A comparison of toughness of

The low-temperature toughness of C-Mn weld steel with different grain sizes was investigated with notched and precracked specimens. The results indicated that the fine grain steel, evaluated by notched specimens (Charpy V-notch and 4 point bending specimens), is tougher than that of the coarse grain steel over a temperature range from -196 °C to -30 °C. On the other hand, the coarse grain steel, evaluated with precracked specimens, has a remarkably greater plane strain fracture toughness compared to the fine grain steel. The microstructural analysis revealed that the fracture toughness of both the fine grain and the coarse grain steel is not directly related to the distance of the fracture initiation site from the precrack tip or the size of the ferrite grain. The behavioral discrepancy can be explained in terms of the ratio of local fracture stress to yield stress,i.e., σ _f f/σ _y . The fine grain steel had a higherσ _f /σ _y in the notched specimens but a lower value in the precracked specimens compared to the coarse grain steel. The scatter of toughness data can be mainly attributed to the probabilistic distribution of the weakest particle. We suggested thatσ _f /σ _y may be a useful parameter for the engineering evaluation of toughness.     

A comparison of fracture behavior of low alloy steel with different sizes of carbide particles

The fracture behaviors of low alloy steels with similar grain sizes but different sizes of carbide particles were investigated using precracked and notched specimens. The results indicate that in precracked specimens (COD), steel with coarser carbide particles has a lower toughness than steel with finer carbide particles over a temperature range from –196 °C to – 90 °C. However, in notched specimens (four-point bending (4PB) and Charpy V), these two steels shows similar toughness at low temperature where specimens are fractured by cleavage without fibrous cracking. In the transition temperature range, the steel with coarser carbide particles conversely shows a little higher toughness due to the longer extension length of the fibrous crack. This phenomenon indicates that in precracked specimens, the second-phase particles play a leading role in cleavage fracture, while in notched specimens, the grain size dominates the fracture behavior.     

Fracture behavior of C-Mn steel and weld metal in notched and precracked specimens: Part II. micromechanism of fracture

The microscopic fracture behaviors of a C-Mn steel plate and of two types of weld metal in Charpy V, crack tip opening displacement (COD), and precracked impact specimens have been studied by observations of the size distribution of the cleavage-initiating particles, the morphology of the fibrous crack zones, the microstructure in the region initiating the cleavage crack, and the size distribution of microcracks remaining in the specimens. It has been found that the different values of the microscopic cleavage fracture stress, σ_f, measured in notched and precracked specimens of the same metal result from the change in the critical event (critical length) in the fracture processes. The critical event in the Charpy V-notched specimens at —45 °C to —65 °C is the propagation of a ferrite grain-sized microcrack into the ferrite matrix; however, in the precracked COD specimens at —110 °C, it is the propagation of a second-phase particle-sized microcrack into the neighboring ferrite grain. The change of the critical event is considered to be related to the difference of effective shear stress ahead of a notch root or a crack tip. The different sensitivities to the notch acuity of the base and weld metal result from their micro-structures. Finally, the prerequisite for establishing a correlation between Charpy V and COD tests is analyzed.     

Effects of loading rate on fracture behavior of low-alloy steel with different grain sizes

Four-point bend (4PB) tests of notched specimens loaded at various loading rates, for low alloy steel with different grain sizes, were done, and the microscopic observation and finite-element method (FEM) calculations were carried out. It was found that for the coarse-grained (CG) microstructure, an appreciable drop in notch toughness with a loading rate of around 60 mm/min appeared, and further increasing the loading rate leads to a slight additional decrease in notch toughness. For the fine-grained (FG) microstructure, the effect of loading rate was not apparent. The change in toughness resulted from a change of the critical event controlling the cleavage fracture with increasing loading rate. For the CG microstructure with a lower cleavage-fracture stress (σ _f ), with an increasing loading rate, the critical event of cleavage fracture can be changed from the propagation of a pearlite colony-sized crack or a ferrite grain-sized crack, through the mixed critical events of crack propagation and crack nucleation, then to crack nucleation. This change deteriorates the toughness. For the FG microstructure with a higher cleavage-fracture stress, the critical event of cleavage fracture is the crack propagation and does not change in the loading-rate range from 120 to 500 mm/min. The measured σ _f values do not change with loading rate, as long as the critical event of cleavage fracture does not change. The higher notch toughness of the FG microstructure arises from its higher σ _f and the critical plastic strain (ε _pc ) for initiating a crack nucleus, and the fracture behavior of this FG steel is not sensitive to loading rate in the range of this work.     

