·78 ± 0·46°C) and finish ( $ {A}_{\rm \textbf{f}}$ = 22·26 ± 0·24°C) temperatures of coated wires compared to the conventional wires showed (i) ability of the wire to remain in austenitic phase below oral temperature, that permits it to take up greater force during activation, (ii) increased springiness and (iii) consistent force delivery for an extended period of time. Statistical analysis with paired Student’s ‘t’ test did not show any significant difference in mean values of transition temperatures and enthalpies between the two groups which proved similar shape memory and super-elastic properties at the end of intra oral use. Black oxide coating of NiTi wires may, therefore, be effective in diversified oral conditions and may find acceptable for re-use after sterilization. Low enthalpy values (0·92–3·59 j/g) compared to conventional ones, implied complete phase transition at the atomic level that can improve performance of the material in activation and deactivation cycles of NiTi wires. X-ray diffraction analysis of the two groups demonstrated predominance of austenitic phases (A, 110, 220 and 211) with complete reversibility at the atomic level. Discrete crystallographic structure and absence of multiple phases showed complete martensitic–austenitic transition, which authenticated the differential scanning calorimetric findings. This can earn acceptance for the new product in contemporary orthodontic practice with adequate scope for indigenization.     

Wire tensions and bending moments in axially loaded seven wire strand

Carefully instrumented tensile tests were performed on a straight single steel strand of seven-wire construction having core and helical wire diameters of 3–66 mm and 3–33 mm, respectively, and a lay angle of 14-6. Strain gauges in groups of three with their grid axes parallel and having a common backing were attached to all six helical wires at the mid-strand position. For loading within the linear range of the load-extension response (all tests) and load-rotation response (in tests with free and partial torsional restraint of the ends) the outputs from these strain gauges were used to compute wire tensions and bending moments. Strand extension, rotation and torque generated under axial load (fixed-end and partial torsional restraint) were also recorded.
Test results showed that the share of the total strand load taken by the helical wires decreased as the torsional restraint on the strand was reduced. The mean tension in the helical wires was found to be 27-5% smaller in the free-end tests than in fixed-end tests for a given strand load. Theoretical predictions underestimate this reduction in tension by up to 80%. Bending moments in the wires were found to be about 8% less than predicted in the fixed-end condition and over 20% smaller in the free-end condition.
As expected, the slope of the linear regions of the load-extension and load-rotation plots decreased as the torsional restraint was reduced. However, the rate of decrease in the case of load-extension plots was found to be less than predicted theoretically and the rotation measured was generally less than predicted theoretically. This is consistent with the helical wire tensions being smaller than the predicted values since the tangential components of these reduced tensions would have less effect in their unwrapping action on the strand under increasing axial load.     

Stress transmission through Ti-Ni alloy, titanium and stainless steel in impact compression test

Impact stress transmission of Ti-Ni alloy was evaluated for biomedical stress shielding. Transformation temperatures of the alloy were investigated by means of DSC. An impact compression test was carried out with use of split-Hopkinson pressure-bar technique with cylindrical specimens of Ti-Ni alloy, titanium and stainless steel. As a result, the transmitted pulse through Ti-Ni alloy was considerably depressed as compared with those through titanium and stainless steel. The initial stress reduction was large through Ti-Ni alloy and titanium, but the stress reduction through Ti-Ni alloy was more continuous than titanium. The maximum value in the stress difference between incident and transmitted pulses through Ti-Ni alloy or titanium was higher than that through stainless steel, while the stress reduction in the maximum stress through Ti-Ni alloy was statistically larger than that through titanium or stainless steel. Ti-Ni alloy transmitted less impact stress than titanium or stainless steel, which suggested that the loading stress to adjacent tissues could be decreased with use of Ti-Ni alloy as a component material in an implant system. ©2000 Kluwer Academic Publishers     

基于虚轴法的三维数控弯丝机控制系统设计

三维数控弯丝机在弯制工件时不仅需要对各轴进行精确的位置控制,还需要对多轴进行位置的同步控制,而其同步控制的好坏将直接影响到工件成形质量．为提高三维数控弯丝机的位置同步控制精度,应用西门子Simotion C240为运动控制器,采用位置闭环控制方案,针对旋转式三维数控弯丝机进行了控制系统设计．在该控制系统基础上,通过采用虚拟轴同步控制策略的方法,对弯丝机多轴位置同步控制进行了实验,根据实验得到的多轴同步的实际运行曲线,对测试结果进行了分析．实验表明,与其他同步控制策略相比,基于虚拟轴同步控制策略的弯丝机控制系统同步控制精度高,稳定性好,满足工件加工的同步控制要求．     

双轴压弯作用下RC桥墩矩形空心截面性能评价

针对双轴压弯作用下钢筋混凝土(RC)空心截面性能评价问题,该文根据双轴压弯作用下RC矩形空心截面中和轴布置的不同形式,推导了双轴压弯作用下其承载力计算公式和曲率计算公式。对双轴压弯作用下轴压比、配筋率和配箍率不同的3个RC矩形空心截面试件体桥墩的墩底控制截面,进行了承载力和转动延性分析,得出其在给定轴力作用下的M_x-M_y曲线和弯矩-曲率曲线,并通过其双轴压弯循环荷载试验,验证了分析结果的正确性和精确性。在此基础上,对一连续刚构桥梁的RC矩形空心桥墩的承载能力、截面转动延性以及相关参数进行了分析。结果表明,双轴压弯作用下两主轴方向弯矩耦合作用降低了截面的极限承载能力,单轴压弯作用的截面设计对结构是偏于不安全的;随中和轴与某一轴夹角的增大,该轴极限弯矩和曲率逐渐减小,而沿另一主轴方向的极限弯矩和曲率逐渐增大,但均小于其强轴方向的极限弯矩和转动曲率,该文的结论可为RC矩心空心截面桥墩的抗震设计和性能评价提供参考。     

Bending property and phase transformation of Ti–Ni–Cu alloy dental castings for orthodontic application

Bending property of Ti–Ni–Cu alloy castings was investigated in a three-point bending test for orthodontic application in relation to the phase transformation. The compositions of the alloys were Ti–50.8Ni and Ti–40.8Ni–10.0Cu (mol %), and four cross-sectional shapes of the specimens were selected. Heat treatment was performed at 713, 753 or 793 K for 1.8 ks. The bending load changed by the cross-sectional size and shape mainly because of the difference in the moment of inertia of area, but the load–deflection relation did not differ proportionally in the unloading process. The difference between the load values in the loading and the unloading processes was relatively small for Ti–Ni–Cu alloy. With respect to the residual deflection, there was no significant difference between Ti–Ni and Ti–Ni–Cu alloys with the same treatment condition. The load values in the loading and the unloading processes decreased by each heat treatment for Ti–Ni alloy; however, the decrease in the load values for Ti–Ni–Cu alloy was not distinct. It is proved that Ti–Ni–Cu alloy castings produce effective orthodontic force as well as stable low residual deflection, which is likely to be caused by the high and sharp thermal peaks during phase transformation.     

Stress dependent electrical resistivity of orthodontic wire from the shape memory alloy NiTi

The aim of this study was to compare and evaluate the stress induced martensitic phase under different loading conditions in orthodontic wire from the Shape Memory Alloy Nickel–Titanium (NiTi). For this purpose we investigated the phase transformation from austenite to martensitic due to the different loading conditions by measuring the electrical resistance which could show the type of deformation which occurs at the beginning of phase transformations. In this framework we developed two special devices for measurements of electrical resistance in different types of load and their combination on the orthodontic wire. These results were compared with the analytically calculated stresses in the orthodontic wire. It was shown that they caused complex or multi-axial stress state phase transformation rather than other more simple load such as uniaxial loading. Finally, the article presents the deformation which occurs at the change of phase that is nearly connected to the useful superelasticity effect of the Shape Memory Alloy NiTi.     

Tensile properties and transformation temperatures of Pd added Ti-Ni alloy dental castings

The effect of palladium (Pd) addition to Ti-Ni alloy as the third element was investigated to improve the super-elasticity of the alloy castings at body temperature for dental application. Ti-50.8Ni (at %) alloy, which exhibited super-elasticity at 310 K in castings, was used for comparison. 5.0, 7.5, 10.0 and 15.0 at % Pd was added to Ti-50.0Ni alloy by the substitution for Ni. The change in the proportion of Ti and Ni was also examined at the fixed Pd addition of 7.5 at %. The properties of the alloys were investigated in tensile test and differential scanning calorimetry (DSC). Ti-42.5Ni-7.5Pd alloy castings showed good super-elasticity among the examined alloys from the viewpoint of residual strain and elongation. Moreover, apparent proof stress could be changeable by the proportion of Ti and Ni with residual strain being kept low. Ti-42.5Ni-7.5Pd alloy castings exhibited better super-elastic flexibility than Ti-50.8Ni alloy, which is proven by lower apparent proof stress and larger elongation. This flexibility appears to be caused by its relatively high martensitic transformation starting temperature point. It is suggested that this flexibility with super-elasticity could widen the clinical application of the alloy casting in dentistry. © 2000 Kluwer Academic Publishers     

Effect of welding wire and groove angle on mechanical properties of high strength steel welded joints

Mechanical properties of high strength steel welded joints strictly depend on the welding process, the filler material composition and the welding geometry. This study investigates the effects of using cored and solid welding wires and implementing various groove angles on the mechanical performance of weld joints which were fabricated employing the gas metal arc welding process. It was found that weld joints of low alloy, high strength steels using low alloy steel cored welding wires exhibited higher tensile strength than that of low alloy steel solid wire and chromium‐nickel steel bare welding wire when the method of gas metal arc welding is employed. The effect of groove angle on the strength and toughness of V‐groove and double V‐groove butt‐joints was investigated. V‐groove joints, with higher tensile strength than double V‐groove joints in the whole range of groove angles, were superior in toughness for small groove angles, but impact toughness values of both joints were comparable for large angles. The effect of heat input and cooling rate on the weld microstructure and weld strength was also investigated by performing thermal analysis employing the commercial software ANSYS. It was concluded that cooling rate and solidification growth rate determined the microstructure of the weld zone which had great consequences in regard to mechanical properties.     

Fabrication of Al thin wire by utilizing controlled accumulation of atoms due to electromigration

A technique of fabricating metallic thin wires by utilizing effective collection of the atoms caused by electromigration, which is a phenomenon of atomic diffusion due to high current density, is presented. Atoms diffused by electron flow can be used for making metallic thin wires. To form metallic thin wire at the intended position, we used passivated Al thin film line that had a slit at the anode end of the line as a test sample. As a result of current applying, the Al thin wire of a high aspect ratio was fabricated.