Fracture behavior of C-Mn steel and weld metal in notched and precracked specimens: Part I. fracture behavior

In this investigation, fracture loads, toughness values, and the lengths of fibrous cracks on fracture surfaces were measured in Charpy V, crack tip opening displacement (COD), and precracked impact testing at various temperatures for C-Mn base steel and C-Mn and Ti-B weld metals. The uniaxial tensile properties of these metals were measured as well. By plotting the parameters related to toughness against the length of fibrous cracks measured, the energy absorbed by unit crack extension was estimated. The local cleavage fracture stresses, oy, were measured in Charpy V-notched and COD precracked specimens. The results showed σ_f about 600 MPa higher in the latter than in the former. Based on the results obtained, the factors controlling the toughness were analyzed. This was explained by the brittle transition temperature of the base metal being higher than that of the weld metal in the Charpy V test; however, it was lower in the COD test. The differences in fracture behavior between various types of toughness specimens were analyzed. The prerequisite condition for establishing the correlation between the results of Charpy V and COD tests was also discussed.     

Effects of tensile prestrain on the notch toughness of low-alloy steel

Tensile prestrains of various levels were applied to blank steel specimens. Four-point bend tests of notched specimens at various temperatures revealed an appreciable drop in the notch toughness of the specimens, which experienced 3 pct tensile prestrain. Further prestrains of up to 20 pct had a negligible effect on the notch toughness despite additional increases in the yield strength. Microscopic analyses combined with finite element method (FEM) calculations revealed that the decrease in toughness resulted from a change of the critical event controlling the cleavage fracture. The increase in yield strength provided by prestraining allowed the normal tensile stress at the notch tip to exceed the local fracture stress σ _f for propagating a just-nucleated microcrack. As a result, for the coarsegrained steel with low σ _f tested presently, the critical event was changed from tensile stress-controlled propagation of a nucleated microcrack to plastic strain-controlled nucleation of the microcrack at the notch tip. A reduction of toughness was induced as a result of this. The increase in yield strength provided by decreasing the test temperature acted in the same way.     

Study of mechanism of cleavage fracture at low temperature

In this investigation, a series of crack opening displacement (COD) tests were carried out at several low temperatures for C-Mn weld steel. Some of the specimens were loaded until fracture, and the mechanical properties and microscopic parameters on fracture surfaces were measured. Other specimens were unloaded before fracture at different applied loads. The distributions of the elongated cavities and the cleavage microcracks ahead of fatigue crack tips were observed in detail. Based on the experimental results, the combined criterion of a critical strainε _p ≥ ε_c) for initiating a crack nucleus, a critical stress triaxiality(σ _m/σ ≥ t_c) for preventing it from blunting, and a critical normal stress(σ _yy/σ_f) for the cleavage extension was proposed again, and the critical values of ε_p and σ_m/−σ for the C-Mn weld steel were measured. The reason why the minimum COD value could not be zero is explained. The mechanism of generation of the lower limit COD value on the lower shelf of the toughness transition curve is proposed.     

Observations on the effect of cementite particles on the fracture toughness of spheroidized carbon steels

The results of experimental studies of the influence of cementite particles on the fracture toughness of a number of spheroidized carbon steels at low temperatures were analyzed in terms of current theories of crack-tip behavior. The fracture toughness parameterK _IC was evaluated by using circumferentially notched and fatigue-cracked cylindrical specimens. The conclusions are summarized as follows: 1) In general,K _IC decreases with increasing volume fraction and increasing size of the carbide particles. 2) Crack initiation occurs at the carbide particles. 3) Crack propagation occurs by cleavage if the stress conditions satisfy the Ritchie, Knott and Rice criterion that a critical cleavage stress is achieved over a minimum microstructural size scale. The critical stress is that required to propagate a crack from a particle and the minimum size scale is of the order of 1 to 2 grain sizes. 4) Crack propagation occurs initially by fibrous rupture if the stress intensification is insufficient to attain the critical cleavage stress. P. Rawal was formerly affiliated.     

Variation of the fracture mode in temper embrittled 2.25 Cr-1 Mo steel

Temper embrittled 2.25 Cr-1 Mo steel was tested by slow bending of notched specimens at various temperatures, and the fracture mode was examined by SEM fractography. Comparison of the local fracture mode with the load-displacement curves showed that intergranular fracture occurred most prominently in the region where cracking initiated, but that the fracture mode tended to change to cleavage as the cracking propagated and accelerated. When the area fraction of intergranular fracture was plotted as a function of test temperature, a maximum appeared, and the temperature of this maximum tended to increase with specimen hardness. It is argued that the gap between the cleavage fracture stress (σ _F ^CL ) and that of intergranular fracture (σ _F ^IG ) was greatest at some particular temperature, allowing a maximum amount of grain boundary fracture. However, the gap (σ _F ^CL -σ _F ^IG ) diminished as cracking accelerated, and the fracture mode tended to switch to cleavage. The contrast in behavior between temper embrittled CrMo and NiCr steels is discussed.     

Effect of Solute Segregation on Fracture Toughness in a Ni-Cr Steel

A study has been made of the influence of intergranular solute segregation on fracture toughness K_1c in a series of Ni-Cr steels individually doped with Sb, Sn, and P. By means of toughness measurements in steels having two different intergranular Sb distributions, of measurements of acoustic emissions and of scanning electron micrographs of a load-interrupted and post-test-fatigued specimen, the values of K_1c, computed from the “pop-in” load of the loadvs clip gauge displacement curves, are found to represent the formation of many patches of contiguous intergranular microcracks ahead of the precrack. The present experiments demonstrate that in the early stage of solute segregation, K_1c decreases more substantially than does the strength of grain boundaries σ* (measured in the notched bar tests), although the embrittlement effects of metalloid elements are the same order for both K_1c and σ*. A proposed model for the stress-gradient-control of brittle fracture supports the finding that the measurements of K_1c give a distorted view of the progress of intergranular embrittlement.     

Correlations of microstructure with dynamic and quasi-static fracture in a plain carbon steel

An investigation was conducted into the effects of temperature, loading rate, and various micro-structural parameters on the initiation of plane strain fracture of a plain carbon AISI 1020 steel. Ferrite and prior austenite grain sizes were chosen as the principal microstructural features to be in-vestigated. The microstructural variations were accomplished by changing the austenitizing tempera-ture and by altering the cooling rate during normalization. Fracture toughness tests were conducted using precracked notched round bars loaded in tension to produce two stress intensity rates,viz.,K ₁ = 1 MPa √m s^-1 andK ₁ = 2 × 10⁶ MPa √m s^-1. In addition, Charpy impact tests along with quasistatic and high rate plasticity tests were conducted. The plasticity tests were done in torsion at shear strain rates of . Testing temperatures covered the range from -150 °C to 150 °C which encompassed fracture initiation modes involving transgranular cleavage to fully ductile fracture. Micromechanical processes involved in void and cleavage micro-crack formation were identified and quantified. For these purposes notched round tensile tests and subsequent metallographic observations along with TEM and SEM observations of the plane strain fracture toughness specimens were performed. The experimental results and quantitative micro-modeling using simple fracture models provide a means of correlating both quasistatic and dynamic fracture toughness with microstructures.     

Further study on the mechanism of the ductile-to-brittle fracture transition in C-Mn base and weld steel

In the present study, the crack opening displacement (COD) tests of specimens of C-Mn base and weld steel were carried out in the ductile-brittle transition temperature region. The majority of the specimens were fractured and others were unloaded prior to fracture after ductile fracture initiated and extended. The cavities and cleavage microcracks located in the vicinities of tips of fibrous cracks of the unloaded specimens were observed in detail. The finite element method (FEM) calculations of the stress and strain distribution ahead of the tip of an extending fibrous crack were completed. The mechanism of the ductile-to-brittle fracture transition was further investigated. It was revealed that in the ductile-brittle transition temperature region, the ductile fracture process was independent of temperature. The ductile-to-brittle fracture transition was triggered by initiating a catastrophic extension of a cleavage crack ahead of the fibrous crack tip, which occurred in a condition satisfying a combined criterion composed of three items, i.e., ε _p ≥ ε _pc for initiating a crack nucleus; σ _m √σ ≥ T _c for preventing the crack nucleus from blunting; and σ _yy ≥ σ _f for propagating the crack nucleus. For a specimen in which a fibrous crack occurred and propagated, the critical event for initiating a brittle cleavage fracture was the propagation of a ferrite grain-sized crack into neighboring grains. With extension of a fibrous crack, the behavior of the ductile-to-brittle fracture transition could be analyzed by the effect of the size of an “active zone” on the initiation of the brittle cleavage fracture.     

Effect of TiN particles and microstructure on fracture toughness in simulated heat-affected zones of a structural steel

Thermally stable TiN particles can effectively pin austenite grain boundaries in weld heat-affected zones (HAZs), thereby improving toughness, but can also act as cleavage initiators. The HAZs simulated in a GLEEBLE 1500 TCS using two peak temperatures (T _p ) and three cooling times (Δ∼ _8/5) have determined the effects of matrix microstructure and TiN particle distribution on the fracture toughness (crack tip opening displacement (CTOD)) of three steels microalloyed with 0.006, 0.045, and 0.1 wt pct Ti. Coarse TiN (0.5 to 6 μm) particles are identified in steels with the two higher levels of Ti, and fine Ti(C, N) (35 to 500 nm) particles were present in all three steels. Large prior austenite grain size caused by higher T _p decreased fracture toughness considerably in steels containing coarse TiN particles but had little effect in their absence. Fracture toughness was largely independent of matrix microstructure in the presence of coarse particles. Cleavage fracture initiation was observed to occur at coarse TiN particles in the samples with a large prior austenite grain size. Alloy thermodynamics have been used to rationalize the influence of Ti content on TiN formation and its size.     

Effects of test temperature and grain size on the charpy impact toughness and dynamic toughness (<Emphasis Type="Italic">K</Emphasis><Subscript><Emphasis Type="Italic">ID</Emphasis></Subscript>) of polycrystalline niobium

The effects of changes in test temperature (−196 °C to 25 °C) and grain size (40 to 165 μm) on the dynamic cleavage fracture toughness (K _ID ) and Charpy impact toughness of polycrystalline niobium (Nb) have been investigated. The ductile-to-brittle transition was found to be affected by both changes in grain size and the severity of stress concentration (i.e., notch vs fatigue-precrack). In addition to conducting impact tests on notched and fatigue-precracked Charpy specimens, extensive fracture surface analyses have been performed in order to determine the location of apparent cleavage nucleation sites and to rationalize the effects of changes in microstructure and experimental variables on fracture toughness. Existing finite element analyses and the stress field distributions ahead of stress concentrators are used to compare the experimental observations with the predictions of various fracture models. The dynamic cleavage fracture toughness, K _ID , was shown to be 37±4 MPa√m and relatively independent of grain size (i.e., 40 to 105 μm) and test temperature over the range −196 °C to 25 °C.     

Critical assessment of the local cleavage stress σ ƒ * in notch specimens of C-Mn steel

An elastic-plastic finite element method (FEM) was used to calculate the stress and strain distributions ahead of notches with various root radii in a bending specimen of C-Mn steel with grain sizes of 10 and 30 μm. By accurately measuring the distance of the cleavage initiation site from the root of the notch, the local cleavage stress σ _ƒ ^* was measured. When the notch radius increased from 0.25 to 1.0 mm, the distribution of high stress had a definite variation but the σ _ƒ ^* remained relatively constant. In notch specimens with different root radii, the critical fracture event is identical,i.e., propagation of a ferrite grain-sized crack into the neighboring matrix. Therefore, the σ _ƒ ^* is mainly determined by the length of the critical microcrack, here, the size of ferrite grain instead of the high stress volume for finding an eligible brittle particle. The critical strain for initiating a crack was about 1 pct. The cleavage site ahead of a notch was related to the relative distributions of stress and strain and the random distribution of the weakest grains. The higher fracture load of the fine-grain material can be attributed to its higher value of σ _ƒ ^* /σ_o as compared with the coarse-grain. The σ _ƒ ^* /σ_o is a potential engineering parameter for toughness assessment in notch specimens.     

Microstructural effects on the cleavage fracture stress of fully pearlitic eutectoid steel

The microstructural parameter(s) controlling the critical cleavage fracture stress, σ_F, of fully pearlitic eutectoid steel have been investigated. Independent variation of the pearlite interlamellar spacing,S _p, and the prior austenite grain size were accomplished through heat treatment. Critical cleavage fracture stresses were measured on bluntly-notched bend specimens tested over the temperature range -125 °C to 23 °C. The cleavage fracture stress increased with decreasingS _p, and was independent of prior austenite grain size. Fine pearlitic microstructures exhibited temperature, strain-rate, and notched-bar geometry independent values for σ_F, consistent with propagation-controlled cleavage fracture. Coarse pearlitic specimens exhibited temperature-dependent values for σ_F over a similar temperature range. Inclusion-initiated fractures were generally located at or beyond the location of the peak normal stress in the bend bar, while cracking associated with pearlite colonies was observed to be closer to the notch than the predicted peak stress location. The calculated values for σ_F were independent of both the type and location of initiation site(e. g., inclusion, pearlite colony). Thus, although inclusions may provide potent fracture initiation sites, their presence or absence does not necessarily change σ_F in fully pearlitic microstructures. formerly Graduate Student, Carnegie Mellon University     

Effect of strontium on the microstructure, mechanical properties, and fracture behavior of AZ31 magnesium alloy

The effect of strontium (Sr) on the microstructure, mechanical properties, and fracture behavior of AZ31 magnesium alloy and its sensitivity to cooling rate are investigated. Three phases—blocky-shaped Mg₁₇Al₁₂, acicular Mg₂₀Al₂₀Mn₅Sr, and insular Mg₁₆(Al,Zn)₂Sr—are identified in the Sr-containing AZ31 alloys. With increasing cooling rate, the blocky-shaped Mg₁₇Al₁₂ phase increases, the acicular Mg₂₀Al₂₀Mn₅Sr phase diminishes, and the insular Mg₁₆(Al,Zn)₂Sr phase is refined and granulated. The study suggests that the grain size decreases with increasing cooling rate for a given composition. However, the grain size decreases first, then increases, and finally decreases again with increasing Sr for a given cooling rate. The yield strength (σ _y ) of AZ31 magnesium alloy can be improved by grain refinement and expressed as σ _y =35.88+279.13d ^−1/2 according to the Hall-Petch relationship. The elongation increases when Sr is added up to 0.01 pct and then decreases with increasing Sr addition. Grain refinement changes the fracture behavior from quasicleavage failure for the original AZ31 alloy to mixed features of quasicleavage and microvoid coalescence fracture.     

Fracture toughness of the lean duplex stainless steel LDX 2101

Fracture toughness testing was performed on the recently developed lean duplex stainless steel LDX 2101 (EN 1.4162, UNS S32101). The results were evaluated by master curve analysis, including deriving a reference temperature. The master curve approach, originally developed for ferritic steels, has been used successfully. The reference temperature corresponds to a fracture toughness of 100 MPa√m, which characterizes the onset of cleavage cracking at elastic or elastic-plastic instabilities. The reference temperature, T ₀, was −112 °C and −92 °C for the base and weld materials, respectively. In addition, the fracture toughness is compared with impact toughness results. Complementary crack tip opening displacements (CTODs) have also been calculated. The toughness properties found in traditional duplex stainless steels (DSS) are generally good. The current study verifies a high fracture toughness for both base and weld materials and for the low alloyed grade LDX 2101. Even though the fracture toughness was somewhat lower than for duplex stainless steel 2205, it is still sufficiently high for most low-temperature applications.